ChemicalBook > CAS DataBase List > 3-benzyl-1-methyl-1H-indole
3-benzyl-1-methyl-1H-indole
Preparation- Product Name
- 3-benzyl-1-methyl-1H-indole
- CAS No.
- 24486-66-6
- Chemical Name
- 3-benzyl-1-methyl-1H-indole
- Synonyms
- 3-benzyl-1-methyl-1H-indole;1H-Indole, 1-methyl-3-(phenylmethyl)-
- CBNumber
- CB04798167
- Molecular Formula
- C16H15N
- Formula Weight
- 221.3
- MOL File
- 24486-66-6.mol
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3-benzyl-1-methyl-1H-indole Property
- Melting point:
- 61 °C
- Boiling point:
- 374.7±11.0 °C(Predicted)
- Density
- 1.03±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
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3-benzyl-1-methyl-1H-indole Chemical Properties,Usage,Production
Preparation
3-benzyl-1-methyl-1H-indole is prepared by the following steps:To a solution of oxindole 40 (1.0 g, 4.22 mol) in THF, BMS complex was added dropwise at room temperature. The reaction mixture was stirred for 30 minutes. Then the reaction mixture was washed with brine, dried over anhydrous Na2SO4 and filtered. Solvent was evaporated under reduced pressure. Column chromatographic purification over neutral alumina using EtOAc-pet ether (1:9) gave indole 41 (0.653 g).Yield : 70%
Synthesis Reference(s)
Journal of the American Chemical Society, 73, p. 970, 1951 DOI: 10.1021/ja01147a024
3-benzyl-1-methyl-1H-indole Preparation Products And Raw materials
Raw materials
Preparation Products
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