ChemicalBook > CAS DataBase List > 1-(4-Bromophenyl)-2-methylpropan-1-one

1-(4-Bromophenyl)-2-methylpropan-1-one

Product Name: 1-(4-Bromophenyl)-2-methylpropan-1-one
CAS No.: 49660-93-7
Chemical Name: 1-(4-Bromophenyl)-2-methylpropan-1-one
Synonyms: 1-(4-Bromophenyl)-2-methyl-1-propanone;1-(4-Bromophenyl)-2-methylpropan-1-one;1-Propanone, 1-(4-bromophenyl)-2-methyl-;1-(4-Bromophenyl)-2-methyl-1-propanone - [B93233]
CBNumber: CB02563594
Molecular Formula: C10H11BrO
Formula Weight: 227.1
MOL File: 49660-93-7.mol

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1-(4-Bromophenyl)-2-methylpropan-1-one Property

Melting point:: 18°C(lit.)
Boiling point:: 87°C/3mmHg(lit.)
Density: 1.331±0.06 g/cm3(Predicted)
refractive index: 1.5550 to 1.5590
storage temp.: Sealed in dry,Room Temperature
form: clear liquid
color: Colorless to Almost colorless

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Safety

HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: B5232
Product name: 1-(4-Bromophenyl)-2-methyl-1-propanone
Purity: >95.0%(GC)
Packaging: 1g
Price: $136
Updated: 2025/07/31

TCI Chemical

Product number: B5232
Product name: 1-(4-Bromophenyl)-2-methyl-1-propanone
Purity: >95.0%(GC)
Packaging: 5g
Price: $468
Updated: 2021/12/16

TRC

Product number: B698400
Product name: 1-(4-Bromophenyl)-2-methylpropan-1-one
Packaging: 250mg
Price: $105
Updated: 2021/12/16

AK Scientific

Product number: V6185
Product name: 1-(4-Bromophenyl)-2-methylpropan-1-one
Packaging: 1g
Price: $138
Updated: 2021/12/16

Rieke Metals

Product number: K0521202
Product name: 1-(4-Bromo-phenyl)-2-methyl-propan-1-one
Packaging: 1g
Price: $260
Updated: 2021/12/16

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1-(4-Bromophenyl)-2-methylpropan-1-one Chemical Properties,Usage,Production

Synthesis

56985-67-2

49660-93-7

General procedure for the synthesis of 1-(4-bromophenyl)-2-methylpropan-1-one from 1-(4-bromophenyl)-2-methylpropan-1-ol: To a dichloromethane ( at 0 °C) containing 1-(4-bromophenyl)-2-methylpropan-1-ol (13.6 g, 60 mmol), ammonium acetate (13.8 g, 178 mmol) and 4?molecular sieves (30 g) ( 500 mL) suspension was added pyridinium chlorochromate (PCC, 19.2 g, 89 mmol) in batches. The reaction mixture was gradually warmed to room temperature and stirred continuously for 14 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and washed with dichloromethane. The volatiles in the filtrate were removed under reduced pressure, and the resulting crude product was purified by silica gel column chromatography to afford 1-(4-bromophenyl)-2-methylpropan-1-one (12.7 g, 94% yield) as a light yellow oil, using dichloromethane as eluent. The product characterization data were as follows: mass spectra (GC-MS) m/z = 226 (100%, [M]+, C10H11BrO), 228 (100%, [M+2]+, C10H11BrO). 1H NMR (400 MHz, CDCl3) δ 7.81 (2H, d, J = 8.6Hz), 7.59 (2H, d, J = 8.6Hz ), 3.49 (1H, sept, J = 6.8Hz), 1.20 (6H, d, J = 6.8Hz).13C NMR (100MHz, CDCl3) δ 203.3, 135.0, 142.7, 132.0, 129.9, 127.9, 35.5, 19.1.

References

[1] Beilstein Journal of Organic Chemistry, 2015, vol. 11, p. 972 - 979
[2] Organic Letters, 2018, vol. 20, # 10, p. 2906 - 2910

1-(4-Bromophenyl)-2-methylpropan-1-one Preparation Products And Raw materials

Raw materials

Preparation Products

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49660-93-7, 1-(4-Bromophenyl)-2-methylpropan-1-oneRelated Search:

1-(4-Bromophenyl)-2-methylpropan-1-one

1-(4-Bromophenyl)-2-methyl-1-propanone

1-Propanone, 1-(4-bromophenyl)-2-methyl-

1-(4-Bromophenyl)-2-methyl-1-propanone - [B93233]

49660-93-7