ChemicalBook > CAS DataBase List > 2-(3-BROMOPHENYL)PROPAN-2-OL
2-(3-BROMOPHENYL)PROPAN-2-OL
- Product Name
- 2-(3-BROMOPHENYL)PROPAN-2-OL
- CAS No.
- 30951-66-7
- Chemical Name
- 2-(3-BROMOPHENYL)PROPAN-2-OL
- Synonyms
- SKL668;2-(3-BROMOPHENYL)PROPAN-2-OL;2-(3-bromophenyl)-2-propanol;3-Bromophenyldimethylcarbinol;3-Bromo-α,α-dimethylbenzenemethanol;Benzenemethanol, 3-bromo-α,α-dimethyl-
- CBNumber
- CB02465317
- Molecular Formula
- C9H11BrO
- Formula Weight
- 215.09
- MOL File
- 30951-66-7.mol
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2-(3-BROMOPHENYL)PROPAN-2-OL Property
- Boiling point:
- 107-108℃ (3 Torr)
- Density
- 1.403±0.06 g/cm3 (20 ºC 760 Torr)
- refractive index
- 1.5602 (589.3 nm 20℃)
- Flash point:
- 109.8±20.4℃
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.41±0.29(Predicted)
- Appearance
- White to off-white Solid
- CAS DataBase Reference
- 30951-66-7
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- BML00258
- Product name
- 2-(3-Bromophenyl)propan-2-ol
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $99.7
- Updated
- 2023/01/07
TRC
- Product number
- B698525
- Product name
- 2-(3-Bromophenyl)propan-2-ol
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB153544
- Product name
- 2-(3-Bromophenyl)propan-2-ol
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB153544
- Product name
- 2-(3-Bromophenyl)propan-2-ol
- Packaging
- 2g
- Price
- $128
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 2603-9-07
- Product name
- 2-(3-Bromophenyl)propan-2-ol
- Packaging
- 1g
- Price
- $237
- Updated
- 2021/12/16
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2-(3-BROMOPHENYL)PROPAN-2-OL Chemical Properties,Usage,Production
Synthesis
618-89-3
75-16-1
30951-66-7
Step 1: Preparation of 2-(3-bromophenyl)-2-propanol (27) Methyl 3-bromobenzoate (4.3 g, 20 mmol) dissolved in 25 mL of anhydrous THF was added dropwise over 10 min to 75 mL of ether solution containing 75 mmol of methylmagnesium bromide under nitrogen protection. After the dropwise addition, the reaction mixture was slowly warmed to room temperature and stirred for 3.5 hours. Subsequently, the reaction system was cooled to 0°C and the reaction was quenched by slow addition of 10% aqueous HCl solution. The acidified mixture was extracted with ethyl acetate (2×) and the organic phases were combined and washed sequentially with 1N NaHCO3 solution and saturated saline. The organic layer was dried over anhydrous Na2SO4 and concentrated under reduced pressure, and the resulting crude product was purified by silica gel column chromatography using 15% ethyl acetate/heptane as eluent to afford 4.00 g (18.6 mmol, 93%) of 2-(3-bromophenyl)-2-propanol (27) as a pale yellow oil.
References
[1] Patent: WO2005/95326, 2005, A2. Location in patent: Page/Page column 189-190
[2] Journal of Organic Chemistry, 1960, vol. 25, # 10, p. 1691 - 1693
[3] Patent: WO2005/70932, 2005, A2. Location in patent: Page/Page column 51
[4] Patent: WO2015/89067, 2015, A1. Location in patent: Page/Page column 122
[5] Patent: US9126993, 2015, B2. Location in patent: Page/Page column 50
2-(3-BROMOPHENYL)PROPAN-2-OL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(3-BROMOPHENYL)PROPAN-2-OL manufacturers
Shaanxi Dideu Medichem Co. Ltd
- Product
- 2-(3-BROMOPHENYL)PROPAN-2-OL 30951-66-7
- Price
- US $1.00/Kg
- Min. Order
- 1Kg
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2024-07-22