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4-(2-Bromoethynyl)benzoic acid

Product Name
4-(2-Bromoethynyl)benzoic acid
CAS No.
1485684-77-2
Chemical Name
4-(2-Bromoethynyl)benzoic acid
Synonyms
4- (broMoethynyl)benzoic acid;4-(2-bromoethynyl)benzoic acid;Benzoic acid, 4-(2-bromoethynyl)-;4-(2-BROMOETHYNYL)BENZOIC ACID(WXC01681)
CBNumber
CB02677145
Molecular Formula
C9H5BrO2
Formula Weight
225.04
MOL File
1485684-77-2.mol
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Hazard and Precautionary Statements (GHS)

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4-(2-Bromoethynyl)benzoic acid Chemical Properties,Usage,Production

Synthesis

To a solution of methyl 4,-(bromomethyl) benzoate (67 g, 250 mmol, 10 equiv) in (1100 mL) was added NaOH (44,84 g, 4,0 equiv) and the reaction mixture was stirred at 25°C for 3 hr. The volatiles were removed under reduced pressure and the resulting solution was neutralized with 1 HCl to pH 3-5. 4- (bromomethyl) benzoic acid (INT-1.5) was collected by filtration. The filter cake was washed with water and dried in an oven at 50°C for 5 hr to yield 4- (broMoethynyl)benzoic acid (61g, 96%).
    

4-(2-Bromoethynyl)benzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-(2-Bromoethynyl)benzoic acid manufacturers

Career Henan Chemical Co
Product
4- (broMoethynyl)benzoic acid 1485684-77-2
Price
US $1.00/g
Min. Order
1g
Purity
≥98%
Supply Ability
g/kg/Ton
Release date
2019-12-25

1485684-77-2, 4-(2-Bromoethynyl)benzoic acidRelated Search:


  • 4- (broMoethynyl)benzoic acid
  • 4-(2-BROMOETHYNYL)BENZOIC ACID(WXC01681)
  • 4-(2-bromoethynyl)benzoic acid
  • Benzoic acid, 4-(2-bromoethynyl)-
  • 1485684-77-2