4-BroMo-1-iodo-2-isopropylbenzene

Product Name: 4-BroMo-1-iodo-2-isopropylbenzene
CAS No.: 1147014-97-8
Chemical Name: 4-BroMo-1-iodo-2-isopropylbenzene
Synonyms: 5-BroMo-2-iodoisopropyl benzene;4-BroMo-1-iodo-2-isopropylbenzene;4-bromo-1-iodo-2-propan-2-ylbenzene;Benzene, 4-bromo-1-iodo-2-(1-methylethyl)-
CBNumber: CB02546049
Molecular Formula: C9H10BrI
Formula Weight: 324.98
MOL File: 1147014-97-8.mol

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4-BroMo-1-iodo-2-isopropylbenzene Property

Boiling point:: 284.8±28.0 °C(Predicted)
Density: 1.828±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
Appearance: Yellow to orange Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B802650
Product name: 5-Bromo-2-iodoisopropylbenzene
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B802650
Product name: 5-Bromo-2-iodoisopropylbenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: Y3717
Product name: 5-Bromo-2-iodoisopropylbenzene
Packaging: 1g
Price: $137
Updated: 2021/12/16

AK Scientific

Product number: Y3717
Product name: 5-Bromo-2-iodoisopropylbenzene
Packaging: 5g
Price: $313
Updated: 2021/12/16

AK Scientific

Product number: Y3717
Product name: 5-Bromo-2-iodoisopropylbenzene
Packaging: 25g
Price: $1049
Updated: 2021/12/16

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4-BroMo-1-iodo-2-isopropylbenzene Chemical Properties,Usage,Production

Synthesis

19099-54-8

1147014-97-8

General procedure for the synthesis of 5-bromo-2-iodoisopropylbenzene from 2-isopropyliodobenzene: 1-iodo-2-isopropylbenzene (1.5 g, 6.1 mmol) was mixed with silver sulfate (1.0 g, 3.1 mmol), concentrated sulfuric acid (5.5 mL), water (0.6 mL) and bromine (0.3 mL, 6.4 mmol) to form a three-phase suspension. The reaction mixture was stirred at room temperature for 1 hour. Upon completion of the reaction, the mixture was poured into a mixture of ether (150 mL) and water (75 mL). The solids were removed by filtration and the organic and aqueous layers were separated. The organic layer was concentrated under vacuum and the residue was purified by preparative high performance liquid chromatography (HPLC) to afford the target product 5-bromo-2-iodoisopropylbenzene as a white solid (189 mg, 10% yield). [0257] 1H NMR (500 MHz, DMSO-d6) δ 1.18 (d, J = 6.8 Hz, 6H), 3.07 (qn, J = 6.8 Hz, 1H), 7.15 (dd, J = 8.4,2.5 Hz, 1H), 7.46 (d, J = 2.4 Hz, 1H), 7.75 (d, J = 8.4 Hz, 1H). 2D NOE (500 MHz, DMSO-d6): cross peak between δ 1.18 and 7.46.

References

[1] Patent: WO2009/55674, 2009, A1. Location in patent: Page/Page column 72-73

4-BroMo-1-iodo-2-isopropylbenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1147014-97-8, 4-BroMo-1-iodo-2-isopropylbenzeneRelated Search:

Tiotropium bromide

5-BroMo-2-iodoisopropyl benzene

4-bromo-1-iodo-2-propan-2-ylbenzene

4-BroMo-1-iodo-2-isopropylbenzene

Benzene, 4-bromo-1-iodo-2-(1-methylethyl)-

1147014-97-8