ChemicalBook > CAS DataBase List > 2,3-Dichloro-5-(trichloromethyl)pyridine

2,3-Dichloro-5-(trichloromethyl)pyridine

Product Name
2,3-Dichloro-5-(trichloromethyl)pyridine
CAS No.
69045-83-6
Chemical Name
2,3-Dichloro-5-(trichloromethyl)pyridine
Synonyms
2,3-Dichloro-5-(trichloromethyl)pyridine;2 3-DICHLORO-5-(TRICHLOROMETHYL)PYRIDIN&;Pyridine,2,3-dichloro-5-(trichloromethyl)-;69045-83-6 2,3-Dichloro-5-(trichloromethyl)pyridine;2,3-Dichloro-5-(trichloromethyl)pyridine ISO 9001：2015 REACH
CBNumber
CB0504856
Molecular Formula
C6H2Cl5N
Formula Weight
265.35
MOL File
69045-83-6.mol
More
Less

2,3-Dichloro-5-(trichloromethyl)pyridine Property

Boiling point:
278-279 °C(lit.)
Density 
1.636 g/mL at 25 °C(lit.)
refractive index 
n20/D 1.5900(lit.)
Flash point:
150 °F
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-3.03±0.10(Predicted)
InChI
InChI=1S/C6H2Cl5N/c7-4-1-3(6(9,10)11)2-12-5(4)8/h1-2H
InChIKey
XVBWGQSXLITICX-UHFFFAOYSA-N
SMILES
C1(Cl)=NC=C(C(Cl)(Cl)Cl)C=C1Cl
EPA Substance Registry System
2,3-Dichloro-5-(trichloromethyl)pyridine (69045-83-6)
More
Less

Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HS Code 
2933399990
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

More
Less

N-Bromosuccinimide Price

Matrix Scientific
Product number
098266
Product name
2,3-Dichloro-5-(trichloromethyl)pyridine
Purity
95+%
Packaging
1g
Price
$125
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-5-BP
Product name
2,3-Dichloro-5-(trichloromethyl)pyridine
Packaging
1g
Price
$208
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD149562
Product name
2,3-Dichloro-5-(trichloromethyl)pyridine
Packaging
2g
Price
$242
Updated
2021/12/16
Matrix Scientific
Product number
098266
Product name
2,3-Dichloro-5-(trichloromethyl)pyridine
Purity
95+%
Packaging
5g
Price
$360
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD149562
Product name
2,3-Dichloro-5-(trichloromethyl)pyridine
Packaging
500mg
Price
$80
Updated
2021/12/16
More
Less

2,3-Dichloro-5-(trichloromethyl)pyridine Chemical Properties,Usage,Production

Uses

2,3-dichloro-5-(trifluoromethyl)pyridine (DCTF) is an important organic intermediate for the agrochemical industry in particular for use in the synthesis of fluazinam and fluopicolide as well as other pesticidal active pyridine compounds.

Synthesis

Conversion of Nicotinic acid to 2,3-dichloro-5-(trichloromethyl)pyridine. Nicotinic acid (2 g, 16.25 mmole) and phosphorous pentachloride (27 g, 130 mmole) was mixed in a 50 ml Teflon autoclave. The autoclave was closed and heated in a 180 °C warm metal block. After 48 hours was the autoclave cooled to 25 °C and opened. The resulting suspension was quenched in a mixture of NaOH (10 %) and dichlorom ethane under stirring, keeping the temperature below 30 °C. The phases were separated and the organic phase was evaporated to dryness to get the crude product. The product was hereafter distilled and 2,8 g of 2,3-dichloro-5-(trichloromethyl)pyridine was obtained (65% yield).

References

[1] Patent: CN106748985, 2017, A. Location in patent: Paragraph 0030; 0032; 0033; 0035
[2] Patent: CN107935920, 2018, A. Location in patent: Paragraph 0026; 0031; 0034

2,3-Dichloro-5-(trichloromethyl)pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

