ChemicalBook > CAS DataBase List > 3-CHLORO-2-METHOXYBENZALDEHYDE

3-CHLORO-2-METHOXYBENZALDEHYDE

Product Name
3-CHLORO-2-METHOXYBENZALDEHYDE
CAS No.
223778-54-9
Chemical Name
3-CHLORO-2-METHOXYBENZALDEHYDE
Synonyms
3-CHLORO-2-METHOXYBENZALDEHYDE;Benzaldehyde,3-chloro-2-methoxy-;4-Fluoro-3-(trifluoromethyl)phenacyl bromide[2-Bromo-4'-fluoro-4'-(trifluoromethyl)acetophenone
CBNumber
CB02453709
Molecular Formula
C8H7ClO2
Formula Weight
170.59
MOL File
223778-54-9.mol
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3-CHLORO-2-METHOXYBENZALDEHYDE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
solid
Appearance
White to yellow Solid-Liquid Mixture
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C360410
Product name
3-Chloro-2-methoxybenzaldehyde
Packaging
250mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
072380
Product name
3-Chloro-2-methoxybenzaldehyde
Purity
95+%
Packaging
500mg
Price
$82
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC144230
Product name
3-Chloro-2-methoxybenzaldehyde
Packaging
500mg
Price
$85
Updated
2021/12/16
ChemScene
Product number
CS-W006013
Product name
3-Chloro-2-methoxybenzaldehyde
Purity
97.08%
Packaging
5g
Price
$97
Updated
2021/12/16
AK Scientific
Product number
J94656
Product name
3-Chloro-2-methoxybenzaldehyde
Packaging
5g
Price
$120
Updated
2021/12/16
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3-CHLORO-2-METHOXYBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

869088-29-9

223778-54-9

General procedure for the synthesis of 3-chloro-2-methoxybenzaldehyde from 3-chloro-2-methoxybenzyl alcohol: Manganese dioxide (16 g, 184 mmol) was added to a solution of 3-chloro-2-methoxybenzyl alcohol (5.68 g, 33 mmol) in dichloromethane (300 mL). The reaction mixture was heated at 45°C for 2.5 hours followed by stirring at room temperature for 18 hours. Upon completion of the reaction, the mixture was filtered through Arbocel (R) and the filter cake was washed with dichloromethane. After combining the filtrates, it was concentrated under reduced pressure to give 3-chloro-2-methoxybenzaldehyde as a yellow oil in 92% (5.2 g) yield. The product was characterized by 1H NMR (CDCl3, 400 MHz) with chemical shifts of δ 4.02 (s, 3H), 7.19 (m, 1H), 7.63 (d, 1H), 7.79 (d, 1H), 10.40 (s, 1H).

References

[1] Patent: US2005/250775, 2005, A1. Location in patent: Page/Page column 32

3-CHLORO-2-METHOXYBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-CHLORO-2-METHOXYBENZALDEHYDE Suppliers

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View Lastest Price from 3-CHLORO-2-METHOXYBENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
3-Chloro-2-methoxybenzaldehyde 223778-54-9
Price
US $1.00/KG
Min. Order
1KG
Purity
Min98% HPLC
Supply Ability
g/kg/ton
Release date
2020-01-30

223778-54-9, 3-CHLORO-2-METHOXYBENZALDEHYDERelated Search:

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  • 3-CHLORO-2-METHOXYBENZALDEHYDE
  • Benzaldehyde,3-chloro-2-methoxy-
  • 4-Fluoro-3-(trifluoromethyl)phenacyl bromide[2-Bromo-4'-fluoro-4'-(trifluoromethyl)acetophenone
  • 223778-54-9