ChemicalBook > CAS DataBase List > 3'-bromo-2'-methylacetophenone
3'-bromo-2'-methylacetophenone
- Product Name
- 3'-bromo-2'-methylacetophenone
- CAS No.
- 52779-76-7
- Chemical Name
- 3'-bromo-2'-methylacetophenone
- Synonyms
- Fluralaner-006;Fluralaner Impurity 32;3'-broMo-2'-Methylacetophenone;1-(3-Bromo-2-methylphenyl)ethanone;1-(3-bromo-2-methylphenyl)ethan-1-one;Ethanone, 1-(3-bromo-2-methylphenyl)-;1-(3-Bromo-2-Methylphenyl)Ethanone(WXC02293)
- CBNumber
- CB02704889
- Molecular Formula
- C9H9BrO
- Formula Weight
- 213.07
- MOL File
- 52779-76-7.mol
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3'-bromo-2'-methylacetophenone Property
- Boiling point:
- 272.7±28.0 °C(Predicted)
- Density
- 1.388±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- InChI
- InChI=1S/C9H9BrO/c1-6-8(7(2)11)4-3-5-9(6)10/h3-5H,1-2H3
- InChIKey
- LBNWYNIGDUWAOQ-UHFFFAOYSA-N
- SMILES
- C(=O)(C1=CC=CC(Br)=C1C)C
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N-Bromosuccinimide Price
TRC
- Product number
- B814718
- Product name
- 1-(3-bromo-2-methylphenyl)ethanone
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
Activate Scientific
- Product number
- AS147016
- Product name
- 1-(3-Bromo-2-methylphenyl)ethanone
- Purity
- 97%
- Packaging
- 5G
- Price
- $554
- Updated
- 2021/12/16
AK Scientific
- Product number
- 1150CZ
- Product name
- 1-(3-Bromo-2-methylphenyl)ethanone
- Packaging
- 5g
- Price
- $789
- Updated
- 2021/12/16
Alichem
- Product number
- 52779767
- Product name
- 3'-Bromo-2'-methylacetophenone
- Packaging
- 500mg
- Price
- $798.7
- Updated
- 2021/12/16
Crysdot
- Product number
- CD12064931
- Product name
- 1-(3-Bromo-2-methylphenyl)ethanone
- Purity
- 95+%
- Packaging
- 10g
- Price
- $832
- Updated
- 2021/12/16
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3'-bromo-2'-methylacetophenone Chemical Properties,Usage,Production
Synthesis
To a stirred and refluxing Grignard-complex, previously prepared starting from 7.3 parts of magnesium, 52.6 parts of methyl iodide in 160 parts of ether, is added dropwise a solution of 19.6 parts of 3'-bromo-2'-methylbenzonitrile in 40 parts of ether. Upon completion, stirring at reflux is continued for 20 hours. The reaction mixture is cooled to 0 C and poured onto 500 parts of ice water while stirring vigorously. The ethereal phase is separated, dried and evaporated. The residue is boiled in 60 parts of a 6N hydrochloric acid solution for 10 minutes. The separated oil is extracted with ether. The extract is washed with water, dried and evaporated. The residue is distilled, yielding 3'-bromo-2'-methylacetophenone.
3'-bromo-2'-methylacetophenone Preparation Products And Raw materials
Raw materials
Preparation Products
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