ChemicalBook > CAS DataBase List > N,N-Dicyclohexyl-2-benzothiazolsulfene amide

N,N-Dicyclohexyl-2-benzothiazolsulfene amide

Product Name
N,N-Dicyclohexyl-2-benzothiazolsulfene amide
CAS No.
4979-32-2
Chemical Name
N,N-Dicyclohexyl-2-benzothiazolsulfene amide
Synonyms
DCBS;m181;DZ(DCBS);soxinoldz;meramiddch;rhodifax30;vulkacitdz;meramid dchm;sulfenamiddc;AcceleratorDZ
CBNumber
CB0397038
Molecular Formula
C19H26N2S2
Formula Weight
346.55
MOL File
4979-32-2.mol
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N,N-Dicyclohexyl-2-benzothiazolsulfene amide Property

Melting point:
104℃
Boiling point:
230°C (rough estimate)
Density 
1.20
vapor pressure 
0Pa at 25℃
refractive index 
1.5800 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Acetone (Slightly), Acetonitrile (Slightly), DMSO (Slightly)
form 
Solid
pka
0.43±0.20(Predicted)
color 
Pale Yellow to Light Yellow
Water Solubility 
1.9μg/L at 25℃
LogP
5.95
CAS DataBase Reference
4979-32-2(CAS DataBase Reference)
EPA Substance Registry System
N,N-Dicyclohexyl-2-benzothiazolesulfenamide (4979-32-2)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H317May cause an allergic skin reaction

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P321Specific treatment (see … on this label).

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
D439458
Product name
N,N-Dicyclohexyl-2-benzothiazolsulfeneAmide
Packaging
250mg
Price
$45
Updated
2021/12/16
TRC
Product number
D439458
Product name
N,N-Dicyclohexyl-2-benzothiazolsulfeneAmide
Packaging
2.5g
Price
$110
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD44040
Product name
N,N-Dicyclohexyl-2-benzothiazolsulfene amide
Packaging
250g
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
099741
Product name
S-(Benzo[d]thiazol-2-yl)-N,N-dicyclohexyl-thiohydroxylamine
Purity
95+%
Packaging
1g
Price
$87
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD44040
Product name
N,N-Dicyclohexyl-2-benzothiazolsulfene amide
Packaging
500g
Price
$95
Updated
2021/12/16
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N,N-Dicyclohexyl-2-benzothiazolsulfene amide Chemical Properties,Usage,Production

Uses

N,N-Dicyclohexyl-2-benzothiazolesulfenamide is a compound with reproductive and developmental toxicity that can affect body weight gain, reproductive organ weight, and multiple reproductive and developmental indicators in rats.

Flammability and Explosibility

Not classified

Contact allergens

This substance is a rubber accelerator of the mercapto- benzothiazole-sulfenamide group.

Synthesis

149-30-4

101-83-7

4979-32-2

(1) Preparation of M-Na salt solution: mix 400g 2-mercaptobenzothiazole (MBT) with 360g 32wt% sodium hydroxide (NaOH) solution, stirring at 50 ℃ for 2 hours, to get the M-Na salt solution; Preparation of dicyclohexylamine hydrochloride solution: mix 567g of dicyclohexylamine with 376g of 31wt% industrial hydrochloric acid, add 567g of water, stirring at 35 ℃. The solution of dicyclohexylamine hydrochloride was obtained. (2) M-Na salt solution (flow rate of 69 mL/min), dicyclohexylamine hydrochloride solution (flow rate of 136 mL/min), toluene (flow rate of 130 mL/min) and sodium hypochlorite solution with 17% effective chlorine (flow rate of 49 mL/min) were continuously pumped into a microchannel reactor to carry out oxidation reaction. The reaction conditions were: residence time of 2 s, reaction temperature of 30°C, and four microchannel reactors in series were used, each with a volume of 3 mL and a total volume of 12.8 mL.(3) The reactor effluent material was collected, stirred and cooled to 5°C for crystallization. The crude product was washed sequentially twice each with 200 mL of isopropanol and 200 mL of water to obtain S-(benzo[d]thiazol-2-yl)-N,N-dicyclohexylmercaptoamine (DCBS) wet product. After drying, DCBS was obtained as a finished product with 96.2% yield (based on MBT content), 99.2 wt% purity, and a light yellow powder appearance. After recovery of isopropanol from continuous distillation effluent, the residual COD was 5900 ppm.

References

[1] Evaluation of reproductive and developmental toxicity of the rubber accelerator N,N-dicyclohexyl-2-benzothiazolesulfenamide in rats DOI:10.1111/j.1741-4520.2007.00161.x

N,N-Dicyclohexyl-2-benzothiazolsulfene amide Preparation Products And Raw materials

Raw materials

Preparation Products

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N,N-Dicyclohexyl-2-benzothiazolsulfene amide Suppliers

XiaoGan ShenYuan ChemPharm co,ltd
Tel
15527768836
Email
1791901229@qq.com
Country
China
ProdList
6950
Advantage
52
Hangzhou Yuhao Chemical Technology Co., Ltd
Tel
0571-82693216
Fax
+86-571-82880190
Email
info@yuhaochemical.com
Country
China
ProdList
6387
Advantage
52
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
Advantage
55
TargetMol Chemicals Inc.
Tel
021-021-33632979 15002134094
Fax
021-33632979
Email
marketing@targetmol.com
Country
China
ProdList
7783
Advantage
58
Shanghai Meishui Chemical Technology Co., Ltd
Tel
021-60549325 18616193163
Fax
021-33250306
Country
China
ProdList
4526
Advantage
56
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Hangzhou J&H Chemical Co., Ltd.
Tel
0571-87396432
Fax
0571-87396431
Email
sales@jhechem.com
Country
China
ProdList
14912
Advantage
59
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Guangdong wengjiang Chemical Reagent Co., Ltd.
Tel
0751-2886750 13927877953
Fax
0751-2886750
Email
3005811397@qq.com
Country
China
ProdList
13305
Advantage
58
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View Lastest Price from N,N-Dicyclohexyl-2-benzothiazolsulfene amide manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
N,N-Dicyclohexyl-2-benzothiazolsulfene amide 4979-32-2
Price
US $10.00-8.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-12-05
Hebei Zhuanglai Chemical Trading Co Ltd
Product
N, N-Dicyclohexyl-2-Benzothiazole Sulfenamide 4979-32-2
Price
US $99.00-45.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20ton
Release date
2024-12-11
Hebei Chuanghai Biotechnology Co., Ltd
Product
Rubber Accelerator DCBS 4979-32-2
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-11-04

4979-32-2, N,N-Dicyclohexyl-2-benzothiazolsulfene amideRelated Search:


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  • N,N-DICYCLOHEXYLBENZOTHIAZOLE-2-SULFENAMIDE(ACCELERATORDZ)
  • N,N-Dicyclohexyl-2-benzothiazyl sulfenamide
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  • Benzothiazolesulfenamide, N,N-dicyclohexyl-
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  • DZ(DCBS)
  • rhodifax30
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  • N,N-Dicyclohexyl-2-benzothiazolesulfonamide
  • N,N-dicyclohexy-2-benzothiazolesulphenamide
  • RUBBER ACCELERATOR DCBS(DZ)
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  • N,N-Dicyclohexylbenzothiazole-2-sulfenamide, DCBS
  • N,N-dicyclohexyl-1,3-benzothiazole-2-sulfonamide
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  • 4979-32-2
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  • C19H26N2O2S2
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