(4-Bromo-2-(trifluoromethoxy)phenyl)methanol

Product Name: (4-Bromo-2-(trifluoromethoxy)phenyl)methanol
CAS No.: 220996-81-6
Chemical Name: (4-Bromo-2-(trifluoromethoxy)phenyl)methanol
Synonyms: (4-Bromo-2-(trifluoromethoxy);4-Bromo-2-trifluoromethoxybenzylalcohol;2-trifluoroMethoxyl-4-broMobenzyl alcohol;(4-Bromo-2-(trifluoromethoxy)phenyl)methanol;Benzenemethanol, 4-bromo-2-(trifluoromethoxy)-;(4-Bromo-2-(trifluoromethoxy)phenyl)methanol b
CBNumber: CB02470007
Molecular Formula: C8H6BrF3O2
Formula Weight: 271.03
MOL File: 220996-81-6.mol

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(4-Bromo-2-(trifluoromethoxy)phenyl)methanol Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Safety

HS Code: 2909498090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B700003
Product name: (4-Bromo-2-(trifluoromethoxy)phenyl)methanol
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: X8215
Product name: 4-Bromo-2-(trifluoromethoxy)benzylalcohol
Packaging: 250mg
Price: $35
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2707-B-46
Product name: [4-Bromo-2-(trifluoromethoxy)phenyl]methanol
Purity: 96%
Packaging: 250mg
Price: $139
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2707-B-46
Product name: [4-Bromo-2-(trifluoromethoxy)phenyl]methanol
Purity: 96%
Packaging: 1g
Price: $199
Updated: 2021/12/16

Matrix Scientific

Product number: 073431
Product name: (4-Bromo-2-(trifluoromethoxy)phenyl)methanol
Purity: 95+%
Packaging: 1g
Price: $278
Updated: 2021/12/16

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(4-Bromo-2-(trifluoromethoxy)phenyl)methanol Chemical Properties,Usage,Production

Synthesis

220996-80-5

220996-81-6

[Step 2] Synthesis of (4-bromo-2-(trifluoromethoxy)phenyl)methanol: To a solution of 4-bromo-2-(trifluoromethoxy)benzaldehyde (16 g, 59 mmol) in methanol (0.23 L) was added sodium borohydride (2.4 g, 63 mmol) in batches at -10 °C. The reaction solution was stirred at -10 °C for 10 min before acetone (10 mL) and 1N hydrochloric acid (10 mL) were added sequentially to quench the reaction. The reaction mixture was concentrated under reduced pressure and water was added to the residue and extracted with ethyl acetate. The organic layers were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (elution gradient: hexane/ethyl acetate = 50:1 → 1:1) to afford 15 g (91% yield) of the title compound (4-bromo-2-(trifluoromethoxy)phenyl)methanol (hereinafter referred to as Reference Example Compound 2).

References

[1] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 9, p. 1311 - 1316
[2] Patent: EP2832724, 2015, A1. Location in patent: Paragraph 0124
[3] Patent: US5968938, 1999, A
[4] Patent: US6090805, 2000, A
[5] Patent: WO2010/96722, 2010, A1. Location in patent: Page/Page column 60-62

(4-Bromo-2-(trifluoromethoxy)phenyl)methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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(4-Bromo-2-(trifluoromethoxy)phenyl)methanol Suppliers

Canada 1 China 60 Germany 1 India 1 United Kingdom 2 United States 7 Global 72

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View Lastest Price from (4-Bromo-2-(trifluoromethoxy)phenyl)methanol manufacturers

Career Henan Chemical Co

Product: (4-Bromo-2-(trifluoromethoxy)phenyl)methanol 220996-81-6
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-09

220996-81-6, (4-Bromo-2-(trifluoromethoxy)phenyl)methanolRelated Search:

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4-Bromo-2-trifluoromethoxybenzylalcohol

2-trifluoroMethoxyl-4-broMobenzyl alcohol

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Benzenemethanol, 4-bromo-2-(trifluoromethoxy)-

(4-Bromo-2-(trifluoromethoxy)phenyl)methanol b

220996-81-6

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