11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
- Product Name
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
- CAS No.
- 1024598-06-8
- Chemical Name
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
- Synonyms
- 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole;11,12-Dihydro-11-phenylindo;11-phenylindolo[2,3-a]carbazole;12-Phenyl-11H-indolo[2,3-a]carbazole;1-Phenyl-11,12-dihydroindolo[2,3-a]carbazole;1,12-Dihydro-11-phenylindolo[2,3-a]carbazole;11,12-Dihydro-11-phenylindolo[2,3-a]carbazole;Indolo[2,3-a]carbazole, 11,12-dihydro-11-phenyl-;11,12-Dihydro-11-phenylindolo[2,3-a]carbazole>11,12-Dihydro-11-phenyl-1H-indolo[2,3-a]carbazole
- CBNumber
- CB02614434
- Molecular Formula
- C24H16N2
- Formula Weight
- 332.4
- MOL File
- 1024598-06-8.mol
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Property
- Boiling point:
- 598.8±32.0 °C(Predicted)
- Density
- 1.26
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- 16.78±0.30(Predicted)
- color
- White to Light yellow to Light orange
- InChI
- InChI=1S/C24H16N2/c1-2-8-16(9-3-1)26-22-13-7-5-11-18(22)20-15-14-19-17-10-4-6-12-21(17)25-23(19)24(20)26/h1-15,25H
- InChIKey
- IENOQUQIVSMWGP-UHFFFAOYSA-N
- SMILES
- N1C2=C(C=CC=C2)C2=C1C1N(C3=CC=CC=C3)C3=C(C=1C=C2)C=CC=C3
- CAS DataBase Reference
- 1024598-06-8
Safety
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- D4860
- Product name
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 200mg
- Price
- $98
- Updated
- 2025/07/31
- Product number
- D4860
- Product name
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 1g
- Price
- $293
- Updated
- 2025/07/31
- Product number
- P321190
- Product name
- 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- P321190
- Product name
- 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole
- Packaging
- 100mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- 42711
- Product name
- 11,12-Dihydro-11-phenylindolo[2,3-α]carbazole,≥97%(HPLC)
- Purity
- ≥97%(HPLC)
- Packaging
- 200MG
- Price
- $113.25
- Updated
- 2021/12/16
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Chemical Properties,Usage,Production
Synthesis
108-86-1
60511-85-5
1024598-06-8
General procedure for the synthesis of 11,12-dihydro-11-phenylindolo[2,3-a]carbazole from bromobenzene and 11,12-dihydroindolo[2,3-a]carbazole: Pd2(dba)3 (178.6 mg, 0.20 mmol) and t-Bu3P (78.9 mg, 0.39 mmol) were mixed with Pd2(dba)3 (178.6 mg, 0.20 mmol) and t-Bu3P (78.9 mg, 0.39 mmol) in o-xylene (50 mL) at room temperature under stirred for 10 min. Subsequently, 11,12-dihydroindolo[2,3-a]carbazole (Intermediate I-1, 5 g, 19.51 mmol), bromobenzene (3.37 g, 21.46 mmol), and t-BuONa (1.12 g, 11.71 mmol) were added and stirred at reflux for 48 hours at 160 °C. After completion of the reaction, it was cooled to room temperature, distilled water (20 mL) was added and extracted with ethyl acetate. The organic phase was dried over magnesium sulfate, filtered and the solvent evaporated. Purification by column chromatography afforded 11,12-dihydro-11-phenylindolo[2,3-a]carbazole (Intermediate I-2, 5.35 g, 83% yield).MS-EI, m/e: 332.13 (calculated), 332.19 (measured).
References
[1] Patent: KR2015/96018, 2015, A. Location in patent: Paragraph 0377-0379
[2] Patent: US2018/90690, 2018, A1. Location in patent: Paragraph 0161; 0162
[3] Patent: KR2018/32519, 2018, A. Location in patent: Paragraph 0120-0122
[4] Patent: EP2894157, 2015, A1. Location in patent: Paragraph 0198
[5] Patent: KR2015/84657, 2015, A. Location in patent: Paragraph 1642-1645
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Preparation Products And Raw materials
Raw materials
Preparation Products
11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Suppliers
- Tel
- 03-36680489
- Fax
- 03-3668-0520
- Sales-JP@TCIchemicals.com
- Country
- Japan
- ProdList
- 28387
- Advantage
- 80
View Lastest Price from 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole manufacturers
- Product
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole 1024598-06-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-14
- Product
- 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole 1024598-06-8
- Price
- US $188.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-05
- Product
- 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole 1024598-06-8
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%Min
- Supply Ability
- 1000kg
- Release date
- 2023-03-12