9-(2-Naphthyl)-3-broMocarbazole
- Product Name
- 9-(2-Naphthyl)-3-broMocarbazole
- CAS No.
- 934545-80-9
- Chemical Name
- 9-(2-Naphthyl)-3-broMocarbazole
- Synonyms
- 3-B2NC;9H-Carbazole, 3-bro;9-(2-phthyl)-3-broMocarbazole;9-(2-Naphthyl)-3-broMocarbazole;3-Bromo-9-(2-naphthyl)carbazole;N-(2-naphthyl)-3-bromocarbazole;3-bromo-9-naphthalen-2-ylcarbazole;3-Bromo-9-(2-naphthyl)-9H-carbazole;3-Bromo-9-(phthalen-2-yl)-9H-carbazole;3-bromo-9-(2-naphthalenyl)-9H-Carbazole
- CBNumber
- CB02655327
- Molecular Formula
- C22H14BrN
- Formula Weight
- 372.26
- MOL File
- 934545-80-9.mol
9-(2-Naphthyl)-3-broMocarbazole Property
- Melting point:
- 131.0 to 135.0 °C
- Boiling point:
- 545.2±32.0 °C(Predicted)
- Density
- 1.39±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Almost white
- InChI
- InChI=1S/C22H14BrN/c23-17-10-12-22-20(14-17)19-7-3-4-8-21(19)24(22)18-11-9-15-5-1-2-6-16(15)13-18/h1-14H
- InChIKey
- MBGUQKKYEOAENA-UHFFFAOYSA-N
- SMILES
- N1(C2=CC=C3C(=C2)C=CC=C3)C2=C(C=CC=C2)C2=C1C=CC(Br)=C2
- CAS DataBase Reference
- 934545-80-9
Safety
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B5028
- Product name
- 3-Bromo-9-(2-naphthyl)carbazole
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 1g
- Price
- $60
- Updated
- 2025/07/31
- Product number
- B5028
- Product name
- 3-Bromo-9-(2-naphthyl)carbazole
- Purity
- >97.0%(HPLC)(N)
- Packaging
- 5g
- Price
- $178
- Updated
- 2025/07/31
- Product number
- B701073
- Product name
- 3-Bromo-9-(naphthalen-2-yl)-9H-carbazole
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B701073
- Product name
- 3-Bromo-9-(naphthalen-2-yl)-9H-carbazole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 6004AL
- Product name
- 3-Bromo-9-(2-naphthyl)carbazole
- Packaging
- 5g
- Price
- $180
- Updated
- 2021/12/16
9-(2-Naphthyl)-3-broMocarbazole Chemical Properties,Usage,Production
Chemical Properties
White crystal
Synthesis
34292-03-0
934545-80-9
General procedure for the synthesis of N-(2-naphthalenyl)-3-bromocarbazole from 9-(naphthalen-2-yl)-9H-carbazole: Compound 3-1 (9-(naphthalen-2-yl)-9H-carbazole) (24 g, 93.2 mmol) and N-bromosuccinimide (14 g, 79 mmol) were dissolved in 832 mL of tetrahydrofuran (THF) and the reaction mixture was stirred at room temperature for 20 hours. Upon completion of the reaction, the organic layer was extracted with ethyl acetate and dried with anhydrous magnesium sulfate to remove residual water. Subsequently, the remaining product was purified by column chromatography to afford compound 3-2 (N-(2-naphthyl)-3-bromocarbazole) (26.4 g, yield: 84%).
References
[1] Patent: WO2016/36207, 2016, A1. Location in patent: Paragraph 116-117; 122-123; 134-135; 138-139
[2] Patent: KR2016/29399, 2016, A. Location in patent: Paragraph 0138; 0139; 0142; 0143
[3] Patent: WO2016/64227, 2016, A1. Location in patent: Paragraph 180
[4] Bulletin of the Korean Chemical Society, 2011, vol. 32, # 3, p. 841 - 846
[5] Patent: KR2015/21171, 2015, A. Location in patent: Paragraph 0239; 0240; 0241; 0248; 0249
9-(2-Naphthyl)-3-broMocarbazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-(2-Naphthyl)-3-broMocarbazole manufacturers
- Product
- 9H-Carbazole, 3-bromo-9-(2-naphthalenyl)- 934545-80-9
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-17
- Product
- 9-(2-Naphthyl)-3-bromocarbazole 934545-80-9
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-31
- Product
- 3-B2NC 934545-80-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11