ChemicalBook > CAS DataBase List > 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE

5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE

Product Name: 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE
CAS No.: 90145-48-5
Chemical Name: 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE
Synonyms: 2-Pyridinecarboxamide,5-bromo;5-Bromopyridine-2-carboxamide 97%;5-Bromo-pyridine-2-carboxylic acid amide;5-Bromopicolinamide, 5-Bromo-2-carbamoylpyridine;5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE;5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE ISO 9001：2015 REACH
CBNumber: CB0500489
Molecular Formula: C6H5BrN2O
Formula Weight: 201.02
MOL File: 90145-48-5.mol

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5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE Property

Melting point:: 218-220
Boiling point:: 329.1±27.0 °C(Predicted)
Density: 1.710±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 14.79±0.50(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C6H5BrN2O/c7-4-1-2-5(6(8)10)9-3-4/h1-3H,(H2,8,10)
InChIKey: IPWPEOLXILHOLV-UHFFFAOYSA-N
SMILES: C1(C(N)=O)=NC=C(Br)C=C1

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Safety

Hazard Codes: Xi
Hazard Note: Irritant/Keep Cold
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B686613
Product name: 5-Bromopicolinamide
Packaging: 500mg
Price: $85
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-9-V4
Product name: 5-Bromopyridine-2-carboxamide
Purity: 97.0%
Packaging: 250mg
Price: $31
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB153951
Product name: 5-Bromopicolinamide
Packaging: 500mg
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-9-V4
Product name: 5-Bromopyridine-2-carboxamide
Purity: 97.0%
Packaging: 1g
Price: $68
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB153951
Product name: 5-Bromopicolinamide
Packaging: 2g
Price: $166
Updated: 2021/12/16

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5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE Chemical Properties,Usage,Production

Synthesis

30766-11-1

90145-48-5

GENERAL PROCEDURE: To a solution of 2-carboxylic acid-5-bromopyridine (200 mg, 1 mmol) in dichloromethane (5 mL) was slowly added thionyl chloride (1 mL) dropwise and a drop of N,N-dimethylformamide (DMF). The reaction mixture was heated to 80 °C and maintained for 1 hour. Upon completion of the reaction, it was cooled to room temperature, the reaction mixture was concentrated and the residue was dissolved in dichloromethane (2 mL). The resulting solution was slowly added dropwise to ammonia (3 mL) at room temperature. Subsequently, the mixture was stirred at room temperature for 1.5 hours. At the end of the reaction, the mixture was concentrated to give 5-bromopyridinecarboxamide (85 mg, 92.4% yield) as a white solid. Liquid mass spectrometry (electrospray ionization) m/z ([M+H]+) measured value 201.2; calculated value 201.0.

References

[1] Patent: WO2014/81619, 2014, A1. Location in patent: Page/Page column 46
[2] Journal of Medicinal Chemistry, 2018, vol. 61, # 11, p. 4860 - 4882
[3] Patent: US2006/217387, 2006, A1. Location in patent: Page/Page column 31
[4] Patent: WO2012/76063, 2012, A1. Location in patent: Page/Page column 39
[5] Patent: US2013/261100, 2013, A1. Location in patent: Paragraph 0279-0280

5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE Suppliers

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View Lastest Price from 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE manufacturers

Dideu Industries Group Limited

Product: 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE 90145-48-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-23

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE 90145-48-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE 90145-48-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

90145-48-5, 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDERelated Search:

N-Ethyl 5-bromopicolinamide (5-Bromopicolinoyl)piperidine, (5-Bromopyridin-2-yl)(piperidin-1-yl)methanone 5-BROMO-PYRIDINE-2-CARBOXYLIC ACID DIMETHYLAMIDE 5-Bromo-N-propylpicolinamide 5-Bromo-N-isopropylpicolinamide 5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE N-Methyl 5-bromopicolinamide 5-Bromo-N-cyclopropylpyridine-2-carboxamide 6-Bromopyridine-2-carboxamide 98% 5-Bromo-N-cyclopentylpicolinamide PYRIDINE-2-CARBOXAMIDE 5-Bromo-N-(4-methoxybenzyl)picolinamide 5-BROMO-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE N-benzyl 5-bromopyridine-2-carboxamide 3,5-DIBROMO-PYRIDINE-2-CARBOXYLIC ACID AMIDE 6-AMINO-5-BROMO-3-FLUOROPYRIDINE-2-CARBOXAMIDE 6-AMINO-5-BROMOPYRIDINE-2-CARBOXAMIDE 6-AMINO-5-BROMO-3-METHYLPYRIDINE-2-CARBOXAMIDE

5-Bromo-pyridine-2-carboxylic acid amide

2-Pyridinecarboxamide,5-bromo

5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE

5-Bromopyridine-2-carboxamide 97%

5-Bromopicolinamide, 5-Bromo-2-carbamoylpyridine

5-BROMOPYRIDINE-2-CARBOXAMIDE 97%5-BROMOPICOLINAMIDE ISO 9001：2015 REACH

90145-48-5

blocks

Bromides

Carboxes

Pyridines