4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester

Product Name: 4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester
CAS No.: 2164-66-1
Chemical Name: 4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester
Synonyms: Methyl 2-aMinopyriMidine-4-carboxylate;2-amino-4-Pyrimidinecarboxylicacid methylester;4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester;2-amino-4-Pyrimidinecarboxylic acid methyl ester (7CI 9CI ACI);4-Pyrimidinecarboxylic acid, 2-amino-, methyl ester (7CI, 9CI, ACI)
CBNumber: CB02548452
Molecular Formula: C6H7N3O2
Formula Weight: 153.14
MOL File: 2164-66-1.mol

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4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester Property

Melting point:: 230 °C
Boiling point:: 344.2±34.0 °C(Predicted)
Density: 1.319±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.10±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: M878098
Product name: Methyl2-aminopyrimidine-4-carboxylate
Packaging: 50mg
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: 1008AB
Product name: Methyl2-aminopyrimidine-4-carboxylate
Packaging: 250mg
Price: $296
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0392928
Product name: METHYL-2-AMINOPYRIMIDINE-4-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $501.18
Updated: 2021/12/16

AK Scientific

Product number: 1008AB
Product name: Methyl2-aminopyrimidine-4-carboxylate
Packaging: 5g
Price: $2201
Updated: 2021/12/16

Chemenu

Product number: CM165140
Product name: methyl2-aminopyrimidine-4-carboxylate
Purity: 95%
Packaging: 1g
Price: $430
Updated: 2021/12/16

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4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester Chemical Properties,Usage,Production

Synthesis

502164-18-3

50-01-1

2164-66-1

Methyl 4-butoxy-2-oxo-3-butenoate (37 g, 200 mmol) and guanidine hydrochloride (23 g, 240 mmol) were suspended in propionitrile (50 mL) and triethylamine (29 mL, 210 mmol) was added. The reaction mixture was stirred at 100 °C for 4 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure and the residue was purified by silica gel column chromatography to afford 18 g of methyl 2-aminopyrimidine-4-carboxylate and its mixture in the form of butyl ester as an off-white solid (yield: 60%). The product was characterized by 1H-NMR (500 MHz, DMSO-d6): δ 3.85 (s, 3H), 6.99-7.06 (m, 3H), 8.48 (d, J = 4.8 Hz, 1H).

References

[1] Patent: EP1864977, 2007, A1. Location in patent: Page/Page column 16

4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester Suppliers

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2164-66-1, 4-PyriMidinecarboxylic acid, 2-aMino-, Methyl esterRelated Search:

4-PyriMidinecarboxylic acid, 2-aMino-, Methyl ester

Methyl 2-aMinopyriMidine-4-carboxylate

2-amino-4-Pyrimidinecarboxylicacid methylester

4-Pyrimidinecarboxylic acid, 2-amino-, methyl ester (7CI, 9CI, ACI)

2-amino-4-Pyrimidinecarboxylic acid methyl ester (7CI 9CI ACI)

2164-66-1