5-bromo-3-tert-butyl-2-hydroxybenzaldehyde

Product Name: 5-bromo-3-tert-butyl-2-hydroxybenzaldehyde
CAS No.: 153759-58-1
Chemical Name: 5-bromo-3-tert-butyl-2-hydroxybenzaldehyde
Synonyms: 3-tert-butyl-5-bromo-2-hydroxybenzaldehyde;5-bromo-3-tert-butyl-2-hydroxybenzaldehyde;Benzaldehyde, 5-bromo-3-(1,1-dimethylethyl)-2-hydroxy-
CBNumber: CB02513948
Molecular Formula: C11H13BrO2
Formula Weight: 257.12
MOL File: 153759-58-1.mol

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5-bromo-3-tert-butyl-2-hydroxybenzaldehyde Property

Melting point:: 58-60 °C
Boiling point:: 266.5±35.0 °C(Predicted)
Density: 1.409±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 8.99±0.23(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B678808
Product name: 5-Bromo-3-(tert-butyl)-2-hydroxybenzaldehyde
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B678808
Product name: 5-Bromo-3-(tert-butyl)-2-hydroxybenzaldehyde
Packaging: 100mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0135032
Product name: 5-BROMO-3-TERT-BUTYL-2-HYDROXYBENZALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $502.01
Updated: 2021/12/16

AK Scientific

Product number: 7062CD
Product name: 5-Bromo-3-(tert-butyl)-2-hydroxybenzaldehyde
Packaging: 25g
Price: $1846
Updated: 2021/12/16

Ambeed

Product number: A424828
Product name: 5-Bromo-3-(tert-butyl)-2-hydroxybenzaldehyde
Purity: 95%
Packaging: 100mg
Price: $17
Updated: 2021/12/16

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5-bromo-3-tert-butyl-2-hydroxybenzaldehyde Chemical Properties,Usage,Production

Uses

5-Bromo-3-(tert-butyl)-2-hydroxybenzaldehyde can be used as a highly sensitive dual-channel chemical sensor for selective identification of B4O2-7.

Synthesis

24623-65-2

153759-58-1

Step 2: Synthesis of 5-bromo-3-tert-butyl-2-hydroxybenzaldehyde (7b) Bromine (2.95 g, 18 mmol) was slowly added to a solution of 3-tert-butyl-2-hydroxybenzaldehyde (7a, 3.0 g, 17 mmol) in acetic acid (15 mL). The reaction was carried out at room temperature and stirring was continued for 3 h after the drop was completed. The progress of the reaction was monitored by thin layer chromatography (TLC, unfolding agent ratio petroleum ether: ethyl acetate = 50:1) to confirm the completion of the reaction. The reaction mixture was quenched with water, washed with sodium bisulfite solution (50 mL) and extracted with ether. The organic layers were combined and concentrated under reduced pressure to give the crude product 5-bromo-3-tert-butyl-2-hydroxybenzaldehyde (7b, 3.2 g, 73% yield) as a white solid.

References

[1] Journal of Medicinal Chemistry, 2013, vol. 56, # 20, p. 8163 - 8182
[2] Advanced Synthesis and Catalysis, 2009, vol. 351, # 9, p. 1325 - 1332
[3] Inorganic Chemistry, 2017, vol. 56, # 20, p. 12357 - 12361
[4] Chemistry - A European Journal, 2006, vol. 12, # 2, p. 576 - 583
[5] European Journal of Organic Chemistry, 2001, # 24, p. 4639 - 4649

5-bromo-3-tert-butyl-2-hydroxybenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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5-bromo-3-tert-butyl-2-hydroxybenzaldehyde Suppliers

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153759-58-1, 5-bromo-3-tert-butyl-2-hydroxybenzaldehydeRelated Search:

5-bromo-3-tert-butyl-2-hydroxybenzaldehyde

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153759-58-1