2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE

Product Name: 2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE
CAS No.: 63155-43-1
Chemical Name: 2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE
Synonyms: NSC 17578;2-(4,6-Dichloropyrimidin-2-yl);4,6-Dichloropyrimidine-2-acetonitrile;4,6-Dichloro-2-pyrimidineacetonitrile;2-PyriMidineacetonitrile, 4,6-dichloro-;(4,6-Dichloro-2-pyrimidinyl)acetonitrile;(4,6-Dichloro-pyrimidin-2-yl)-acetonitrile;2-(4,6-Dichloro-2-pyrimidinyl)acetonitrile;2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE
CBNumber: CB02534507
Molecular Formula: C6H3Cl2N3
Formula Weight: 188.01
MOL File: 63155-43-1.mol

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2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: W7518
Product name: 2-(4,6-Dichloropyrimidin-2-yl)acetonitrile
Packaging: 100mg
Price: $184
Updated: 2021/12/16

AK Scientific

Product number: W7518
Product name: 2-(4,6-Dichloropyrimidin-2-yl)acetonitrile
Packaging: 250mg
Price: $253
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0362615
Product name: 2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE
Purity: 95.00%
Packaging: 5MG
Price: $497.28
Updated: 2021/12/16

Matrix Scientific

Product number: 144199
Product name: 2-(4,6-Dichloropyrimidin-2-yl)acetonitrile
Purity: 95%
Packaging: 5g
Price: $1014
Updated: 2021/12/16

Matrix Scientific

Product number: 144199
Product name: 2-(4,6-Dichloropyrimidin-2-yl)acetonitrile
Purity: 95%
Packaging: 25g
Price: $2850
Updated: 2021/12/16

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2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE Chemical Properties,Usage,Production

Synthesis

28215-45-4

63155-43-1

(B) 2-(4,6-dihydroxypyrimidin-2-yl)acetamide (6.28 g, 37.1 mmol) was used as a raw material, which was dissolved in phosphorus trichloride (19 ml, 204 mmol) in a flask equipped with a reflux condenser. N,N-dimethylaniline (10 ml, 79 mmol) was slowly added through the condenser. The reaction mixture was gently heated in an oil bath and quickly removed from the heat source once the reaction was initiated. After the initial vigorous reaction had subsided, the reaction was continued at reflux for 10 min. The hot reaction solution was carefully decanted onto 100 g of ice and the resulting suspension was extracted with dichloromethane (3 x CH2Cl2). The organic layers were combined, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure. Purification by silica gel column chromatography (SiO2, 15-20% ethyl acetate/hexane) afforded 2-(4,6-dichloropyrimidin-2-yl)acetonitrile (5.10 g, 27.1 mmol, 73%) as a yellow solid.

References

[1] Patent: US2007/299080, 2007, A1. Location in patent: Page/Page column 80-81
[2] Patent: US2010/81673, 2010, A1. Location in patent: Page/Page column 20
[3] Patent: WO2016/206573, 2016, A1. Location in patent: Paragraph 081; 084; 085

2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE Suppliers

China 37 India 1 United Kingdom 1 United States 5 Global 44

Chengdu Forest Science and Technology Development Co., Ltd.

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View Lastest Price from 2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-(4,6-dichloropyriMidin-2-yl)acetonitrile 63155-43-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2020-05-15

Career Henan Chemical Co

Product: (4,6-Dichloro-2-pyrimidinyl)acetonitrile 63155-43-1
Price: US $1.00/g
Min. Order: 1g
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-09

63155-43-1, 2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILERelated Search:

2-(4,6-DICHLOROPYRIMIDIN-2-YL)ACETONITRILE

2-PyriMidineacetonitrile, 4,6-dichloro-

2-(4,6-Dichloro-2-pyrimidinyl)acetonitrile

4,6-Dichloro-2-pyrimidineacetonitrile

(4,6-Dichloro-pyrimidin-2-yl)-acetonitrile

NSC 17578

2-(4,6-Dichloropyrimidin-2-yl)

(4,6-Dichloro-2-pyrimidinyl)acetonitrile

4,6-Dichloropyrimidine-2-acetonitrile

63155-43-1