5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine

Product Name: 5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine
CAS No.: 862729-13-3
Chemical Name: 5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine
Synonyms: 5-iodo-7-methylpyrrolo[2,3-d]pyrimidin-4-amine;5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine;4-Amino-5-iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidine;5-iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-ylamine;7H-Pyrrolo[2,3-d]pyriMidin-4-aMine, 5-iodo-7-Methyl-
CBNumber: CB02598790
Molecular Formula: C7H7IN4
Formula Weight: 274.06
MOL File: 862729-13-3.mol

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5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine Property

Boiling point:: 436.3±40.0 °C(Predicted)
Density: 2.24±0.1 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 5.07±0.30(Predicted)
Appearance: Light brown to gray Solid
InChI: InChI=1S/C7H7IN4/c1-12-2-4(8)5-6(9)10-3-11-7(5)12/h2-3H,1H3,(H2,9,10,11)
InChIKey: VNFSLRASQZPDFQ-UHFFFAOYSA-N
SMILES: C1=NC(N)=C2C(I)=CN(C)C2=N1

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 3489AC
Product name: 5-Iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Packaging: 100mg
Price: $97
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367493
Product name: 5-IODO-7-METHYL-7H-PYRROLO[2,3-D]PYRIMIDIN-4-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $500.87
Updated: 2021/12/16

Matrix Scientific

Product number: 096424
Product name: 5-Iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Purity: 95+%
Packaging: 250mg
Price: $742
Updated: 2021/12/16

Matrix Scientific

Product number: 096424
Product name: 5-Iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Purity: 95+%
Packaging: 1g
Price: $1647
Updated: 2021/12/16

AK Scientific

Product number: 3489AC
Product name: 5-Iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
Packaging: 10g
Price: $1738
Updated: 2021/12/16

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5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine Chemical Properties,Usage,Production

Synthesis

163622-50-2

74-88-4

862729-13-3

GENERAL STEPS: To a solution of 750 mg (2.88 mmol) of 5-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-amine dissolved in 20 mL of anhydrous N,N-dimethylformamide (DMF), 190 μL (3.02 mmol) of iodomethane and 795 mg (5.76 mmol) of anhydrous potassium carbonate were added. The reaction mixture was stirred for 8 h at room temperature. After completion of the reaction, the solvent was removed by rotary evaporator. The residue was dissolved in dichloromethane (DCM) and washed with deionized water. The organic layer was dried with anhydrous sodium sulfate, filtered and the solvent was again removed by rotary evaporator to give 394 mg (50% yield) of the target compound 5-iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine. High resolution mass spectrometry (HRMS, electrospray ionization ESI) analysis resulted in the calculated value of C7H7N4I [M + H]+ 274.9788 and the measured value of 274.9788, which is in agreement with expectations.

References

[1] Patent: WO2014/184069, 2014, A1. Location in patent: Page/Page column 34; 35

5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine Suppliers

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