1-(3-broMo-5-nitrophenyl)ethan-1-one

Product Name: 1-(3-broMo-5-nitrophenyl)ethan-1-one
CAS No.: 127413-59-6
Chemical Name: 1-(3-broMo-5-nitrophenyl)ethan-1-one
Synonyms: 1-(3-Bromo-5-nitrophenyl);3'-bromo-5'-nitroacetophenone;1-(3-BroMo-5-nitrophenyl)ethanone;Ethanone, 1-(3-bromo-5-nitrophenyl)-;1-(3-broMo-5-nitrophenyl)ethan-1-one
CBNumber: CB02596039
Molecular Formula: C8H6BrNO3
Formula Weight: 244.04
MOL File: 127413-59-6.mol

More

Less

1-(3-broMo-5-nitrophenyl)ethan-1-one Property

Boiling point:: 293.4±25.0 °C(Predicted)
Density: 1.637±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature

More

Less

Hazard and Precautionary Statements (GHS)

More

Less

N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0361863
Product name: 1-(3-BROMO-5-NITROPHENYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $495.2
Updated: 2021/12/16

AK Scientific

Product number: 5341AA
Product name: 1-(3-Bromo-5-nitrophenyl)ethanone
Packaging: 250mg
Price: $174
Updated: 2021/12/16

Crysdot

Product number: CD12156209
Product name: 1-(3-Bromo-5-nitrophenyl)ethanone
Purity: 98%
Packaging: 1g
Price: $243
Updated: 2021/12/16

Crysdot

Product number: CD12156209
Product name: 1-(3-Bromo-5-nitrophenyl)ethanone
Purity: 98%
Packaging: 5g
Price: $569
Updated: 2021/12/16

Alichem

Product number: 127413596
Product name: 1-(3-Bromo-5-nitrophenyl)ethanone
Packaging: 5g
Price: $1465.2
Updated: 2021/12/16

More

Less

1-(3-broMo-5-nitrophenyl)ethan-1-one Chemical Properties,Usage,Production

Synthesis

7787-71-5

121-89-1

127413-59-6

Example 15: In an ice-water cooled three-necked flask equipped with a magnetic stirrer and condenser, a mixture consisting of 2.5 mL (0.05 mol) of bromine trifluoride and 3.2 mL (0.056 mol) of bromine was vigorously stirred. To the suspension in this flask was added 36 g (0.2 mol) of 3-nitroacetophenone dissolved in 80 mL of Freon 113. The above mixture was added dropwise while maintaining vigorous stirring at a temperature of 20°C. Upon completion of the reaction, the crude reaction mixture was poured into stirred ice and treated with 5% sodium sulfite solution. The organic layer was separated and the aqueous layer was extracted twice with 100 mL of dichloromethane. The organic layers were combined and washed sequentially with 5% sodium bicarbonate solution and water. The organic phase was dried with anhydrous magnesium sulfate and the solvent was evaporated. The residue was removed from unreacted substrate by distillation under reduced pressure and finally recrystallized from toluene. 7.3 g of 3-bromo-5-nitroacetophenone was obtained in 85% yield (calculated based on the reacted substrate).

References

[1] Patent: US4954648, 1990, A

1-(3-broMo-5-nitrophenyl)ethan-1-one Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

1-(3-broMo-5-nitrophenyl)ethan-1-one Suppliers

China 25 India 1 United States 2 Global 28

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

skychemical Co.Ltd

Tel: 021-20960837,QQ1332204249
Fax: 021-20960837
Email: sales@skychemical.com
Country: China
ProdList: 3341
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Suzhou Ruichi Pharmaceutical Technology Co., Ltd.

Tel: 0512-50152853
Fax: 0512-50152853
Email: jjks1111@126.com
Country: China
ProdList: 623
Advantage: 58

Aikon International Limited

Tel: 025-58851090 15955137747
Fax: (6)02557626880
Email: sales01@aikonchem.com
Country: China
ProdList: 15949
Advantage: 58

Shanghai ZiHao Pharmaceutical Co., Ltd.

Tel: 021-13482410-12 13482410112
Fax: -
Email: 362383684@qq.com
Country: China
ProdList: 737
Advantage: 58

Shanghai Benso Pharmaceutical Technology Co., Ltd.

