1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride
- Product Name
- 1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride
- CAS No.
- 242452-35-3
- Chemical Name
- 1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride
- Synonyms
- 1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride
- CBNumber
- CB02735971
- Molecular Formula
- C10H17ClN2
- Formula Weight
- 200.70838
- MOL File
- 242452-35-3.mol
1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
N-Bromosuccinimide Price
- Product number
- 5268EA
- Product name
- 1-(4-(Aminomethyl)phenyl)-N,N-dimethylmethanaminehydrochloride
- Packaging
- 10g
- Price
- $647
- Updated
- 2021/12/16
- Product number
- A229911
- Product name
- 1-(4-(Aminomethyl)phenyl)-N,N-dimethylmethanaminehydrochloride
- Purity
- 95%
- Packaging
- 250mg
- Price
- $38
- Updated
- 2021/12/16
- Product number
- A229911
- Product name
- 1-(4-(Aminomethyl)phenyl)-N,N-dimethylmethanaminehydrochloride
- Purity
- 95%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- CM192147
- Product name
- 1-(4-(aminomethyl)phenyl)-N,N-dimethylmethanaminehydrochloride
- Purity
- 95%
- Packaging
- 5g
- Price
- $252
- Updated
- 2021/12/16
- Product number
- CD12092599
- Product name
- 1-(4-(Aminomethyl)phenyl)-N,N-dimethylmethanaminehydrochloride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $267
- Updated
- 2021/12/16
1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride Chemical Properties,Usage,Production
Synthesis
35525-86-1
242452-35-3
General procedure for the synthesis of 1-(4-(aminomethyl)phenyl)-N,N-dimethylmethylamine hydrochloride from 4-[(dimethylamino)methyl]benzonitrile: To a solution of 4-[(dimethylamino)methyl]benzonitrile (1.30 g, 8.12 mmol, 1.0 eq.) in tetrahydrofuran (THF, 10 mL), was added 1 M borane-tetrahydrofuran complex ( 24.4 mL, 24.4 mmol, 3.0 equiv). The reaction mixture was heated to reflux temperature and kept under nitrogen protection for 16 hours. After completion of the reaction, it was cooled to room temperature, a methanol solution of 1 M hydrochloric acid (20 mL) was added and heated to reflux again for 1 hour. After the reaction mixture was cooled to room temperature, the precipitate was collected by filtration. The resulting solid was washed with ether and dried in vacuum to give 1-(4-(aminomethyl)phenyl)-N,N-dimethylmethylamine hydrochloride (1.50 g, 7.50 mmol, 92.6% yield) as a white solid.
References
[1] Patent: WO2016/144792, 2016, A1. Location in patent: Paragraph 00900; 00902
[2] Patent: US2004/10033, 2004, A1. Location in patent: Page/Page column 22-23
[3] Patent: EP1105120, 2005, B1. Location in patent: Page/Page column 25
1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
1-(4-(AMinoMethyl)phenyl)-N,N-diMethylMethanaMine hydrochloride Suppliers
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