(1S,3S)-phenylethylpyrrolidinylMethanol

Product Name: (1S,3S)-phenylethylpyrrolidinylMethanol
CAS No.: 173724-95-3
Chemical Name: (1S,3S)-phenylethylpyrrolidinylMethanol
Synonyms: (1S,3S)-phenylethylpyrrolidinylMethanol;Benzenemethanol,α-(aminomethyl)-5-bromo-;((S)-1-((S)-1-Phenylethyl)pyrrolidin-3-yl)methanol;3-Pyrrolidinemethanol, 1-[(1S)-1-phenylethyl]-, (3S)-
CBNumber: CB02676597
Molecular Formula: C13H19NO
Formula Weight: 205.3
MOL File: 173724-95-3.mol

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(1S,3S)-phenylethylpyrrolidinylMethanol Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Activate Scientific

Product number: AS111401
Product name: ((S)-1-((S)-1-Phenylethyl)pyrrolidin-3-yl)methanol
Purity: 95% ee
Packaging: 250mg
Price: $356
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CCH0001575
Product name: ((S)-1-((S)-1-PHENYLETHYL)PYRROLIDIN-3-YL)METHANOL
Purity: 95.00%
Packaging: 5MG
Price: $504.24
Updated: 2021/12/16

Activate Scientific

Product number: AS111401
Product name: ((S)-1-((S)-1-Phenylethyl)pyrrolidin-3-yl)methanol
Purity: 95% ee
Packaging: 1g
Price: $831
Updated: 2021/12/16

Activate Scientific

Product number: AS111401
Product name: ((S)-1-((S)-1-Phenylethyl)pyrrolidin-3-yl)methanol
Purity: 95% ee
Packaging: 100mg
Price: $268
Updated: 2021/12/16

Ambeed

Product number: A215492
Product name: ((S)-1-((S)-1-Phenylethyl)pyrrolidin-3-yl)methanol
Purity: 95%
Packaging: 1g
Price: $325
Updated: 2021/12/16

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(1S,3S)-phenylethylpyrrolidinylMethanol Chemical Properties,Usage,Production

Synthesis

146348-14-3

173724-95-3

General procedure for the synthesis of ((S)-1-((S)-1-phenylethyl)pyrrolidin-3-yl)methanol from (S)-methyl 5-oxoimino-1-((S)-1-phenylethyl)pyrrolidin-3-carboxylate: methyl 5-oxo-1-(1-phenylethyl)-pyrrolidine-3-carboxylate (10.0 g, 40.5 mmol) was dissolved in ether and slowly added to an ether slurry of lithium aluminum hydride (LAH, 2.31 g, 60.86 mmol). The reaction mixture was heated to reflux for 4 hours. Upon completion of the reaction, it was cooled to room temperature and the reaction was quenched with an ether/water mixture. The resulting solution was continued to be stirred at room temperature for 1 hour. The reaction mixture was filtered and the solid was washed with dichloromethane. The filtrate was concentrated under reduced pressure to give 7.76 g of the target product ((S)-1-((S)-1-phenylethyl)pyrrolidin-3-yl)methanol in 94% yield. Mass spectral analysis (APCI+): m/z 206 ([M+H]+).

References

[1] Patent: WO2005/49602, 2005, A1. Location in patent: Page/Page column 88; 89; 122
[2] Patent: WO2005/49605, 2005, A1. Location in patent: Page/Page column 116; 117; 150
[3] Organic and Biomolecular Chemistry, 2017, vol. 15, # 11, p. 2397 - 2402
[4] Patent: WO2007/100670, 2007, A1. Location in patent: Page/Page column 50-51

(1S,3S)-phenylethylpyrrolidinylMethanol Preparation Products And Raw materials

Raw materials

Preparation Products

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(1S,3S)-phenylethylpyrrolidinylMethanol Suppliers

China 16 India 1 United States 2 Global 19

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