2,3-Dichloro-5-(trifluoromethyl)pyridine
More
Less

2,3-Dichloro-5-(trichloromethyl)pyridine Suppliers

China 83 India 1 Slovakia 1 Switzerland 1 United Kingdom 6 United States 9 Global 101
JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
Country
China
ProdList
9976
Advantage
60
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
ZHEJIANG ZETIAN FINE CHEMICALS CO.,LTD
Tel
0571-87322520 18957127338
Fax
QQ:3007632051
Email
sales@zetchem.com
Country
China
ProdList
467
Advantage
55
Shanghai Synchem Pharma Co., ltd
Tel
21-619849051-1 18521059765
Email
synchempharma@aliyun.com
Country
China
ProdList
6468
Advantage
55
JW & Y Pharmlab Co., Ltd.
Tel
021-64340559 13651849907;
Fax
021- 64345308
Email
xinyu_shi@jwypharmlab.com.cn
Country
China
ProdList
12000
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Nanijing m&m biotechnology Co. ,Ltd.
Tel
025-87782433 18021532344
Fax
025-87782433
Email
1345332203@qq.com
Country
China
ProdList
4135
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-（0）57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Aikon International Limited
Tel
025-58859352 18068836627
Fax
(5)02557626880
Email
dt3@aikonchem.com
Country
China
ProdList
15493
Advantage
58
Hubei Xinyuanshun Pharmaceutical Chemical Co., Ltd.
Tel
027-51831887 15337167856
Fax
027-51837635 QQ1165326703
Email
hubeixinyuanshun@163.com
Country
China
ProdList
10295
Advantage
58
Shandong utilizing biological technology co., LTD
Tel
15966937598
Fax
3407640895 3071519937
Email
3407650895@qq.com
Country
China
ProdList
2274
Advantage
58
Zhengzhou Acme Chemical Co., Ltd.
Tel
0371-63315541 13323832564
Fax
QQ:3001332135
Email
3001332135@qq.com
Country
China
ProdList
9972
Advantage
58
Guangdong wengjiang Chemical Reagent Co., Ltd.
Tel
0751-2815688 13927872512
Fax
0751-8963795
Email
3007421951@qq.com
Country
China
ProdList
9939
Advantage
58
Shanghai zhigan biotechnology co., LTD
Tel
Email
zhiqianbio@126.com
Country
China
ProdList
19778
Advantage
58
Shanghai changwei industrial development co., LTD
Tel
13262956501
Email
cli@sunwayshanghai.com
Country
China
ProdList
298
Advantage
58
Henan Alpha Chemical Co., Ltd.
Tel
0371-55055611 18137792234
Fax
QQ：3002694073
Email
3002694073@qq.com
Country
China
ProdList
9987
Advantage
58
Henan Alfa Chemical Co., Ltd
Tel
+8615838112936
Email
alfa10@alfachem.cn
Country
China
ProdList
12921
Advantage
58
ANHUI WITOP BIOTECH CO., LTD
Tel
+8615255079626
Email
eric@witopchemical.com
Country
China
ProdList
23541
Advantage
58
Hefei TNJ Chemical Industry Co.,Ltd.
Tel
+86-0551-65418684 +8618949823763
Fax
0086-551-65418684
Email
sales@tnjchem.com
Country
China
ProdList
25356
Advantage
58
Dideu Industries Group Limited
Tel
+86-29-89586680 +86-15129568250
Email
1026@dideu.com
Country
China
ProdList
20284
Advantage
58
CD Chemical Group Limited
Tel
+8615986615575
Fax
0086-13651442114
Email
info@codchem.com
Country
China
ProdList
20342
Advantage
58
Dayang Chem (Hangzhou) Co.,Ltd.
Tel
+86-0571-88938639 +8617705817739
Fax
+86-571-88938652，+86-571- 88492614
Email
info@dycnchem.com
Country
China
ProdList
52846
Advantage
58
Longyan Tianhua Biological Technology Co., Ltd
Tel
0086 18039857276 18039857276
Country
CHINA
ProdList
2783
Advantage
58
SIMAGCHEM CORP
Tel
+86-5922680277 +86-13806087780
Email
sale@simagchem.com
Country
China
ProdList
17346
Advantage
58
Hebei Chuanghai Biotechnology Co., Ltd
Tel
+8615350571055
Fax
whatapp+8619930503282
Email
Sibel@chuanghaibio.com
Country
China
ProdList
8768
Advantage
58
Hubei xin bonus chemical co. LTD
Tel
86-13657291602
Fax
027-59338440
Email
linda@hubeijusheng.com
Country
CHINA
ProdList
22963
Advantage
58
Qi Qi hang Biotechnology Co., Ltd.
Tel
18151111370
Email
1046215251@qq.com
Country
China
ProdList
5999
Advantage
58
Shanghai Boyi Biomedical Technology Co., Ltd.
Tel
021-021-54331997 18321536537
Email
info@ansionpharma.com
Country
China
ProdList
2336
Advantage
58
Yangzhou modier Electronic Materials Co., Ltd
Tel
0514-82098883; 13761402923
Email
market@modeltemol.com
Country
China
ProdList
996
Advantage
58
CONIER CHEM AND PHARMA LIMITED
Tel
+8618523575427
Email
sales@conier.com
Country
China
ProdList
49975
Advantage
58
career henan chemical co
Tel
+86-0371-86658258 +8613203830695
Fax
0086-371-86658258
Email
factory@coreychem.com
Country
China
ProdList
29798
Advantage
58
Nanjing shengyilai Chemical Co., Ltd
Tel
19951936396
Email
3158688292@qq.com
Country
China
ProdList
4856
Advantage
58
Antai Fine Chemical Technology Co.,Limited
Tel
18503026267
Email
info@antaichem.com
Country
CHINA
ProdList
9636
Advantage
58
Hubei SVETO New Material Technology Co., Ltd
Tel
13277095679
Fax
027-65662438
Email
1375175909@qq.com
Country
China
ProdList
638
Advantage
58
Mainchem Co., Ltd.
Tel
--
Fax
--
Email
sarah@mainchem.com
Country
China
ProdList
6547
Advantage
58
Shanghai Sunway Pharmaceutical Technology Co.,Ltd.
Tel
021-51816796-820 13611835272
Fax
021-5161 3951
Email
sales2@sunwaypharm.com
Country
China
ProdList
44119
Advantage
58
Bide Pharmatech Ltd.
Tel
400-1647117 13681763483
Email
product02@bidepharm.com
Country
China
ProdList
59936
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39653
Advantage
58
Jiangsu Runfeng Synthetic Technology Co., Ltd.
Tel
0513-66017678 18551497631
Email
507167383@qq.com
Country
China
ProdList
4990
Advantage
58
Hebei Dueling International Trade Co. LTD
Tel
18032116176
Email
399549586@qq.com
Country
China
ProdList
1181
Advantage
58
Jiangsu Pules Bio-tech Co.,Ltd
Tel
0513-66017706 18551496367
Email
2186883463@qq.com
Country
China
ProdList
4999
Advantage
58
Jilin Chinese Academy of Sciences - Yanshen Technology Co., Ltd
Tel
0431-80514535 19917294565
Email
et@chemextension.com
Country
China
ProdList
5061
Advantage
58
Shaanxi Dideu Newmaterial Co., Ltd.
Tel
029-63373950 17392213970
Email
1052@dideu.com
Country
China
ProdList
9998
Advantage
58
Hubei chengfeng chemical co. LTD
Tel
15827338311
Email
1802085297@qq.com
Country
China
ProdList
4002
Advantage
58
Shanghai Haohong Scientific Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Hubei Chenghai Chemical Co., Ltd
Tel
027-59220433 18327245847
Email
1400838877@qq.com
Country
China
ProdList
9875
Advantage
58
Beijing Solarbio Science & Tecnology Co., Ltd.
Tel
010-50973130 17801761073
Email
Gsiyu@solarbio.com
Country
China
ProdList
50464
Advantage
58
Shanghai Jieshikai Biotechnology Co. , Ltd.
Tel
021-57520305 13795461237
Email
zhuruyan@jskchem.com
Country
China
ProdList
49234
Advantage
58
https://hanhongsci.com/
Tel
021-54306202 18917919676
Email
info@hanhongsci.com
Country
China
ProdList
29995
Advantage
58
Zhengzhou JACS Chemical Product Co., LTD
Tel
0371-86259281 13223061139
Email
893596907@qq.com
Country
China
ProdList
7993
Advantage
58
More
Less

