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GENTIOBIOSE

Product Name
GENTIOBIOSE
CAS No.
554-91-6
Chemical Name
GENTIOBIOSE
Synonyms
BETA-GENTIOBIOSE;AMYGDALOSE;GENTIOBIOSE;GENTIOBIOSE β;Gentiobiose>BETA-GENTOBIOSE;B-D-GENTIOBIOSE;Gentiobiose,97%;BETA-D-GENTIOBIOSE;β-Gentiobiose, 99%+
CBNumber
CB0315621
Molecular Formula
C12H22O11
Formula Weight
342.3
MOL File
554-91-6.mol
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GENTIOBIOSE Property

Melting point:
195-197 °C (dec.)
Boiling point:
397.76°C (rough estimate)
Density 
1.4149 (rough estimate)
refractive index 
9.5 ° (C=4, H2O)
storage temp. 
Sealed in dry,2-8°C
solubility 
Water (Sparingly)
pka
12.45±0.20(Predicted)
form 
Powder
color 
White to Off-white
optical activity
Alpha type +21.4 → +8.7 Beta type -11 → +9.6
Water Solubility 
Slightly soluble in water.
Merck 
14,4396
BRN 
93354
CAS DataBase Reference
554-91-6(CAS DataBase Reference)
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Safety

WGK Germany 
3
3-10
HS Code 
29400090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
G3000
Product name
β-Gentiobiose
Purity
≥85% (remainder primarily α-anomer)
Packaging
1g
Price
$432
Updated
2024/03/01
Sigma-Aldrich
Product number
G3000
Product name
β-Gentiobiose
Purity
≥85% (remainder primarily α-anomer)
Packaging
5g
Price
$1120
Updated
2024/03/01
TCI Chemical
Product number
G0026
Product name
Gentiobiose
Purity
>96.0%(HPLC)
Packaging
100mg
Price
$113
Updated
2024/03/01
Alfa Aesar
Product number
J66750
Product name
beta-D-Gentiobiose, 98%
Packaging
100mg
Price
$41.65
Updated
2024/03/01
Alfa Aesar
Product number
J66750
Product name
beta-D-Gentiobiose, 98%
Packaging
1g
Price
$234.65
Updated
2024/03/01
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GENTIOBIOSE Chemical Properties,Usage,Production

Chemical Properties

white to off-white fine crystalline powder

Uses

A disaccharide composed of two units of D-glucose

Uses

Gentiobiose was used in binding assays to determine if coelomic cytolytic factor 1 (CCF-1) binds to β-1,3-glucans to stimulate the pro-PO-activating system.

Purification Methods

-Gentiobiose is best purified via the octaacetate which is recrystallised from MeOH, EtOH or better from methyl cellosolve by heating at 80o. The octaacetate (15g) is hydrolysed by suspending it in dry 0.05N NaOMe in MeOH (180mL) for 1hour with occasional shaking at room temperature. Dilute this with H2O to dissolve suspended matter, pass through Amberlite IR-120 and Duolite A-4 columns and the eluate is evaporated under reduced pressure to a syrup. Residual H2O is removed by repeated distillation with absolute EtOH under reduced pressure. The syrup is dissolved in methyl cellosolve (~40mL), filtered, nucleated and placed in an oven at 80o. The crystals are filtered off, washed with absolute EtOH (yield 6.7g, 89%), dried and have m 187-189o. Further recrystallisation from methyl cellosolve gives m 190o, and mutarotates from [] D 28 -1.5o (initial) to +10.6o (final, c 4, H2O). The -octaacetate has m 193o (crystallised from 95% EtOH) and has [] D 20 -5o (c 1.8, CHCl3). [Goldstein & Whelan Methods in Carbohydrate Chemistry I 313 1962, Academic Press, Beilstein 17/7 V 203.]

GENTIOBIOSE Preparation Products And Raw materials

Raw materials

Preparation Products

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GENTIOBIOSE Suppliers

Olix (Shanghai) Pharmaceutical Technology Co., Ltd
Tel
17316404525
Email
209533805@qq.com
Country
China
ProdList
9765
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
3B Pharmachem (Wuhan) International Co.,Ltd.
Tel
821-50328103-801 18930552037
Fax
86-21-50328109
Email
3bsc@sina.com
Country
China
ProdList
15839
Advantage
69
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44688
Advantage
61
Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18738
Advantage
57
Sinopharm Chemical Reagent Co,Ltd.
Tel
86-21-63210123
Fax
86-21-63290778 86-21-63218885
Email
sj_scrc@sinopharm.com
Country
China
ProdList
9815
Advantage
79
Hunan Hui Bai Shi Biotechnology Co., Ltd.
Tel
0731-85526065 13308475853
Email
ivy@hnhbsj.com
Country
China
ProdList
4554
Advantage
62
ShangHai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847 13636370518
Fax
021-55068248
Email
shyysw007@163.com
Country
China
ProdList
4940
Advantage
60
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View Lastest Price from GENTIOBIOSE manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
Gentiobiose 554-91-6
Price
US $0.00/G
Min. Order
10G
Purity
98%min
Supply Ability
30kg/month
Release date
2023-02-09
Hebei Weibang Biotechnology Co., Ltd
Product
GENTIOBIOSE 554-91-6
Price
US $9.90/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-12-04
Hebei Mojin Biotechnology Co., Ltd
Product
GENTIOBIOSE 554-91-6
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-08-23

554-91-6, GENTIOBIOSERelated Search:


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  • 554-91-6
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