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(3-Bromophenyl)triphenylsilane

Product Name
(3-Bromophenyl)triphenylsilane
CAS No.
185626-73-7
Chemical Name
(3-Bromophenyl)triphenylsilane
Synonyms
3-Bromotetraphenylsilane;(3-Bromophenyl)triphenylsilane;(3-Bromopheny|) tripheny|si|ane;Silane, (3-bromophenyl)triphenyl-;1-bromo-3-(triphenylsilyl)-Benzene;3-bromophenyltriphenylsilyl chloride;Benzene, 1-bromo-3-(triphenylsilyl)-;(3-Bromophenyl)triphenylsilane - [B89405]
CBNumber
CB02973311
Molecular Formula
C24H19BrSi
Formula Weight
415.4
MOL File
185626-73-7.mol
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(3-Bromophenyl)triphenylsilane Property

Melting point:
135.0 to 139.0 °C
Boiling point:
469.9±37.0 °C(Predicted)
Density 
1.30±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Light yellow
InChI
InChI=1S/C24H19BrSi/c25-20-11-10-18-24(19-20)26(21-12-4-1-5-13-21,22-14-6-2-7-15-22)23-16-8-3-9-17-23/h1-19H
InChIKey
WTYKIOBQNRWDQP-UHFFFAOYSA-N
SMILES
C1(Br)=CC=CC([Si](C2=CC=CC=C2)(C2=CC=CC=C2)C2=CC=CC=C2)=C1
CAS DataBase Reference
185626-73-7
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Safety

HS Code 
2931.90.6000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B5222
Product name
(3-Bromophenyl)triphenylsilane
Purity
>98.0%(GC)
Packaging
1g
Price
$198
Updated
2025/07/31
TCI Chemical
Product number
B5222
Product name
(3-Bromophenyl)triphenylsilane
Purity
>98.0%(GC)
Packaging
200mg
Price
$52
Updated
2025/07/31
TRC
Product number
B807933
Product name
(3-Bromophenyl)triphenylsilane
Packaging
25mg
Price
$75
Updated
2021/12/16
AK Scientific
Product number
8632AH
Product name
(3-Bromophenyl)triphenylsilane
Packaging
1g
Price
$139
Updated
2021/12/16
AK Scientific
Product number
8632AH
Product name
(3-Bromophenyl)triphenylsilane
Packaging
5g
Price
$379
Updated
2021/12/16
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(3-Bromophenyl)triphenylsilane Chemical Properties,Usage,Production

Uses

(3-Bromophenyl)triphenylsilane is used as a material for organic electroluminescent elements, display devices and lighting devices.

Synthesis

1,3-Dibromobenzene 20 g (84.77 mmol) was dissolved in THF 500 mL and then cooled to a temperature of -78. n-BuLi 2.5M 33.9 mL(84.77 mmol) was slowly added thereinto and then stirred at a temperature of -78 for 1 hour. Chlorotriphenylsilane ((C6H5)3SiCl) 29.9 g was dissolved in THF 100 mL, and this solution was added to the above reaction mixture. The resultant mixture was slowly warmed to room temperature and stirred for 12 hours. Then, extraction with EA, wash with distilled water and aqueous NaCl solution, drying over MgSO4, distillation under reduced pressure, and recrystallization with MC-MeOH in the ratio of 1:10, were sequentially performed, thereby obtaining (3-Bromophenyl)triphenylsilane 18 g(95 percent).

References

[1] Patent: EP2857395, 2015, A1. Location in patent: Paragraph 0071
[2] Patent: WO2011/99718, 2011, A1. Location in patent: Page/Page column 15
[3] RSC Advances, 2015, vol. 5, # 35, p. 27235 - 27241
[4] Patent: CN103819455, 2016, B. Location in patent: Paragraph 0053; 0060; 0061
[5] Patent: KR2015/34146, 2015, A. Location in patent: Paragraph 0045; 0052; 0053

(3-Bromophenyl)triphenylsilane Preparation Products And Raw materials

Raw materials

Preparation Products

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(3-Bromophenyl)triphenylsilane Suppliers

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View Lastest Price from (3-Bromophenyl)triphenylsilane manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
(3-Bromophenyl)triphenylsilane 185626-73-7
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-09-27
Hebei Chuanghai Biotechnology Co,.LTD
Product
(3-Bromophenyl) Triphenylsilane 185626-73-7
Price
US $11.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-21
Career Henan Chemical Co
Product
3-bromophenyltriphenylsilyl chloride 185626-73-7
Price
US $8.80/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
100kg
Release date
2019-07-09

185626-73-7, (3-Bromophenyl)triphenylsilaneRelated Search:

Chlorotrimethylsilane TRIMETHYLSILANE

  • (3-Bromophenyl)triphenylsilane
  • Silane, (3-bromophenyl)triphenyl-
  • 3-bromophenyltriphenylsilyl chloride
  • 1-bromo-3-(triphenylsilyl)-Benzene
  • Benzene, 1-bromo-3-(triphenylsilyl)-
  • 3-Bromotetraphenylsilane
  • (3-Bromophenyl)triphenylsilane - [B89405]
  • (3-Bromopheny|) tripheny|si|ane
  • 185626-73-7