ChemicalBook > CAS DataBase List > 2-ForMylisonicotinic acid

2-ForMylisonicotinic acid

Product Name
2-ForMylisonicotinic acid
CAS No.
855636-38-3
Chemical Name
2-ForMylisonicotinic acid
Synonyms
2-ForMylisonicotinic acid;2-formyl-4-Pyridinecarboxylic acid;2-formylpyridine-4-carboxylic acid;4-Pyridinecarboxylic acid, 2-formyl-
CBNumber
CB02727538
Molecular Formula
C7H5NO3
Formula Weight
151.12
MOL File
855636-38-3.mol
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2-ForMylisonicotinic acid Property

storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
F754670
Product name
2-FormylisonicotinicAcid
Packaging
25mg
Price
$155
Updated
2021/12/16
AK Scientific
Product number
3286AC
Product name
2-Formylisonicotinicacid
Packaging
1g
Price
$3117
Updated
2021/12/16
AccelPharmtech
Product number
D2593
Product name
2-formyl-4-Pyridinecarboxylicacid
Purity
97.00%
Packaging
1G
Price
$3120
Updated
2021/12/16
AccelPharmtech
Product number
D2593
Product name
2-formyl-4-Pyridinecarboxylicacid
Purity
97.00%
Packaging
5G
Price
$5360
Updated
2021/12/16
Crysdot
Product number
CD11044191
Product name
2-Formylisonicotinicacid
Purity
95+%
Packaging
250mg
Price
$251
Updated
2021/12/16
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2-ForMylisonicotinic acid Chemical Properties,Usage,Production

Synthesis

4021-11-8

855636-38-3

2-Methyl-4-pyridinecarboxylic acid (5.0 g, 36.5 mmol) was used as raw material and mixed with selenium dioxide (10.1 g, 91.3 mmol) in 250 ml of dioxane. The reaction mixture was heated to 110°C and the reaction was continued under magnetic stirring for 24 hours. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was filtered while hot to remove insoluble impurities. Subsequently, the solvent was removed by distillation under reduced pressure to obtain the crude product. The crude product was purified by recrystallization from anhydrous ethanol and finally dried under vacuum to give 2-formyl-4-pyridinecarboxylic acid as a white solid in 72% yield and 98% purity.

References

[1] Patent: CN107686464, 2018, A. Location in patent: Paragraph 0021; 0022; 0024; 0026; 0028; 0030

2-ForMylisonicotinic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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855636-38-3, 2-ForMylisonicotinic acidRelated Search:


  • 2-ForMylisonicotinic acid
  • 2-formyl-4-Pyridinecarboxylic acid
  • 4-Pyridinecarboxylic acid, 2-formyl-
  • 2-formylpyridine-4-carboxylic acid
  • 855636-38-3