2-(3-bromophenyl)Naphthalene
- Product Name
- 2-(3-bromophenyl)Naphthalene
- CAS No.
- 667940-23-0
- Chemical Name
- 2-(3-bromophenyl)Naphthalene
- Synonyms
- 2-(3-broMophenyl)naphthale;2-(3-bromophenyl)phthalene;2-(3-bromophenyl)Naphthalene;Naphthalene, 2-(3-bromophenyl)-;2-(3-Bromophenyl)naphthalene,98%;2-(3-Bromophenyl)naphthalene >
- CBNumber
- CB02489593
- Molecular Formula
- C16H11Br
- Formula Weight
- 283.16
- MOL File
- 667940-23-0.mol
2-(3-bromophenyl)Naphthalene Property
- Melting point:
- 97.0 to 101.0 °C
- Boiling point:
- 385.2±11.0 °C(Predicted)
- Density
- 1.381±0.06 g/cm3 (20 ºC 760 Torr)
- storage temp.
- Sealed in dry,Room Temperature
- form
- Solid
- color
- White to Yellow to Orange
- InChI
- InChI=1S/C16H11Br/c17-16-7-3-6-14(11-16)15-9-8-12-4-1-2-5-13(12)10-15/h1-11H
- InChIKey
- FWPXWVYUNHYGPE-UHFFFAOYSA-N
- SMILES
- C1=C2C(C=CC=C2)=CC=C1C1=CC=CC(Br)=C1
- CAS DataBase Reference
- 667940-23-0
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B4568
- Product name
- 2-(3-Bromophenyl)naphthalene
- Purity
- >95.0%(GC)
- Packaging
- 1g
- Price
- $33
- Updated
- 2025/07/31
- Product number
- B4568
- Product name
- 2-(3-Bromophenyl)naphthalene
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $165
- Updated
- 2025/07/31
- Product number
- B678240
- Product name
- 2-(3-Bromophenyl)naphthalene
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B678240
- Product name
- 2-(3-Bromophenyl)naphthalene
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- B678240
- Product name
- 2-(3-Bromophenyl)naphthalene
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
2-(3-bromophenyl)Naphthalene Chemical Properties,Usage,Production
Chemical Properties
Type of white solid
Synthesis
591-18-4
32316-92-0
667940-23-0
1. Preparation of Compound 2a: 1-Bromo-3-iodobenzene (10 g, 35.35 mmol) and 2-naphthaleneboronic acid (5.47 g, 31.82 mmol) were dissolved in anhydrous tetrahydrofuran (THF, 100 mL) under dry conditions. Subsequently, tetrakis(triphenylphosphine)palladium (Pd(PPh3)4, 1.2 g, 1.06 mmol) and 2M aqueous potassium carbonate (K2CO3) (50 mL) were added. The reaction mixture was heated to reflux for 24 hours. After completion of the reaction, the organic layer was extracted with ethyl acetate and dried with anhydrous magnesium sulfate (MgSO4). After filtration to remove the desiccant, the organic layer was concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography followed by recrystallization in a solvent mixture of tetrahydrofuran (THF) and ethanol (EtOH) to afford the white solid compound 2a (8.5 g, 85% yield). Mass spectrometry analysis showed [M + H]+ peak located at 283 m/z.
References
[1] Patent: WO2008/13399, 2008, A1. Location in patent: Page/Page column 14-15
[2] Patent: US2010/331585, 2010, A1. Location in patent: Page/Page column 94-95
[3] Organic and Biomolecular Chemistry, 2017, vol. 15, # 19, p. 4096 - 4114
2-(3-bromophenyl)Naphthalene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(3-bromophenyl)Naphthalene manufacturers
- Product
- 2-(3-bromophenyl)Naphthalene 667940-23-0
- Price
- US $101.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-28
- Product
- 2-(3-bromophenyl)Naphthalene 667940-23-0
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-09-14
- Product
- 2-(3-Bromophenyl)naphthalene 667940-23-0
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1Kg
- Purity
- 99.9%
- Supply Ability
- 30000 Kg
- Release date
- 2023-10-31