1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one

Uses

Product Name: 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
CAS No.: 649736-31-2
Chemical Name: 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
Synonyms: CEDI-005;FMX15115-A4;1-(2-Fluoro-3-hydroxy-6-nitrophenyl);2-Fluoro-3-hydroxy-6-nitrophenylacetone;1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one;2-Propanone, 1-(2-fluoro-3-hydroxy-6-nitrophenyl)-
CBNumber: CB02514086
Molecular Formula: C9H8FNO4
Formula Weight: 213.16
MOL File: 649736-31-2.mol

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1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one Property

Boiling point:: 353.0±42.0 °C(Predicted)
Density: 1.417±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 5.58±0.24(Predicted)
form: Solid
InChI: InChI=1S/C9H8FNO4/c1-5(12)4-6-7(11(14)15)2-3-8(13)9(6)10/h2-3,13H,4H2,1H3
InChIKey: IPRZVDNMKMONNN-UHFFFAOYSA-N
SMILES: C(C1=C([N+]([O-])=O)C=CC(O)=C1F)C(=O)C
CAS DataBase Reference: 649736-31-2

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Safety

HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: F600868
Product name: 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
Packaging: 50mg
Price: $175
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0037302
Product name: 1-(2-FLUORO-3-HYDROXY-6-NITROPHENYL)PROPAN-2-ONE
Purity: 95.00%
Packaging: 1G
Price: $1033.73
Updated: 2021/12/16

Matrix Scientific

Product number: 143736
Product name: 1-(2-Fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
Purity: 95%
Packaging: 1g
Price: $1458
Updated: 2021/12/16

Matrix Scientific

Product number: 143736
Product name: 1-(2-Fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
Purity: 95%
Packaging: 5g
Price: $2916
Updated: 2021/12/16

Chemenu

Product number: CM254328
Product name: 1-(2-Fluoro-3-hydroxy-6-nitrophenyl)propan-2-one
Purity: 95+%
Packaging: 1g
Price: $196
Updated: 2021/12/16

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1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one Chemical Properties,Usage,Production

Uses

1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one (cas# 649736-31-2) is a useful research chemical.

Synthesis

121247-16-3

649736-31-2

Step 3b: A mixture of 1-(2,3-difluoro-6-nitrophenyl)propan-2-one (Compound 302, 4.30 g, 0.02 mol), sodium acetate (AcONa, 1.72 g, 0.021 mol) and N,N-dimethylformamide (DMF, 40 mL) was stirred and reacted for 12 hours at 100 °C. After completion of the reaction, the mixture was filtered and the solvent was removed by distillation under reduced pressure. The residue was extracted with ethyl acetate (100 mL) and the organic layer was washed sequentially with water and saturated saline, dried over anhydrous magnesium sulfate (MgSO?) and concentrated. The crude product was purified by silica gel column chromatography (eluent: ethyl acetate/petroleum ether = 1/1) to afford 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one (Compound 303, 2.3 g, 54%) as a light yellow solid.LCMS: 214 [M + 1]? ; 1H NMR (DMSO-d6): δ 2.30 (s, 3H), 4.26 (s, 2H), 7.67 (m, 1H), 8.05 (m, 1H).

References

[1] Patent: US2009/76044, 2009, A1. Location in patent: Page/Page column 27-28
[2] Organic Process Research and Development, 2014, vol. 18, # 1, p. 89 - 102

1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one 649736-31-2
Price: US $0.10/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000 tons
Release date: 2020-04-27

Shanghai VastPro Technology Development Co., Ltd.

Product: 1-(2-Fluoro-3-hydroxy-6-nitrophenyl)propan-2-one 649736-31-2
Price: US $0.00/KG
Min. Order: 1g
Purity: 99
Supply Ability: 100kg
Release date: 2020-08-10

Shaanxi Dideu Medichem Co. Ltd

Product: 1-(2-Fluoro-3-hydroxy-6-nitrophenyl)propan-2-one 649736-31-2
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99.0%+
Supply Ability: 100 tons
Release date: 2019-12-30

649736-31-2, 1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-oneRelated Search:

p-Cresol

1-(2-fluoro-3-hydroxy-6-nitrophenyl)propan-2-one

2-Fluoro-3-hydroxy-6-nitrophenylacetone

CEDI-005

2-Propanone, 1-(2-fluoro-3-hydroxy-6-nitrophenyl)-

FMX15115-A4

1-(2-Fluoro-3-hydroxy-6-nitrophenyl)

649736-31-2