Benzonitrile, 3-amino-4-nitro-

Product Name: Benzonitrile, 3-amino-4-nitro-
CAS No.: 99512-10-4
Chemical Name: Benzonitrile, 3-amino-4-nitro-
Synonyms: 3-amino-4-nitrobenzonitrile;Benzonitrile, 3-amino-4-nitro-
CBNumber: CB01865545
Molecular Formula: C7H5N3O2
Formula Weight: 163.13
MOL File: 99512-10-4.mol

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Benzonitrile, 3-amino-4-nitro- Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Yellow to orange Solid

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Safety

RIDADR: 3439
HazardClass: 6.1
PackingGroup: Ⅲ

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: A615095
Product name: 3-Amino-4-nitrobenzonitrile
Packaging: 500mg
Price: $70
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA140196
Product name: 3-Amino-4-nitrobenzonitrile
Packaging: 1g
Price: $63
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA140196
Product name: 3-Amino-4-nitrobenzonitrile
Packaging: 2g
Price: $109
Updated: 2021/12/16

AK Scientific

Product number: W9876
Product name: 3-Amino-4-nitrobenzonitrile
Packaging: 1g
Price: $117
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA140196
Product name: 3-Amino-4-nitrobenzonitrile
Packaging: 5G
Price: $217
Updated: 2021/12/16

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Benzonitrile, 3-amino-4-nitro- Chemical Properties,Usage,Production

Synthesis

1635-61-6

99512-10-4

5-Chloro-2-nitroaniline (6.902 g, 40 mmol) was used as a raw material and mixed with Zn(CN)2 (2.818 g, 24 mmol) and Pd(PPh3)4 (2.311 g, 2 mmol) in DMF (40 mL). The reaction mixture was heated to 120 °C for 4 days. After completion of the reaction, it was cooled to room temperature. The reaction mixture was partitioned between ethyl acetate and water. The organic layer was separated, washed with brine, dried (MgSO4), filtered, and concentrated under vacuum. The residue was purified by fast column chromatography on silica gel using 4:1 hexane/ethyl acetate as eluent to give 1.49 g (23% yield) of 3-amino-4-nitrobenzonitrile.

References

[1] Patent: WO2004/76424, 2004, A1. Location in patent: Page 268

Benzonitrile, 3-amino-4-nitro- Preparation Products And Raw materials

Raw materials

Preparation Products

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Benzonitrile, 3-amino-4-nitro- Suppliers

China 34 Europe 1 Germany 1 India 1 United Kingdom 1 United States 5 Global 43

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