ChemicalBook > CAS DataBase List > Methyl 2-(Boc-amino)isonicotinate

Methyl 2-(Boc-amino)isonicotinate

Product Name
Methyl 2-(Boc-amino)isonicotinate
CAS No.
639091-75-1
Chemical Name
Methyl 2-(Boc-amino)isonicotinate
Synonyms
Methyl 2-(Boc-amino)isonicotinate;2-Boc-amino-isonicotinic acid methyl ester;Methyl 2-((tert-butoxycarbonyl)aMino)isonicotinate;2-tert-Butoxycarbonylamino-isonicotinic acid methyl ester;methyl 2-(tert-butoxycarbonylamino)pyridine-4-carboxylate;Methyl 2-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-4-carboxylate;2-[[(1,1-Dimethylethoxy)carbonyl]amino]-4-pyridinecarboxylic acidmethylester;4-Pyridinecarboxylic acid, 2-[[(1,1-diMethylethoxy)carbonyl]aMino]-, Methyl ester
CBNumber
CB02499400
Molecular Formula
C12H16N2O4
Formula Weight
252.27
MOL File
639091-75-1.mol
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Methyl 2-(Boc-amino)isonicotinate Property

Melting point:
75.1～75.2℃
Boiling point:
325.5±27.0 °C(Predicted)
Density 
1.203±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
12.12±0.70(Predicted)
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Safety

HS Code 
2922390090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

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N-Bromosuccinimide Price

TRC
Product number
M295635
Product name
Methyl2-(Boc-amino)isonicotinate
Packaging
250mg
Price
$55
Updated
2021/12/16
Matrix Scientific
Product number
018214
Product name
2-(2,2-Dimethyl-propionylamino)-isonicotinic acidmethyl ester
Packaging
500mg
Price
$116
Updated
2021/12/16
Matrix Scientific
Product number
118101
Product name
Methyl 2-((tert-butoxycarbonyl)amino)isonicotinate
Packaging
5g
Price
$301
Updated
2021/12/16
SynQuest Laboratories
Product number
4H58-1-8C
Product name
Methyl 2-((tert-butoxycarbonyl)amino)isonicotinate
Packaging
5G
Price
$356
Updated
2021/12/16
AK Scientific
Product number
Y6341
Product name
Methyl2-(tert-butoxycarbonylamino)isonicotinate
Packaging
10g
Price
$370
Updated
2021/12/16
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Methyl 2-(Boc-amino)isonicotinate Chemical Properties,Usage,Production

Synthesis

A 500 mL round bottomed flask was charged with methyl 2-aminoisonicotinate (5.0 g, 32.9 mmol) and suspended in t-BuOH (200 mL). To this stirring solution was added di-tert-butyl dicarbonate (7.53 g, 34.5 mmol). The flask was vented and placed in an oil bath preheated to 50°C. The reaction mixture was let stir overnight. After 22 hours LCMS showed near complete conversion of starting material. The mixture was cooled to room temperature and filtered. The material was taken on without any further purification. Yield 5.93 g of white solid, Methyl 2-(Boc-amino)isonicotinate.  1H NMR (400 MHz, DMSO-d6) δ ppm 10.14 (1H, s), 8.43 (1H, dd, J=5.02, 0.75 Hz), 8.33 (1H, s), 7.45 (1H, dd, J=5.02, 1.51 Hz), 3.89 (3H, s), 1.48 (9H, s).

Methyl 2-(Boc-amino)isonicotinate Preparation Products And Raw materials

Raw materials

Preparation Products

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639091-75-1, Methyl 2-(Boc-amino)isonicotinateRelated Search:


  • 2-[[(1,1-Dimethylethoxy)carbonyl]amino]-4-pyridinecarboxylic acidmethylester
  • Methyl 2-(Boc-amino)isonicotinate
  • 2-tert-Butoxycarbonylamino-isonicotinic acid methyl ester
  • 4-Pyridinecarboxylic acid, 2-[[(1,1-diMethylethoxy)carbonyl]aMino]-, Methyl ester
  • Methyl 2-((tert-butoxycarbonyl)aMino)isonicotinate
  • 2-Boc-amino-isonicotinic acid methyl ester
  • Methyl 2-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-4-carboxylate
  • methyl 2-(tert-butoxycarbonylamino)pyridine-4-carboxylate
  • 639091-75-1