CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER

Product Name: CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER
CAS No.: 161117-88-0
Chemical Name: CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER
Synonyms: tert-butyl 5-nitropyridin-2-ylcarbaMate;tert-butyl N-(5-nitro-2-pyridyl)carbamate;tert-butyl N-(5-nitropyridin-2-yl)carbamate;tert-butyl N-(5-nitro-2-pyridyl)carbamate - [B83341];N-(5-nitro-2-pyridinyl)carbamic acid tert-butyl ester;CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER;Carbamic acid, N-(5-nitro-2-pyridinyl)-, 1,1-dimethylethyl ester
CBNumber: CB02468075
Molecular Formula: C10H13N3O4
Formula Weight: 239.23
MOL File: 161117-88-0.mol

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CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Property

Boiling point:: 325.2±27.0 °C(Predicted)
Density: 1.303±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 11.35±0.70(Predicted)
Appearance: Light yellow to yellow Solid

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Safety

Hazard Codes: Xn
Risk Statements: 22-36-43
Safety Statements: 26-36/37

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B700748
Product name: tert-Butyl(5-Nitropyridin-2-yl)carbamate
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54521
Product name: tert-Butyl 5-nitropyridin-2-ylcarbamate
Packaging: 100mg
Price: $93
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54521
Product name: tert-Butyl 5-nitropyridin-2-ylcarbamate
Packaging: 250mg
Price: $112.5
Updated: 2021/12/16

AK Scientific

Product number: Y7705
Product name: tert-Butyl5-nitropyridin-2-ylcarbamate
Packaging: 100mg
Price: $140
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54521
Product name: tert-Butyl 5-nitropyridin-2-ylcarbamate
Packaging: 500mg
Price: $250
Updated: 2021/12/16

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CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Chemical Properties,Usage,Production

Synthesis

4214-76-0

24424-99-5

161117-88-0

5-Nitropyridin-2-amine (1 eq.), di-tert-butyl dicarbonate (1.2 eq.) and 4-dimethylaminopyridine (0.2 eq.) were added to a reaction vial under nitrogen protection. Dichloromethane was added as solvent at room temperature and the reaction mixture was stirred overnight. Upon completion of the reaction, ethyl acetate was added to the crude product, the precipitate was collected by filtration and washed with ethyl acetate to afford the target product (5-nitropyridin-2-yl)carbamic acid tert-butyl ester. It was analyzed by HPLC-MS (Method A): retention time (Rt) = 2.88 min, m/z of [M + H]+: 240. 80% yield.

References

[1] Patent: WO2016/120808, 2016, A1. Location in patent: Page/Page column 103; 104
[2] Patent: EP2314593, 2016, B1. Location in patent: Paragraph 0132
[3] Patent: WO2015/131080, 2015, A1. Location in patent: Paragraph 001167; 001168
[4] Patent: US2010/249099, 2010, A1. Location in patent: Page/Page column 96-97
[5] Patent: US2011/9405, 2011, A1. Location in patent: Page/Page column 54

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER manufacturers

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: tert-Butyl (5-nitropyridin-2-yl)carbamate 161117-88-0
Price: US $11.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50kg
Release date: 2021-09-24

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: tert-Butyl (5-nitropyridin-2-yl)carbamate 161117-88-0
Price: US $11.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2021-09-24

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: tert-Butyl (5-nitropyridin-2-yl)carbamate 161117-88-0
Price: US $11.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2021-11-26

161117-88-0, CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTERRelated Search:

tert-butyl 5-nitropyridin-2-ylcarbaMate

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER

N-(5-nitro-2-pyridinyl)carbamic acid tert-butyl ester

Carbamic acid, N-(5-nitro-2-pyridinyl)-, 1,1-dimethylethyl ester

tert-butyl N-(5-nitro-2-pyridyl)carbamate

tert-butyl N-(5-nitropyridin-2-yl)carbamate

tert-butyl N-(5-nitro-2-pyridyl)carbamate - [B83341]

161117-88-0