3,5-DIBROMO-4-CHLOROPYRIDINE
- Product Name
- 3,5-DIBROMO-4-CHLOROPYRIDINE
- CAS No.
- 13626-17-0
- Chemical Name
- 3,5-DIBROMO-4-CHLOROPYRIDINE
- Synonyms
- 3,5-Dibromo-4-chL;4-Chloro-3,5-dibroMopyridine;3,5-DIBROMO-4-CHLOROPYRIDINE;Pyridine, 3,5-dibromo-4-chloro-;3,5-DIBROMO-4-CHLOROPYRIDINE ISO 9001:2015 REACH
- CBNumber
- CB0246062
- Molecular Formula
- C5H2Br2ClN
- Formula Weight
- 271.34
- MOL File
- 13626-17-0.mol
3,5-DIBROMO-4-CHLOROPYRIDINE Property
- Melting point:
- 98 °C
- Boiling point:
- 256.4±35.0 °C(Predicted)
- Density
- 2.136±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 0.30±0.10(Predicted)
- Appearance
- Off-white to light yellow Solid
- CAS DataBase Reference
- 13626-17-0
N-Bromosuccinimide Price
- Product number
- ADE001379
- Product name
- 3,5-Dibromo-4-chloropyridine
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $783
- Updated
- 2025/07/31
- Product number
- B426208
- Product name
- 3,5-Dibromo-4-chloropyridine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B426208
- Product name
- 3,5-Dibromo-4-chloropyridine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B426208
- Product name
- 3,5-Dibromo-4-chloropyridine
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- J96554
- Product name
- 3,5-Dibromo-4-chloropyridine
- Packaging
- 250mg
- Price
- $10
- Updated
- 2021/12/16
3,5-DIBROMO-4-CHLOROPYRIDINE Chemical Properties,Usage,Production
Synthesis
28419-11-6
13626-17-0
General procedure for the synthesis of 3,5-dibromo-4-chloropyridine from 3,5-dibromopyridin-4(1H)-one: to 3,5-dibromopyridin-4(1H)-one (0.25 g, 1.0 mmol) was added phosphorous trichloride (POCl3, 2 mL), and the reaction mixture was heated and refluxed for 2 hours at 100 °C. Upon completion of the reaction, the mixture was slowly poured into an ice-water mixture (25 g) and the pH was adjusted to alkaline with saturated sodium bicarbonate solution. Subsequently, the aqueous phase was extracted with dichloromethane (CH2Cl2, 2 x 20 mL), the organic phases were combined and washed with brine (25 mL). The organic layer was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure to afford 3,5-dibromo-4-chloropyridine as a white solid (275 mg, 100% yield). The melting point of the product was 101-103 °C; mass spectrometry analysis showed m/z 272 (100%, [M+H]+).
References
[1] Patent: WO2010/41054, 2010, A1. Location in patent: Page/Page column 39
[2] Tetrahedron, 2010, vol. 66, # 13, p. 2398 - 2403
[3] Journal of Organic Chemistry, 2000, vol. 65, # 10, p. 3154 - 3159
[4] Patent: US2003/17942, 2003, A1
[5] Journal of the American Chemical Society, 2012, vol. 134, # 22, p. 9390 - 9399
3,5-DIBROMO-4-CHLOROPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-DIBROMO-4-CHLOROPYRIDINE manufacturers
- Product
- 3,5-DIBROMO-4-CHLOROPYRIDINE 13626-17-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-30
- Product
- 3,5-DIBROMO-4-CHLOROPYRIDINE 13626-17-0
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
- Product
- 3,5-DIBROMO-4-CHLOROPYRIDINE 13626-17-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-08-24