5-Amino-2-phenylindole

Product Name: 5-Amino-2-phenylindole
CAS No.: 6855-64-7
Chemical Name: 5-Amino-2-phenylindole
Synonyms: 5-Amino-2-phenylindole;2-phenyl-1H-indol-5-aMine;1H-Indol-5-amine, 2-phenyl-
CBNumber: CB02507594
Molecular Formula: C14H12N2
Formula Weight: 208.26
MOL File: 6855-64-7.mol

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5-Amino-2-phenylindole Property

Melting point:: 231.5-233 °C(Solv: benzene (71-43-2))
Boiling point:: 469.3±25.0 °C(Predicted)
Density: 1.229±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 17.19±0.30(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0388559
Product name: 2-PHENYL-1H-INDOL-5-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $495.04
Updated: 2021/12/16

AK Scientific

Product number: 0590AC
Product name: 2-Phenyl-1H-indol-5-amine
Packaging: 5g
Price: $1152
Updated: 2021/12/16

Chemenu

Product number: CM132610
Product name: 2-phenyl-1H-indol-5-amine
Purity: 95+%
Packaging: 10g
Price: $1388
Updated: 2021/12/16

Crysdot

Product number: CD11072517
Product name: 2-Phenyl-1H-indol-5-amine
Purity: 97%
Packaging: 10g
Price: $1471
Updated: 2021/12/16

AccelPharmtech

Product number: H3766
Product name: 2-phenyl-1H-Indol-5-amine
Purity: 97.00%
Packaging: 1G
Price: $2460
Updated: 2021/12/16

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5-Amino-2-phenylindole Chemical Properties,Usage,Production

Synthesis

4993-87-7

6855-64-7

Under nitrogen protection, 5-nitro-2-phenyl-1H-indole (2.83 g, 10 mmol) was dissolved in methanol (30 mL) and Raney Ni catalyst (510 mg) was added. The reaction mixture was placed under hydrogen atmosphere (1 atm) and the reaction was stirred at room temperature overnight. Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth pad and the filtrate was concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate=5:1) to afford 2-phenyl-1H-indol-5-amine (1.6 g, 77% yield). The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3) and mass spectrometry (ESI): 1H NMR δ 7.76 (d, J=7.6 Hz, 2H), 7.39 (t, J=7.6 Hz, 2H), 7.24 (t, J=7.6 Hz, 1H), 7.07 (d, J=8.4 Hz, 1H), 6.64 (d, J=1.6 Hz, 1H), 6.60 (d, J=1.2 Hz, 1H), 6.48 (dd, J=2.0,8.4 Hz, 1H), 4.48 (brs, 2H); MS (ESI) m/e 209.0 ([M+H]+).

References

[1] Tetrahedron Letters, 2002, vol. 43, # 43, p. 7699 - 7702
[2] Journal of Medicinal Chemistry, 2010, vol. 53, # 10, p. 4085 - 4093
[3] Patent: US2007/244159, 2007, A1. Location in patent: Page/Page column 120
[4] Patent: US2011/98311, 2011, A1
[5] Patent: US2015/231142, 2015, A1. Location in patent: Paragraph 1672

5-Amino-2-phenylindole Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Amino-2-phenylindole Suppliers

China 33 Germany 1 India 1 United States 3 Global 38

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6855-64-7, 5-Amino-2-phenylindoleRelated Search:

5-Amino-2-phenylindole

2-phenyl-1H-indol-5-aMine

1H-Indol-5-amine, 2-phenyl-

6855-64-7