2-Methyl-5-acetylpyriMidine
- Product Name
- 2-Methyl-5-acetylpyriMidine
- CAS No.
- 1225223-42-6
- Chemical Name
- 2-Methyl-5-acetylpyriMidine
- Synonyms
- 2-Methl-5-acetylpyrimidine;2-Methyl-5-acetylpyriMidine;1-(2-Methyl-5-pyriMidyl)ethanone;1-(2-MethylpyriMidin-5-yl)ethanone;1-(2-Methyl-5-pyrimidinyl)ethanone;Ethanone, 1-(2-methyl-5-pyrimidinyl)-;1-(2-methylpyrimidin-5-yl)ethan-1-one
- CBNumber
- CB02602417
- Molecular Formula
- C7H8N2O
- Formula Weight
- 136.15
- MOL File
- 1225223-42-6.mol
2-Methyl-5-acetylpyriMidine Property
- Boiling point:
- 219.9±13.0 °C(Predicted)
- Density
- 1.100±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 0.02±0.22(Predicted)
- Appearance
- White to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M221075
- Product name
- 1-(2-Methyl-5-pyrimidyl)ethanone
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 4912AJ
- Product name
- 1-(2-Methylpyrimidin-5-yl)ethanone
- Packaging
- 1g
- Price
- $397
- Updated
- 2021/12/16
- Product number
- 123631
- Product name
- 1-(2-Methylpyrimidin-5-yl)ethanone
- Purity
- 95+%
- Packaging
- 1g
- Price
- $826
- Updated
- 2021/12/16
- Product number
- CD11323434
- Product name
- 1-(2-Methylpyrimidin-5-yl)ethanone
- Purity
- 97%
- Packaging
- 250mg
- Price
- $157
- Updated
- 2021/12/16
- Product number
- CD11323434
- Product name
- 1-(2-Methylpyrimidin-5-yl)ethanone
- Purity
- 97%
- Packaging
- 1g
- Price
- $410
- Updated
- 2021/12/16
2-Methyl-5-acetylpyriMidine Chemical Properties,Usage,Production
Synthesis
1421922-89-5
1225223-42-6
General procedure for the synthesis of 1-(2-methyl-5-pyrimidinyl)ethanone from the compound (CAS: 1421922-89-5): the compound (0.47 g) obtained in Reference Example 38-1 was dissolved in acetone (8.0 mL), 1.0 mol/L aqueous hydrochloric acid (2.0 mL) was added, and the reaction was stirred for 24 hours at room temperature. After completion of the reaction, water and saturated aqueous sodium bicarbonate solution were added to the reaction mixture, stirred and extracted using chloroform. The organic layer was separated by a phase separator and the solvent was subsequently removed by distillation under reduced pressure to afford 1-(2-methyl-5-pyrimidinyl)ethanone (0.40 g), the product was a pale yellow solid.1H NMR (600 MHz, chloroform-d) δ ppm: 2.63 (3H, s), 2.80-2.84 (3H, m), 9.13 (2H, s).
References
[1] Patent: US2014/155597, 2014, A1. Location in patent: Paragraph 0373; 0374; 0375
2-Methyl-5-acetylpyriMidine Preparation Products And Raw materials
Raw materials
Preparation Products
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