ChemicalBook > CAS DataBase List > 2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID

2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID

Product Name: 2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID
CAS No.: 874784-14-2
Chemical Name: 2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID
Synonyms: BUTTPARK 51\07-22;2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID;2-amino-3-fluoro-5-bromobenzoic acid;Benzoic acid, 2-amino-5-bromo-3-fluoro-
CBNumber: CB0441939
Molecular Formula: C7H5BrFNO2
Formula Weight: 234.02
MOL File: Mol file

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2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID Property

Boiling point:: 321.7±42.0 °C(Predicted)
Density: 1.877±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.21±0.10(Predicted)
form: very claggy powder
color: Off white to faint cream/beige
InChI: InChI=1S/C7H5BrFNO2/c8-3-1-4(7(11)12)6(10)5(9)2-3/h1-2H,10H2,(H,11,12)
InChIKey: CLJZODGTJUYULK-UHFFFAOYSA-N
SMILES: C(O)(=O)C1=CC(Br)=CC(F)=C1N

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Safety

HS Code: 2916310090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC501399
Product name: 2-Amino-5-bromo-3-fluorobenzoicacid
Packaging: 250mg
Price: $73
Updated: 2021/12/16

Apolloscientific

Product number: PC501399
Product name: 2-Amino-5-bromo-3-fluorobenzoicacid
Packaging: 1g
Price: $145
Updated: 2021/12/16

AK Scientific

Product number: J50322
Product name: 2-Amino-5-bromo-3-fluorobenzoicacid
Packaging: 1g
Price: $150
Updated: 2021/12/16

Apolloscientific

Product number: PC501399
Product name: 2-Amino-5-bromo-3-fluorobenzoicacid
Packaging: 5g
Price: $348
Updated: 2021/12/16

Ambeed

Product number: A131821
Product name: 2-Amino-5-bromo-3-fluorobenzoicacid
Purity: 97%
Packaging: 250mg
Price: $16
Updated: 2021/12/16

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2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

825-22-9

874784-14-2

Step 1: 2-Amino-3-fluorobenzoic acid (1.0 g, 6.45 mmol) was dissolved in N,N-dimethylformamide (DMF, 10 mL) at -10 °C. Subsequently, a solution of N-bromosuccinimide (NBS, 1.15 g, 6.45 mmol) in DMF (4 mL) was added dropwise to the above solution over 10 min. After the dropwise addition was completed, the reaction mixture was kept at -10°C and stirring was continued for 1 hour. Upon completion of the reaction, the reaction was quenched with aqueous sodium bisulfate (50 mL), at which point a large amount of solid precipitated. The solid product was collected by filtration and dried under vacuum to give 2-amino-5-bromo-3-fluorobenzoic acid (1.2 g, yield: 80%) as a yellow solid.

References

[1] Patent: WO2018/17490, 2018, A1. Location in patent: Paragraph 0153; 0154
[2] Patent: WO2015/200534, A2. Location in patent: Paragraph 00535
[2] Patent: , 2015, . Location in patent: Paragraph 00535
[4] Patent: WO2017/158388, 2017, A1. Location in patent: Page/Page column 212
[5] Patent: WO2014/11900, 2014, A2. Location in patent: Page/Page column 77

2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID Suppliers

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874784-14-2, 2-AMINO-5-BROMO-3-FLUOROBENZOIC ACIDRelated Search:

BUTTPARK 51\07-22

2-AMINO-5-BROMO-3-FLUOROBENZOIC ACID

Benzoic acid, 2-amino-5-bromo-3-fluoro-

2-amino-3-fluoro-5-bromobenzoic acid

874784-14-2