1-amino-2-naphthonitrile
- Product Name
- 1-amino-2-naphthonitrile
- CAS No.
- 3100-67-2
- Chemical Name
- 1-amino-2-naphthonitrile
- Synonyms
- CPD0714;1-amino-2-naphthonitrile;1-Amino-2-Cyanonaphthalene;1-amino-2-naphthalenecarbonitrile;2-Naphthalenecarbonitrile, 1-amino-
- CBNumber
- CB01886841
- Molecular Formula
- C11H8N2
- Formula Weight
- 168.19
- MOL File
- 3100-67-2.mol
1-amino-2-naphthonitrile Property
- Melting point:
- 191-192 °C(Solv: water (7732-18-5); benzene (71-43-2))
- Boiling point:
- 151-152 °C(Press: 0.3 Torr)
- Density
- 1.22±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- -0.32±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A578475
- Product name
- 1-Amino-2-naphthonitrile
- Packaging
- 100mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- A417494
- Product name
- 1-Amino-2-naphthonitrile
- Purity
- 98+%
- Packaging
- 100mg
- Price
- $15
- Updated
- 2021/12/16
- Product number
- A417494
- Product name
- 1-Amino-2-naphthonitrile
- Purity
- 98+%
- Packaging
- 250mg
- Price
- $34
- Updated
- 2021/12/16
- Product number
- A417494
- Product name
- 1-Amino-2-naphthonitrile
- Purity
- 98+%
- Packaging
- 1g
- Price
- $94
- Updated
- 2021/12/16
- Product number
- CD12085035
- Product name
- 1-Amino-2-naphthonitrile
- Purity
- 95+%
- Packaging
- 1g
- Price
- $231
- Updated
- 2021/12/16
1-amino-2-naphthonitrile Chemical Properties,Usage,Production
Synthesis
86-57-7
105-56-6
3100-67-2
General procedure for the synthesis of 1-amino-2-cyano naphthalene from 1-nitronaphthalene and ethyl cyanoacetate: In a dry 2L reactor, 139.8 g (1.236 mol) of ethyl cyanoacetate, 29.5 g (0.453 mol) of potassium cyanide, 46.2 g (0.824 mol) of potassium hydroxide, and 920 mL of dimethylformamide were added, and dissolved with stirring at 10 °C. Stirring was continued for 20 minutes under nitrogen protection. Subsequently, the reaction mixture was heated to 60°C and the reaction was stirred for 4 hours. Upon completion of the reaction, the reaction solvent was concentrated and 600 mL of 10% aqueous sodium hydroxide solution was added and stirred under reflux conditions for 1 hour. The reaction mixture was filtered and purified by column chromatography using dichloromethane and heptane as eluents to give 50 g (yield: 60%) of the target product labeled as [Intermediate 1-a].
References
[1] Patent: KR2015/111106, 2015, A. Location in patent: Paragraph 0259-0262
[2] Patent: KR2016/2328, 2016, A. Location in patent: Paragraph 0476
[3] Patent: KR2015/144120, 2015, A. Location in patent: Paragraph 0310-0313
[4] Patent: KR2018/10087, 2018, A. Location in patent: Paragraph 0578-0582
[5] Pest Management Science, 2001, vol. 57, # 7, p. 625 - 632
1-amino-2-naphthonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
1-amino-2-naphthonitrile Suppliers
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View Lastest Price from 1-amino-2-naphthonitrile manufacturers
- Product
- 1-amino-2-naphthonitrile 3100-67-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-11
- Product
- 1-amino-2-naphthonitrile 3100-67-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons/month
- Release date
- 2020-01-09