ChemicalBook > CAS DataBase List > 4-IODOISOXAZOLE

4-IODOISOXAZOLE

Product Name
4-IODOISOXAZOLE
CAS No.
847490-69-1
Chemical Name
4-IODOISOXAZOLE
Synonyms
4-IODOISOXAZOLE;4-Lodoisoxazole;Isoxazole, 4-iodo-;4-iodo-1,2-oxazole
CBNumber
CB02453769
Molecular Formula
C3H2INO
Formula Weight
194.96
MOL File
847490-69-1.mol
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4-IODOISOXAZOLE Property

Boiling point:
214.8±13.0 °C(Predicted)
Density 
2.227±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Store in freezer, under -20°C
pka
-3.78±0.50(Predicted)
form 
solid
color 
Yellow
InChI
InChI=1S/C3H2INO/c4-3-1-5-6-2-3/h1-2H
InChIKey
BKACOOKVHZFHEW-UHFFFAOYSA-N
SMILES
O1C=C(I)C=N1
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Safety

HS Code 
2934999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H317May cause an allergic skin reaction

H371May cause damage to organs

H373May cause damage to organs through prolonged or repeated exposure

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
I708108
Product name
4-Iodoisoxazole
Packaging
500mg
Price
$110
Updated
2021/12/16
Matrix Scientific
Product number
072483
Product name
4-Iodoisoxazole
Purity
95+%
Packaging
1g
Price
$153
Updated
2021/12/16
AK Scientific
Product number
W8742
Product name
4-Iodoisoxazole
Packaging
1g
Price
$181
Updated
2021/12/16
Matrix Scientific
Product number
072483
Product name
4-Iodoisoxazole
Purity
95+%
Packaging
5g
Price
$450
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0104962
Product name
4-IODO-ISOXAZOLE
Purity
95.00%
Packaging
1G
Price
$1034.88
Updated
2021/12/16
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4-IODOISOXAZOLE Chemical Properties,Usage,Production

Synthesis

288-14-2

847490-69-1

Synthesis of Intermediate 46: 3-(Isoxazol-4-yl)benzaldehyde: Step 1: Synthesis of 4-iodoisoxazole: To a solution of N-iodosuccinimide (NIS, 23.0 g, 100 mmol) in trifluoroacetic acid (TFA, 200 mL) was added isoxazole (6.9 g, 100 mmol) all at once at room temperature. The reaction mixture was stirred for 18 hours. After completion of the reaction, the mixture was partitioned between petroleum ether (PE, 200 mL) and water (1000 mL). The organic phase was separated, washed with saturated sodium bisulfate solution, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give the yellow solid product 4-iodoisoxazole (1.2 g, 7% yield).

References

[1] Angewandte Chemie - International Edition, 2016, vol. 55, # 43, p. 13580 - 13584
[2] Angew. Chem., 2016, vol. 128, p. 13778 - 13782,5
[3] Patent: US2006/46991, 2006, A1. Location in patent: Page/Page column 50
[4] Patent: WO2006/21886, 2006, A1. Location in patent: Page/Page column 83
[5] Patent: WO2011/38204, 2011, A1. Location in patent: Page/Page column 150

4-IODOISOXAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODOISOXAZOLE Suppliers

China 55 India 2 United States 6 Global 63
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View Lastest Price from 4-IODOISOXAZOLE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
4-IODOISOXAZOLE 847490-69-1
Price
US $10.00/KG
Min. Order
100KG
Purity
99%
Supply Ability
100 mt
Release date
2024-11-22
Career Henan Chemical Co
Product
4-IODOISOXAZOLE 847490-69-1
Price
US $1.00/KG
Min. Order
1KG
Purity
98%-99.9%
Supply Ability
200kg
Release date
2020-01-10

847490-69-1, 4-IODOISOXAZOLERelated Search:

4-IODO-5-METHYL-ISOXAZOLE 4-IODO-3-METHYL-5-PHENYLISOXAZOLE 4-IODO-3-ISOPROPOXY-ISOXAZOLE-5-CARBONITRILE 4-Iodo-3,5-dimethylisoxazole 3-TERT-BUTYL-4-IODO-5-PHENYLISOXAZOLE 3-Amino-4-iodo-5-methylisoxazole 4-IODO-3-PHENYL-5-TRIISOPROPYLSILANYLISOXAZOLE 4-iodo-3-methylisoxazol-5-amine 5-TERT-BUTYL-4-IODO-3-PHENYLISOXAZOLE 4-IODO-3,5-DIPHENYLISOXAZOLE 4-IODO-5-METHYL-3-PHENYLISOXAZOLE 4-IODO-5-PHENYLISOXAZOLE 3-(4-IODO-5-PHENYLISOXAZOL-3-YL)-1-METHYLINDOLE 5-CYCLOHEX-1-ENYL-4-IODO-3-PHENYLISOXAZOLE 3-HEXYL-4-IODO-5-PHENYLISOXAZOLE 4-IODOISOXAZOLE

  • 4-Lodoisoxazole
  • 4-IODOISOXAZOLE
  • 4-iodo-1,2-oxazole
  • Isoxazole, 4-iodo-
  • 847490-69-1
  • C3H2INO