View Lastest Price from 2,3-Dichloro-5-(trichloromethyl)pyridine manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2,3-Dichloro-5-(trichloromethyl)pyridine 69045-83-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-12-02
Dideu Industries Group Limited
Product
2,3-Dichloro-5-(trichloromethyl)pyridine 69045-83-6
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-27
Longyan Tianhua Biological Technology Co., Ltd
Product
2,3-Dichloro-5-(trichloromethyl)pyridine 69045-83-6
Price
US $14.00/Kg/Bag
Min. Order
10Kg/Bag
Purity
99%
Supply Ability
20 Tons
Release date
2020-10-28

69045-83-6, 2,3-Dichloro-5-(trichloromethyl)pyridineRelated Search:

2,3-Dichlorobenzotrifluoride ISOCYANIC ACID 3,6-DICHLORO-2-(TRICHLOROMETHYL)PYRIDINE 2,6-DICHLORO-3-(TRICHLOROMETHYL)PYRIDINE 2,3-Dichloro-6-(trichloromethyl)pyridine 2,4-Dichloro-6-(trichloromethyl)pyridine 3,5-dichloro-2-(trichloromethyl)pyridine 2,6-DICHLORO-4-(TRICHLOROMETHYL)PYRIDINE 2,4-Dimethoxy-3,5-dichloro-6-(trichloromethyl)pyridine 2,6-DICHLORO-3-(TRICHLOROMETHYL)PYRIDINE, TECH 2,5,6-TRICHLORO-3-TRIFLUOROMETHYLPYRIDINE N-[2,3,6-TRICHLORO-5-(TRIFLUOROMETHYL)PYRIDIN-4-YL]BENZENE-1,2-DIAMINE 2,3-Dichloro-5-(trichloromethyl)pyridine 2,3,6-TRICHLORO-4-[(4-METHYLPHENYL)THIO]-5-(TRIFLUOROMETHYL)PYRIDINE

  • 2 3-DICHLORO-5-(TRICHLOROMETHYL)PYRIDIN&
  • 2,3-Dichloro-5-(trichloromethyl)pyridine
  • Pyridine,2,3-dichloro-5-(trichloromethyl)-
  • 2,3-Dichloro-5-(trichloromethyl)pyridine ISO 9001：2015 REACH
  • 69045-83-6 2,3-Dichloro-5-(trichloromethyl)pyridine
  • 69045-83-6
  • C6H2NCl5
  • Pyridine series
  • blocks
  • FluoroCompounds
  • Pyridines