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1-amino-2-naphthonitrile

Product Name
1-amino-2-naphthonitrile
CAS No.
3100-67-2
Chemical Name
1-amino-2-naphthonitrile
Synonyms
CPD0714;1-amino-2-naphthonitrile;1-Amino-2-Cyanonaphthalene;1-amino-2-naphthalenecarbonitrile;2-Naphthalenecarbonitrile, 1-amino-
CBNumber
CB01886841
Molecular Formula
C11H8N2
Formula Weight
168.19
MOL File
3100-67-2.mol
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1-amino-2-naphthonitrile Property

Melting point:
191-192 °C(Solv: water (7732-18-5); benzene (71-43-2))
Boiling point:
151-152 °C(Press: 0.3 Torr)
Density 
1.22±0.1 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
-0.32±0.10(Predicted)
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A578475
Product name
1-Amino-2-naphthonitrile
Packaging
100mg
Price
$220
Updated
2021/12/16
Ambeed
Product number
A417494
Product name
1-Amino-2-naphthonitrile
Purity
98+%
Packaging
100mg
Price
$15
Updated
2021/12/16
Ambeed
Product number
A417494
Product name
1-Amino-2-naphthonitrile
Purity
98+%
Packaging
250mg
Price
$34
Updated
2021/12/16
Ambeed
Product number
A417494
Product name
1-Amino-2-naphthonitrile
Purity
98+%
Packaging
1g
Price
$94
Updated
2021/12/16
Crysdot
Product number
CD12085035
Product name
1-Amino-2-naphthonitrile
Purity
95+%
Packaging
1g
Price
$231
Updated
2021/12/16
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1-amino-2-naphthonitrile Chemical Properties,Usage,Production

Synthesis

86-57-7

105-56-6

3100-67-2

General procedure for the synthesis of 1-amino-2-cyano naphthalene from 1-nitronaphthalene and ethyl cyanoacetate: In a dry 2L reactor, 139.8 g (1.236 mol) of ethyl cyanoacetate, 29.5 g (0.453 mol) of potassium cyanide, 46.2 g (0.824 mol) of potassium hydroxide, and 920 mL of dimethylformamide were added, and dissolved with stirring at 10 °C. Stirring was continued for 20 minutes under nitrogen protection. Subsequently, the reaction mixture was heated to 60°C and the reaction was stirred for 4 hours. Upon completion of the reaction, the reaction solvent was concentrated and 600 mL of 10% aqueous sodium hydroxide solution was added and stirred under reflux conditions for 1 hour. The reaction mixture was filtered and purified by column chromatography using dichloromethane and heptane as eluents to give 50 g (yield: 60%) of the target product labeled as [Intermediate 1-a].

References

[1] Patent: KR2015/111106, 2015, A. Location in patent: Paragraph 0259-0262
[2] Patent: KR2016/2328, 2016, A. Location in patent: Paragraph 0476
[3] Patent: KR2015/144120, 2015, A. Location in patent: Paragraph 0310-0313
[4] Patent: KR2018/10087, 2018, A. Location in patent: Paragraph 0578-0582
[5] Pest Management Science, 2001, vol. 57, # 7, p. 625 - 632

1-amino-2-naphthonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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1-amino-2-naphthonitrile Suppliers

ShangHai Caerulum Pharma Discovery Co., Ltd.
Tel
18149758185 18149758185
Email
sales-cpd@caerulumpharma.com
Country
China
ProdList
3505
Advantage
58
Finetech Industry Limited
Tel
027-87465837 19945049750
Fax
027-8777-2287
Email
sales@finetechnology-ind.com
Country
China
ProdList
9548
Advantage
58
Cool Pharm, Ltd
Tel
021-60455363 18019463053
Fax
50966098
Email
sales@coolpharm.com
Country
China
ProdList
12346
Advantage
58
Shanghai SuperLan Chemcial Technique Centre
Tel
0-2022843681 15618226720
Fax
+86-21-51601218
Email
chaolaichem@foxmail.com
Country
China
ProdList
9955
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Suzhou Shanyang Pharmaceutical Technology Co.,
Tel
0512-63268889 18506119477
Email
82169840@qq.com
Country
China
ProdList
603
Advantage
58
Aikon International Limited
Tel
025-58859352 15955137747
Fax
02557626880
Email
sales01@aikonchem.com
Country
China
ProdList
16027
Advantage
58
SHANGHAI FDC-CHEMICAL CO.,LTD
Tel
021-61469567 13482353728
Fax
021-61161605
Email
sales@fdc-chemical.com
Country
China
ProdList
9964
Advantage
58
Jinan Yaoyan Pharmaceutical Co., Ltd.
Tel
Fax
-
Email
jnyaoyan@163.com
Country
China
ProdList
3069
Advantage
58
Shanghai Aocheng Biological Technology Co., Ltd.
Tel
13917627064
Fax
-qq:56229367
Email
56229367@qq.com
Country
China
ProdList
642
Advantage
58
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View Lastest Price from 1-amino-2-naphthonitrile manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
1-amino-2-naphthonitrile 3100-67-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-08-11
Career Henan Chemical Co
Product
1-amino-2-naphthonitrile 3100-67-2
Price
US $1.00/KG
Min. Order
1KG
Purity
98% HPLC
Supply Ability
10 tons/month
Release date
2020-01-09

3100-67-2, 1-amino-2-naphthonitrileRelated Search:


  • 1-amino-2-naphthonitrile
  • 2-Naphthalenecarbonitrile, 1-amino-
  • 1-amino-2-naphthalenecarbonitrile
  • 1-Amino-2-Cyanonaphthalene
  • CPD0714
  • 3100-67-2