ChemicalBook > CAS DataBase List > 4-Phenyl-4H-1,2,4-triazole

4-Phenyl-4H-1,2,4-triazole

Product Name: 4-Phenyl-4H-1,2,4-triazole
CAS No.: 16227-12-6
Chemical Name: 4-Phenyl-4H-1,2,4-triazole
Synonyms: Brn 0115833;4-Phenyl-1,2,4-triazole;1-Phenyl-1,3,4-triazole;4-Phenyl-4H-1,2,4-triazole;4-Phenyl-1H-1,2,4-triazole;1H-1,2,4-Triazole, 4-phenyl-;4H-1,2,4-Triazole, 4-phenyl-;4-phenyl-1,2,4-triazolidin-4-ium;4-phenyl-1,2,4-triazol-4-yl)phenol
CBNumber: CB02360186
Molecular Formula: C8H7N3
Formula Weight: 145.16
MOL File: 16227-12-6.mol

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4-Phenyl-4H-1,2,4-triazole Property

Melting point:: 122 °C
Boiling point:: 292℃
Density: 1.16
Flash point:: 131℃
storage temp.: Sealed in dry,Room Temperature
pka: 2.52±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 8231AA
Product name: 4-Phenyl-4H-1,2,4-triazole
Packaging: 100mg
Price: $163
Updated: 2021/12/16

Ark Pharm

Product number: AK102376
Product name: 4-Phenyl-4H-1,2,4-triazole
Purity: 98%
Packaging: 250mg
Price: $69
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM1037986
Product name: 4-PHENYL-1H-1,2,4-TRIAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $497.05
Updated: 2021/12/16

AK Scientific

Product number: 8231AA
Product name: 4-Phenyl-4H-1,2,4-triazole
Packaging: 1g
Price: $502
Updated: 2021/12/16

Ambeed

Product number: A403811
Product name: 4-Phenyl-4H-1,2,4-triazole
Purity: 98%
Packaging: 1g
Price: $147
Updated: 2021/12/16

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4-Phenyl-4H-1,2,4-triazole Chemical Properties,Usage,Production

Synthesis

591-50-4

288-88-0

16227-12-6

General method: iodobenzene (1.2 mmol), 1,2,4-triazole (1.0 mmol), cesium carbonate (2 mmol) and Cu(OAc)2-H2O (0.01 mmol) were dissolved in N,N-dimethylformamide (2 mL) under nitrogen protection. The reaction mixture was stirred at 110 °C for 24 hours. After completion of the reaction, it was cooled to room temperature and the mixture was partitioned between water and ethyl acetate. The organic phase was separated and the aqueous phase was extracted with ethyl acetate. The organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford the target product 4-phenyl-4H-1,2,4-triazole.

References

[1] Tetrahedron, 2011, vol. 67, # 29, p. 5282 - 5288

4-Phenyl-4H-1,2,4-triazole Preparation Products And Raw materials

Raw materials

Preparation Products

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16227-12-6, 4-Phenyl-4H-1,2,4-triazoleRelated Search:

Alprazolam Triazolam Tricyclazole ALPRAZOLAM-D5 1,2,4-TRIAZOLO[4,3-A]QUINOLINE 4-(4-CHLORO-PHENYL)-5-(4-TRIFLUOROMETHOXY-PHENYL)-4H-[1,2,4]TRIAZOLE-3-THIOL 4-(2-CHLORO-PHENYL)-5-(4-TRIFLUOROMETHOXY-PHENYL)-4H-[1,2,4]TRIAZOLE-3-THIOL 4-(4-METHOXYPHENYL)-5-[4-(TRIFLUOROMETHOXY)PHENYL]-4H-1,2,4-TRIAZOLE-3-THIOL 4-(2,4-DICHLOROPHENYL)-5-(1-METHYL-1H-PYRROL-2-YL)-4H-1,2,4-TRIAZOLE-3-THIOL 4-(4-CHLORO-PHENYL)-5-(3,4-DIMETHOXY-BENZYL)-4H-[1,2,4]TRIAZOLE-3-THIOL 3-(BENZYLTHIO)-1,4-DIPHENYL-1H-1,2,4-TRIAZOL-4-IUM CHLORIDE 2-([5-[(2,6-DICHLOROBENZYL)THIO]-4-(3,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOL-3-YL]METHYL)-5-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-2H-1,2,3,4-TETRAAZOLE 5-(3,4-DIMETHOXY-BENZYL)-4-(3-TRIFLUOROMETHYL-PHENYL)-4H-[1,2,4]TRIAZOLE-3-THIOL 1,4-DIPHENYL-1H-1,2,4-TRIAZOL-4-IUM-3-THIOLATE 5-(4-METHOXY-PHENYL)-4-(3-TRIFLUOROMETHYL-PHENYL)-4H-[1,2,4]TRIAZOLE-3-THIOL 5-([(2,6-DICHLORO-4-PYRIDYL)METHYL]THIO)-4-PHENYL-4H-1,2,4-TRIAZOL-3-OL 1,4,5-TRIPHENYL-4H-1,2,4-TRIAZOL-1-IUM-3-THIOLATE BUTTPARK 61\40-40

4-phenyl-1,2,4-triazol-4-yl)phenol

4-Phenyl-4H-1,2,4-triazole

1H-1,2,4-Triazole, 4-phenyl-

4-Phenyl-1H-1,2,4-triazole

Brn 0115833

4H-1,2,4-Triazole, 4-phenyl-

1-Phenyl-1,3,4-triazole

4-Phenyl-1,2,4-triazole

4-phenyl-1,2,4-triazolidin-4-ium

16227-12-6