(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor

Product Name: (3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor
CAS No.: 907606-68-2
Chemical Name: (3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor
Synonyms: (1S,3aR,6aS)-1-Boc-octahydrocyclopenta[c]pyrrole Oxalate;-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate;(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrro...;(3aR,6aS)-1-(tert-Butoxycarbonyl)octahydrocyclopenta[c]pyrroliuM oxalate;(1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrol-1-carboxylate oxalate;(1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate;(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor;(1S,3aR,6aS)-Octahydrocyclopenta[c]pyrrole-1-carboxylic acid t-butyl ester oxalate;(1S,3aR,6aS)-Octahydro-cyclopentacpyrrol-1-carboxylic acid tert-butyl ester oxalate;(1S,3aR,6aS)-Octahydrocyclopenta[c]pyrrole-1-carboxylic acid tert-butyl ester oxalate
CBNumber: CB02582861
Molecular Formula: C14H23NO6
Formula Weight: 301.34
MOL File: 907606-68-2.mol

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(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor Property

Density: 1.26 at 20℃
vapor pressure: 0Pa at 25℃
storage temp.: 2-8°C
Appearance: White to off-white Solid
LogP: 2.7 at 25℃ and pH10
Surface tension: 70mN/m at 1g/L and 20℃

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Safety

HS Code: 2902190000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P273Avoid release to the environment.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB142099
Product name: (1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate
Packaging: 100mg
Price: $51
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142099
Product name: (1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate
Packaging: 250mg
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: Z5320
Product name: (1S,3aR,6aS)-tert-Butyloctahydrocyclopenta[c]pyrrole-1-carboxylateoxalate
Packaging: 250mg
Price: $146
Updated: 2021/12/16

ChemScene

Product number: CS-M2255
Product name: Cyclopenta[c]pyrrole-1-carboxylicacid,octahydro-,1,1-dimethylethylester,(1S,3aR,6aS)-,ethanedioate1:1
Packaging: 1g
Price: $170
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142099
Product name: (1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate
Packaging: 500mg
Price: $175
Updated: 2021/12/16

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(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor Chemical Properties,Usage,Production

Synthesis

540-88-5

1205676-44-3

144-62-7

907606-68-2

[Isolation of hydroxyoxalate] To a mixture of 250 mg of (1S,3aR,6aS)-octahydrocyclopenta[c]pyrrole-1-carboxylic acid hydrochloride (i) and the ammonium chloride prepared in Example 29 was added 4 mL of chloroform and 1.7 mL of tert-butyl acetate. The resulting suspension was cooled to 0°C and then 0.25 mL of methanesulfonic acid was added. The mixture was slowly warmed to 25°C and stirred at this temperature for 18 hours. The resulting white suspension was again cooled to 0°C, and then 1.3 mL of 50% aqueous sodium hydroxide was slowly added while controlling the temperature to not exceed 20°C. 15 mL of water and 15 mL of chloroform were added and stirred for 15 minutes. The organic and aqueous layers were separated and the aqueous layer was extracted three times with 15 mL of chloroform. The organic layers were combined, dried with magnesium sulfate, filtered and the solvent concentrated under reduced pressure. To the light green residue was added 2.5 mL of tert-butyl acetate and 146.7 mg of oxalic acid in a 2.5 mL 2-propanol solution. The mixture was heated to 75-80 °C, stirred for 30 minutes, cooled to room temperature (about 20 °C), continued stirring for 18 hours, and then filtered. The resulting solid was washed sequentially with 5 mL of 2-propanol and 5 mL of methyl tert-butyl ether, and dried to give 0.08 g (0.27 mmol, 25% overall yield based on nitrile (h)) of tert-butyl (1S,3aR,6aS)-octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate (j) as a white solid.

References

[1] Patent: US2014/94616, 2014, A1. Location in patent: Paragraph 0155

(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor Preparation Products And Raw materials

Raw materials

Preparation Products

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(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor Suppliers

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View Lastest Price from (3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor manufacturers

Career Henan Chemical Co

Product: (3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor 907606-68-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 150KG
Release date: 2019-07-09

907606-68-2, (3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyforRelated Search:

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(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrrol-2-iuM carboxyfor

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Cyclopenta[c]pyrrole-1-carboxylic acid, octahydro-, 1,1-diMethylethyl ester, (1S,3aR,6aS)-, ethanedioate (1:1)

Cyclopenta[c]pyrrole-1-carboxylic acid, octahydro-, 1,1-diMethylethyl ester, (1S,3aR,6aS)-, ethanedioate

(1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate

(3aR,6aS)-1-(tert-Butoxycarbonyl)octahydrocyclopenta[c]pyrroliuM oxalate

2-Methyl-2-propanyl (1S,3aR,6aS)-octahydrocyclopenta[c]pyrrole-1-carboxylate ethanedioate (1:1)

(1S,3aR,6aS)-Octahydrocyclopenta[c]pyrrole-1-carboxylic acid t-butyl ester oxalate

-tert-Butyl octahydrocyclopenta[c]pyrrole-1-carboxylate oxalate

tert-butyl (3S,3aS,6aR)-1,2,3,3a,4,5,6,6a-octahydrocyclopenta[c]pyrrole-3-carboxylate

(3aR,6aS)-1-[(tert-butoxy)carbonyl]-octahydrocyclopenta[c]pyrrol-2-ium hydrogen oxalate

(1S,3aR,6aS)-1-Boc-octahydrocyclopenta[c]pyrrole Oxalate

(3aR,6aS)-1-(tert-butoxycarbonyl)octahydrocyclopenta[c]pyrro...

Cyclopenta[c]pyrrole-1-carboxylic acid, octahydro-, 1,1-dimethylethyl ester, (1S,3aR,6aS)-, ethanedioate (1:1) (9CI, ACI)

(1S,3aR,6aS)-octahydro-Cyclopenta[c]pyrrole-1-carboxylic acid 1,1-dimethylethyl ester ethanedioate (1:1) (9CI ACI)

(1S,3aR,6aS)-Octahydro-cyclopentacpyrrol-1-carboxylic acid tert-butyl ester oxalate

(1S,3aR,6aS)-tert-Butyl octahydrocyclopenta[c]pyrrol-1-carboxylate oxalate

907606-68-2

C12H21NO2C2H2O4