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5-METHOXYQUINOLIN-2(1H)-ONE

Product Name
5-METHOXYQUINOLIN-2(1H)-ONE
CAS No.
160893-04-9
Chemical Name
5-METHOXYQUINOLIN-2(1H)-ONE
Synonyms
5-methoxyquinolin-2-ol;5-METHOXYQUINOLIN-2(1H)-ONE;2(1H)-Quinolinone, 5-methoxy-;5-Methoxyquinolin-2(1H)-one 95+%
CBNumber
CB02468282
Molecular Formula
C10H9NO2
Formula Weight
175.18
MOL File
160893-04-9.mol
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5-METHOXYQUINOLIN-2(1H)-ONE Property

storage temp. 
Inert atmosphere,Room Temperature
Appearance
Off-white to light yellow Solid
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Safety

HS Code 
2933499090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
8128AA
Product name
5-Methoxyquinolin-2(1H)-one
Packaging
100mg
Price
$259
Updated
2021/12/16
SynQuest Laboratories
Product number
4H56-1-0R8
Product name
5-Methoxyquinolin-2(1H)-one
Packaging
250mg
Price
$375
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0390866
Product name
5-METHOXYQUINOLIN-2(1H)-ONE
Purity
95.00%
Packaging
5MG
Price
$496.58
Updated
2021/12/16
SynQuest Laboratories
Product number
4H56-1-0R8
Product name
5-Methoxyquinolin-2(1H)-one
Packaging
1g
Price
$936
Updated
2021/12/16
AK Scientific
Product number
8128AA
Product name
5-Methoxyquinolin-2(1H)-one
Packaging
5g
Price
$2413
Updated
2021/12/16
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5-METHOXYQUINOLIN-2(1H)-ONE Chemical Properties,Usage,Production

Synthesis

90924-16-6

160893-04-9

4.4 At room temperature, 5-methoxyquinoline azide (Compound 2, 4.09 g, 23.3 mmol) was dissolved in a solvent mixture of 10% aqueous K2CO3 (60 mL) and dichloromethane (60 mL). Subsequently, p-toluenesulfonyl chloride (5.55 g, 29.1 mmol) was added in batches and the reaction mixture was stirred at the same temperature for 18 hours. Upon completion of the reaction, ether was added to precipitate the product, and the precipitate was collected by filtration and washed with ether. The resulting solid was dried in an oven at 65 °C for 2 h to give 5-methoxyquinolin-2(1H)-one as a pale yellow solid, yield: 2.651 g (65%). The product was characterized by 1H NMR (400 MHz, CDCl3) and 13C NMR (100 MHz, CDCl3) with the following data: 1H NMR δ 12.15 (br.s, 1H), 8.25 (d, J = 9.6 Hz, 1H), 7.45 (t, J = 8.4 Hz, 1H), 7.04 (d, J = 8.4 Hz, 1H) 6.67 (t, J = 9.2 Hz, 2H), 3.97 (s, 3H); 13C NMR δ 164.61, 156.09, 139.72, 135.74, 131.40, 119.67, 110.91, 108.66, 102.78, 55.73.

References

[1] European Journal of Medicinal Chemistry, 2015, vol. 101, p. 754 - 768
[2] Patent: KR101778938, 2017, B1. Location in patent: Paragraph 0147-0148; 0155; 0175-0177

5-METHOXYQUINOLIN-2(1H)-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-METHOXYQUINOLIN-2(1H)-ONE Suppliers

China 26 India 1 United Kingdom 1 United States 4 Global 32
Synthonix Inc
Tel
--
Fax
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Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
SynQuest Laboratories, Inc.
Tel
--
Fax
--
Email
info@synquestlabs.com
Country
United States
ProdList
6871
Advantage
62
AstaTech, Inc
Tel
--
Fax
--
Email
sales@astatechinc.com
Country
United States
ProdList
6371
Advantage
58

160893-04-9, 5-METHOXYQUINOLIN-2(1H)-ONERelated Search:


  • 5-METHOXYQUINOLIN-2(1H)-ONE
  • 5-Methoxyquinolin-2(1H)-one 95+%
  • 2(1H)-Quinolinone, 5-methoxy-
  • 5-methoxyquinolin-2-ol
  • 160893-04-9