ChemicalBook > CAS DataBase List > 2-AMino-4-broMo-5-fluorophenol

2-AMino-4-broMo-5-fluorophenol

Product Name: 2-AMino-4-broMo-5-fluorophenol
CAS No.: 1016234-89-1
Chemical Name: 2-AMino-4-broMo-5-fluorophenol
Synonyms: Phenol, 2-amino-4-bromo-5-fluoro-;5-Bromo-4-fluoro-2-hydroxyaniline;2-AMino-4-broMo-5-fluorophenol ISO 9001：2015 REACH
CBNumber: CB02582997
Molecular Formula: C6H5BrFNO
Formula Weight: 206.01
MOL File: 1016234-89-1.mol

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2-AMino-4-broMo-5-fluorophenol Property

Boiling point:: 288.7±40.0 °C(Predicted)
Density: 1.863±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 8.21±0.23(Predicted)
form: powder
color: Dark brown

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Safety

HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: A602225
Product name: 2-Amino-4-bromo-5-fluorophenol
Packaging: 1g
Price: $350
Updated: 2021/12/16

Apolloscientific

Product number: PC3691
Product name: 2-Amino-4-bromo-5-fluorophenol
Packaging: 250mg
Price: $80
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4656-B-08
Product name: 2-Amino-4-bromo-5-fluorophenol
Packaging: 250mg
Price: $88
Updated: 2021/12/16

AK Scientific

Product number: J52039
Product name: 2-Amino-4-bromo-5-fluorophenol
Packaging: 1g
Price: $150
Updated: 2021/12/16

Apolloscientific

Product number: PC3691
Product name: 2-Amino-4-bromo-5-fluorophenol
Packaging: 1g
Price: $174
Updated: 2021/12/16

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2-AMino-4-broMo-5-fluorophenol Chemical Properties,Usage,Production

Synthesis

1016234-87-9

1016234-89-1

GENERAL STEPS: A suspension of sodium conodisulfite (Na2S2O4, 51.6 g, 296 mmol) in water (122 mL) was slowly added to a refluxed solution of 4-bromo-5-fluoro-2-nitrophenol (14 g, 59.3 mmol) in ethanol (1000 mL). The reaction mixture was continued to reflux for 1 hour. After completion of the reaction, it was cooled to room temperature and filtered to remove the resulting salt. The filtrate was partially concentrated and subsequently saturated aqueous sodium chloride solution was added and extracted with ether. The organic phases were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to afford the crude 2-amino-4-bromo-5-fluorophenol (9.2 g, 75% yield), which was used in the subsequent reaction without further purification.1H-NMR (400 MHz, DMSO-d6) δ: 4.65 (br s, 2H, NH2), 6.60 (d, J = 11.3 Hz, 1H ArH), 6.76 (d, J = 7.8 Hz, 1H, ArH), 9.80 (br s, 1H, OH).

References

[1] Patent: WO2008/37746, 2008, A1. Location in patent: Page/Page column 15
[2] Patent: US2008/90804, 2008, A1. Location in patent: Page/Page column 7
[3] Patent: WO2008/37746, 2008, A1. Location in patent: Page/Page column 15
[4] Patent: WO2010/130773, 2010, A2. Location in patent: Page/Page column 66

2-AMino-4-broMo-5-fluorophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-AMino-4-broMo-5-fluorophenol manufacturers

R&D Scientific Inc.

Product: 2-Amino-4-bromo-5-fluorophenol 1016234-89-1
Price: US $700.00/g
Min. Order: 1g
Purity: 98
Supply Ability: 500 Kg
Release date: 2024-02-12

1016234-89-1, 2-AMino-4-broMo-5-fluorophenolRelated Search:

5-Bromo-4-fluoro-2-hydroxyaniline

Phenol, 2-amino-4-bromo-5-fluoro-

2-AMino-4-broMo-5-fluorophenol ISO 9001：2015 REACH

1016234-89-1