N,N-Dicyclohexyl-2-benzothiazolsulfene amide
- Product Name
- N,N-Dicyclohexyl-2-benzothiazolsulfene amide
- CAS No.
- 4979-32-2
- Chemical Name
- N,N-Dicyclohexyl-2-benzothiazolsulfene amide
- Synonyms
- DCBS;m181;DZ(DCBS);soxinoldz;meramiddch;rhodifax30;vulkacitdz;meramid dchm;sulfenamiddc;AcceleratorDZ
- CBNumber
- CB0397038
- Molecular Formula
- C19H26N2S2
- Formula Weight
- 346.55
- MOL File
- 4979-32-2.mol
N,N-Dicyclohexyl-2-benzothiazolsulfene amide Property
- Melting point:
- 104℃
- Boiling point:
- 230°C (rough estimate)
- Density
- 1.20
- vapor pressure
- 0Pa at 25℃
- refractive index
- 1.5800 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Acetone (Slightly), Acetonitrile (Slightly), DMSO (Slightly)
- form
- Solid
- pka
- 0.43±0.20(Predicted)
- color
- Pale Yellow to Light Yellow
- Water Solubility
- 1.9μg/L at 25℃
- LogP
- 5.95
- CAS DataBase Reference
- 4979-32-2(CAS DataBase Reference)
- EPA Substance Registry System
- N,N-Dicyclohexyl-2-benzothiazolesulfenamide (4979-32-2)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H317May cause an allergic skin reaction
H412Harmful to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P272Contaminated work clothing should not be allowed out of the workplace.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P321Specific treatment (see … on this label).
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- D439458
- Product name
- N,N-Dicyclohexyl-2-benzothiazolsulfeneAmide
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D439458
- Product name
- N,N-Dicyclohexyl-2-benzothiazolsulfeneAmide
- Packaging
- 2.5g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- FD44040
- Product name
- N,N-Dicyclohexyl-2-benzothiazolsulfene amide
- Packaging
- 250g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 099741
- Product name
- S-(Benzo[d]thiazol-2-yl)-N,N-dicyclohexyl-thiohydroxylamine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $87
- Updated
- 2021/12/16
- Product number
- FD44040
- Product name
- N,N-Dicyclohexyl-2-benzothiazolsulfene amide
- Packaging
- 500g
- Price
- $95
- Updated
- 2021/12/16
N,N-Dicyclohexyl-2-benzothiazolsulfene amide Chemical Properties,Usage,Production
Uses
N,N-Dicyclohexyl-2-benzothiazolesulfenamide is a compound with reproductive and developmental toxicity that can affect body weight gain, reproductive organ weight, and multiple reproductive and developmental indicators in rats.
Flammability and Explosibility
Not classified
Contact allergens
This substance is a rubber accelerator of the mercapto- benzothiazole-sulfenamide group.
Synthesis
149-30-4
101-83-7
4979-32-2
(1) Preparation of M-Na salt solution: mix 400g 2-mercaptobenzothiazole (MBT) with 360g 32wt% sodium hydroxide (NaOH) solution, stirring at 50 ℃ for 2 hours, to get the M-Na salt solution; Preparation of dicyclohexylamine hydrochloride solution: mix 567g of dicyclohexylamine with 376g of 31wt% industrial hydrochloric acid, add 567g of water, stirring at 35 ℃. The solution of dicyclohexylamine hydrochloride was obtained. (2) M-Na salt solution (flow rate of 69 mL/min), dicyclohexylamine hydrochloride solution (flow rate of 136 mL/min), toluene (flow rate of 130 mL/min) and sodium hypochlorite solution with 17% effective chlorine (flow rate of 49 mL/min) were continuously pumped into a microchannel reactor to carry out oxidation reaction. The reaction conditions were: residence time of 2 s, reaction temperature of 30°C, and four microchannel reactors in series were used, each with a volume of 3 mL and a total volume of 12.8 mL.(3) The reactor effluent material was collected, stirred and cooled to 5°C for crystallization. The crude product was washed sequentially twice each with 200 mL of isopropanol and 200 mL of water to obtain S-(benzo[d]thiazol-2-yl)-N,N-dicyclohexylmercaptoamine (DCBS) wet product. After drying, DCBS was obtained as a finished product with 96.2% yield (based on MBT content), 99.2 wt% purity, and a light yellow powder appearance. After recovery of isopropanol from continuous distillation effluent, the residual COD was 5900 ppm.
References
[1] Evaluation of reproductive and developmental toxicity of the rubber accelerator N,N-dicyclohexyl-2-benzothiazolesulfenamide in rats DOI:10.1111/j.1741-4520.2007.00161.x
N,N-Dicyclohexyl-2-benzothiazolsulfene amide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N,N-Dicyclohexyl-2-benzothiazolsulfene amide manufacturers
- Product
- N,N-Dicyclohexyl-2-benzothiazolsulfene amide 4979-32-2
- Price
- US $10.00-8.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-12-05
- Product
- N, N-Dicyclohexyl-2-Benzothiazole Sulfenamide 4979-32-2
- Price
- US $99.00-45.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20ton
- Release date
- 2024-12-11
- Product
- Rubber Accelerator DCBS 4979-32-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-11-04