Tel: 15088289376
Email: 248775804@qq.com
Country: China
ProdList: 4995
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418684 +8618949823763
Fax: 0086-551-65418684
Email: sales@tnjchem.com
Country: China
ProdList: 25356
Advantage: 58

Win-Win chemical CO., Limited

Tel: +86-0086-577-64498589 +86-15355981851
Fax: 0086-577-56994596
Email: sales@win-winchemical.com
Country: China
ProdList: 14359
Advantage: 58

Shanxi Xuanran Import and Export Trade Co., Ltd.

Tel: +8617735180244
Email: mike_yan@xuanranglobal.com
Country: CHINA
ProdList: 4017
Advantage: 58

Wuxi Kehua Biological Technology Co., Ltd.

Tel: 0510-86838766 13636419861
Email: 2258830676@qq.com
Country: China
ProdList: 5044
Advantage: 58

CONIER CHEM AND PHARMA LIMITED

Tel: +8618523575427
Email: sales@conier.com
Country: China
ProdList: 49975
Advantage: 58

Fuxin Pharmaceutical

Tel: +86-021-021-50872116 +8613122107989
Email: contact@fuxinpharm.com
Country: China
ProdList: 10000
Advantage: 58

Birdo (Shanghai) Medical Technology Co., Ltd.

Tel: 021-58099077-8041 18601625411
Email: sales@birdotech.com
Country: China
ProdList: 9764
Advantage: 58

Taizhou Nanfeng Pharmaceutical Research Institute

Tel: nanfengdrug@163.com; 18616377689
Email: nanfengdrug@163.com
Country: China
ProdList: 20009
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing1@energy-chemical.com
Country: China
ProdList: 44894
Advantage: 58

Hubei Co-prosperity Medicine Technonlogy Co., Ltd

Tel: 2383948258 19172820304
Email: 2383948258@qq.com
Country: China
ProdList: 12987
Advantage: 58

Beijing Jin Ming Biotechnology Co., Ltd.

Tel: 010-60605840 15801484223;
Email: psaitong@jm-bio.com
Country: China
ProdList: 29757
Advantage: 58

Suzhou rich Medicine Technical Co;Ltd

Tel: 15221533763
Email: suzhourich@163.com
Country: China
ProdList: 984
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Henan Weitixi Chemical Technology Co., Ltd

Tel: 0371-53370800 18037197114
Email: 2853031799@qq.com
Country: China
ProdList: 9892
Advantage: 58

Shanghai Haohong Scientific Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Zhuhai Aobokai Biomedical Technology Co., Ltd.

Tel: 400-0628126 15697565236;
Email: sales-team@aobchem.com.cn
Country: China
ProdList: 50000
Advantage: 58

Aromsyn Co., Ltd.

Tel: +86-0571-85585865 +8613336024896
Email: CB@aromsyn.com
Country: China
ProdList: 19183
Advantage: 58

Shanghai Hao Zhun Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: info@zzsrm.com
Country: CHINA
ProdList: 6650
Advantage: 58

127413-59-6, 1-(3-broMo-5-nitrophenyl)ethan-1-oneRelated Search:

3'-CHLORO-2',6'-DIFLUOROACETOPHENONE 3'-CHLORO-5'-(TRIFLUOROMETHYL)ACETOPHENONE 1-(4-Chloro-2-trifluoromethyl-phenyl)-ethanone 4'-BroMo-2',5'-difluoroacetophenone 4'-Bromo-3'-methylacetophenone 1-(3-Fluoro-5-hydroxyphenyl)ethanone 4-Acetyl-2-methylbenzonitrile Ethanone, 1-[3-hydroxy-4-(phenylMethoxy)phenyl]- 4'-CHLORO-2',5'-DIFLUOROACETOPHENONE 1-(4-Bromo-2-chlorophenyl)propan-1-one 1-(3-Hydroxy-5-Methylphenyl)ethanone

1-(3-broMo-5-nitrophenyl)ethan-1-one

1-(3-BroMo-5-nitrophenyl)ethanone

1-(3-Bromo-5-nitrophenyl)

3'-bromo-5'-nitroacetophenone

Ethanone, 1-(3-bromo-5-nitrophenyl)-

127413-59-6