TERT-BUTYLMALONONITRILE
- Product Name
- TERT-BUTYLMALONONITRILE
- CAS No.
- 4210-60-0
- Chemical Name
- TERT-BUTYLMALONONITRILE
- Synonyms
- NISTC4210600;RARECHEM AQ A3 0176;TERT-BUTYLMALONITRILE;TERT-BUTYLMALONONITRILE;2-tert-butylmalononitrile;tert-butylpropanedinitrile;tert-Butylmalononitrile >2-tert-butylpropanedinitrile;tert-Butylmalononitrile;Propanedinitrile, 2-(1,1-dimethylethyl)-
- CBNumber
- CB0371010
- Molecular Formula
- C7H10N2
- Formula Weight
- 122.17
- MOL File
- 4210-60-0.mol
TERT-BUTYLMALONONITRILE Property
- Melting point:
- 84 °C
- Boiling point:
- 80-85 °C(Press: 7 Torr)
- Density
- 0.930±0.06 g/cm3(Predicted)
- solubility
- soluble in Methanol
- form
- powder to crystaline
- color
- White to Orange to Green
- InChIKey
- TUJPHMQZSDKRSL-UHFFFAOYSA-N
- CAS DataBase Reference
- 4210-60-0
Safety
- Risk Statements
- 23/24/25
- Safety Statements
- 26-36/37/39
- RIDADR
- 3276
- HazardClass
- 6.1
- PackingGroup
- III
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B1584
- Product name
- tert-Butylmalononitrile
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $183
- Updated
- 2024/03/01
- Product number
- B1584
- Product name
- tert-Butylmalononitrile
- Purity
- >95.0%(GC)
- Packaging
- 25g
- Price
- $551
- Updated
- 2024/03/01
- Product number
- B789695
- Product name
- tert-Butylmalononitrile
- Packaging
- 250mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- B789695
- Product name
- tert-Butylmalononitrile
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 3137-1-0E
- Product name
- tert-Butylmalononitrile
- Purity
- 95%
- Packaging
- 1g
- Price
- $144
- Updated
- 2021/12/16
TERT-BUTYLMALONONITRILE Chemical Properties,Usage,Production
Uses
TERT-BUTYLMALONONITRILE can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
The reaction was carried out under nitrogen. To the solution of aluminum chloride (14.5 g, 100 mmol) in 40 mL of nitromethane was added malonodinitrile 26 (6.6 g, 100 mmol). The temperature of the reaction mixture was kept between -15 and -20 °C, and tert-butyl bromide (22 g, 160 mmol) was added over a period of 30-45 min. The reaction mixture was allowed to warm to 0-5 °C and was maintained at that temperature. The reaction was monitored by TLC; the eluent was 30% EA/hexane. More tert-butyl bromide was added to complete the reaction. The reaction was worked up after 15 h by addition of a saturated solution of sodium bicarbonate to neutralize the HBr produced. The reaction mixture was extracted with methylene chloride. The organic layer was dried over anhydrous sodium sulfate and concentrated over vacuum. The 27 obtained (8.5 g, 70% yield) can be used for the next step without purification. t-Butylmalonodinitrile 27, yield (8.5 g, 70%) 1H NMR (300 MHz, CDCl3): δ 3.42(s, H), 1.24 (s, 9H).
TERT-BUTYLMALONONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from TERT-BUTYLMALONONITRILE manufacturers
- Product
- TERT-BUTYLMALONONITRILE 4210-60-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons/month
- Release date
- 2020-01-08
- Product
- 2-(tert-butyl)malononitrile 4210-60-0
- Price
- US $0.00/ASSAYS
- Min. Order
- 10ASSAYS
- Purity
- 97
- Supply Ability
- 20
- Release date
- 2019-07-26