4-(3-Pyridyl)-1-butanol

Product Name: 4-(3-Pyridyl)-1-butanol
CAS No.: 60753-14-2
Chemical Name: 4-(3-Pyridyl)-1-butanol
Synonyms: 3-Pyridinebutanol;4-(3-Pyridyl)-1-butanol;4-(Pyridin-3-yl)butan-1-ol
CBNumber: CB02683544
Molecular Formula: C9H13NO
Formula Weight: 151.21
MOL File: 60753-14-2.mol

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4-(3-Pyridyl)-1-butanol Property

Boiling point:: 115-125 °C(Press: 0.5 Torr)
Density: 1.035±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 15.10±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P992580
Product name: 4-(3-Pyridyl)-1-butanol
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: P992580
Product name: 4-(3-Pyridyl)-1-butanol
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Apolloscientific

Product number: OR919224
Product name: 3-Pyridinebutanol
Purity: 95%
Packaging: 1g
Price: $150
Updated: 2021/12/16

Apolloscientific

Product number: OR919224
Product name: 3-Pyridinebutanol
Purity: 95%
Packaging: 5g
Price: $435
Updated: 2021/12/16

AK Scientific

Product number: 5963AJ
Product name: 4-(3-Pyridyl)-1-butanol
Packaging: 5g
Price: $509
Updated: 2021/12/16

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4-(3-Pyridyl)-1-butanol Chemical Properties,Usage,Production

Synthesis

138487-20-4

60753-14-2

General procedure for the synthesis of 4-(3-pyridinyl)-1-butyn-1-ol from 4-(3-pyridinyl)-3-butyn-1-ol: 4-(3-pyridinyl)-3-butyn-1-ol (0.32 g, 2.2 mmol) was dissolved in EtOH (44 mL) and passed through a H-Cube?flow hydrogenation reactor fitted with 10% Pd/C catalyst to carry out the hydrogenation reaction (flow rate : 1.0 mL/min; pressure: 1.0 bar; temperature: 3.5°C). After completion of the reaction, the output solution was concentrated to dryness to give an oily residue (0.31 g). Purification by conventional silica gel fast chromatography (eluent: CH2Cl2/MeOH, 95:5) afforded pure 4-(3-pyridyl)-1-butanol (0.294 g, 89% yield) as a colorless liquid. rf = 1.16 mm. m/z MS (ESI) m/z: 152 [M-H]-. 1H NMR (DMSO-d6) δ: 8.43 (m. 1H), 8.38 (dd, 1H, J = 4.8, 1.5 Hz), 7.61 (dt, 1H, J = 7.8, 2.1 Hz), 7.30 (dd, 1H, J = 7.8, 4.8 Hz), 4.37 (t, 1H, J = 5.2 Hz), 3.41 (q, 2H, J = 5.2 Hz), 2.59 (t, 2H, J = 7.7 Hz), 1.64-1.55 (m, 2H), 1.47-1.38 (m, 2H).

References

[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 6, p. 2573 - 2590
[2] Patent: WO2014/144836, 2014, A2. Location in patent: Paragraph 0614; 0615
[3] Bioorganic and Medicinal Chemistry Letters, 2001, vol. 11, # 8, p. 1077 - 1080

4-(3-Pyridyl)-1-butanol Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(3-Pyridyl)-1-butanol Suppliers

China 27 India 1 United States 4 Global 32

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60753-14-2, 4-(3-Pyridyl)-1-butanolRelated Search:

2-Butanol

4-(3-Pyridyl)-1-butanol

3-Pyridinebutanol

4-(Pyridin-3-yl)butan-1-ol

60753-14-2