5-PHENYLPICOLINIC ACID

Product Name: 5-PHENYLPICOLINIC ACID
CAS No.: 75754-04-0
Chemical Name: 5-PHENYLPICOLINIC ACID
Synonyms: 5-PHENYLPICOLINIC ACID;5-Phenylpyridine-2-carboxylic;5-(4-Ethylphenyl)-picolinic acid;5-(4-Methylphenyl)-picolinic acid;5-(2-Methylphenyl)-picolinic acid;5-(3-Methylphenyl)-picolinic acid;5-Phenylpyridine-2-carboxylic 5-(3-Methoxyphenyl)-picolinic acid;5-(2-Methoxyphenyl)-picolinic acid;5-PHENYLPYRIDINE-2-CARBOXYLIC ACID
CBNumber: CB0238674
Molecular Formula: C12H9NO2
Formula Weight: 199.21
MOL File: 75754-04-0.mol

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5-PHENYLPICOLINIC ACID Property

Melting point:: 156-157℃
Boiling point:: 399℃
Density: 1.241
Flash point:: 195℃
storage temp.: 2-8°C
form: solid
pka: 0.95±0.50(Predicted)
color: White
CAS DataBase Reference: 75754-04-0

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Safety

Risk Statements: 22-36/37/38
Safety Statements: 22-26-36/37/39
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P336368
Product name: 5-PhenylpicolinicAcid
Packaging: 100mg
Price: $90
Updated: 2021/12/16

TRC

Product number: P336368
Product name: 5-PhenylpicolinicAcid
Packaging: 500mg
Price: $330
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0012877
Product name: 5-PHENYLPYRIDINE-2-CARBOXYLIC ACID
Purity: 95.00%
Packaging: 100MG
Price: $613.88
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H21-1-E3
Product name: 5-Phenylpyridine-2-carboxylic acid
Purity: 95%
Packaging: 250mg
Price: $148
Updated: 2021/12/16

AK Scientific

Product number: V7627
Product name: 5-Phenylpicolinicacid
Packaging: 250mg
Price: $151
Updated: 2021/12/16

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5-PHENYLPICOLINIC ACID Chemical Properties,Usage,Production

Synthesis

86574-52-9

75754-04-0

Methyl 5-phenylpyridinecarboxylate (120 mg) was used as a raw material and dissolved in a solvent mixture of tetrahydrofuran (5 mL) and water (5 mL). Lithium hydroxide (100 mg) was added to the solution and the reaction mixture was stirred for 16 hours at room temperature. Upon completion of the reaction, water was added to the reaction solution and extracted with ethyl acetate. The aqueous layer was separated, its pH was adjusted to 6 with hydrochloric acid and extracted again with ethyl acetate. The organic layers were combined, washed with saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by distillation under reduced pressure to give 100 mg of 5-phenylpyridinecarboxylic acid in 89% yield.

References

[1] Patent: JP2017/171619, 2017, A. Location in patent: Paragraph 0103; 0107
[2] Journal of Medicinal Chemistry, 2011, vol. 54, # 13, p. 4721 - 4734

5-PHENYLPICOLINIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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5-PHENYLPICOLINIC ACID Suppliers

Belgium 1 China 35 Germany 1 India 3 United Kingdom 1 United States 6 Global 47

J & K SCIENTIFIC LTD.

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Thermo Fisher Scientific

Tel: 800-810-5118
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Country: China
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9ding chemical ( Shanghai) Limited

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SynAsst Chemical.

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Country: China
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Synchem OHG

Tel: +49 5662 408730
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View Lastest Price from 5-PHENYLPICOLINIC ACID manufacturers

Career Henan Chemical Co

Product: 5-PHENYLPICOLINIC ACID 75754-04-0
Price: US $1.00/KG
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-10

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