ChemicalBook > CAS DataBase List > N-Benzylhydroxylamine hydrochloride

N-Benzylhydroxylamine hydrochloride

Product Name: N-Benzylhydroxylamine hydrochloride
CAS No.: 29601-98-7
Chemical Name: N-Benzylhydroxylamine hydrochloride
Synonyms: Benzyl(hydroxy)ammonium chloride;N-Benzylhydroxylammonium chloride;N-BENZYLHYDROXYLAMINE HYDROCHLORIDE;N-Benzylhydroxylamine Hydrochloride >N-Benzylhydroxylamine hydrochloride 97%;N-Benzylhydroxylamine hydrochloride;N-hydroxy-BenzeneMethanaMine hydrochloride;Benzenemethanamine, N-hydroxy-, hydrochloride;N-Benzylhydroxylamine hydrochloride≥ 98%(HPLC);BenzeneMethanaMine,N-hydroxy-, hydrochloride (1:1)
CBNumber: CB0664646
Molecular Formula: C7H10ClNO
Formula Weight: 159.61
MOL File: 29601-98-7.mol

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N-Benzylhydroxylamine hydrochloride Property

Melting point:: 108-110 °C(lit.)
storage temp.: Inert atmosphere,Room Temperature
solubility: DMSO (Slightly), Ethyl Acetate (Slightly, Heated), Methanol (Slightly)
form: powder to crystal
color: White to Light yellow
BRN: 507948
InChI: InChI=1S/C7H9NO.ClH/c9-8-6-7-4-2-1-3-5-7;/h1-5,8-9H,6H2;1H
InChIKey: YSNXOQGDHGUKCZ-UHFFFAOYSA-N
SMILES: N(CC1=CC=CC=C1)O.[H]Cl
CAS DataBase Reference: 29601-98-7

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
WGK Germany: 3
F: 3-10
HS Code: 29280000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 13454
Product name: N-Benzylhydroxylamine hydrochloride
Purity: puriss., ≥99.0% (AT)
Packaging: 1g
Price: $43.61
Updated: 2025/07/31

Sigma-Aldrich

Product number: 13454
Product name: N-Benzylhydroxylamine hydrochloride
Purity: puriss., ≥99.0% (AT)
Packaging: 5G
Price: $95.5
Updated: 2025/07/31

TCI Chemical

Product number: B4073
Product name: N-Benzylhydroxylamine Hydrochloride
Purity: >98.0%(HPLC)(T)
Packaging: 5g
Price: $189
Updated: 2025/07/31

TCI Chemical

Product number: B4073
Product name: N-Benzylhydroxylamine Hydrochloride
Purity: >98.0%(HPLC)(T)
Packaging: 25g
Price: $670
Updated: 2025/07/31

Sigma-Aldrich

Product number: 365181
Product name: N-Benzylhydroxylamine hydrochloride
Purity: 97%
Packaging: 1g
Price: $64.4
Updated: 2023/06/20

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N-Benzylhydroxylamine hydrochloride Chemical Properties,Usage,Production

Chemical Properties

White crystalline

Uses

N-Benzylhydroxylamine hydrochloride may be used in the preparation of a precursor to hitherto unknown aminocyclopentitol derivative, hydroxy functionalised 4-exo-ethoxycarbonyl-3-oxa-2-azabicyclo[3.3.0]octane system.

General Description

N-Benzylhydroxylamine hydrochloride is a N-substituted-hydroxylamine. It participates in the ring opening of (2S,3R)-1,2-epoxy-4-penten-3-ol. Two-step synthesis of N-benzylhydroxylamine starting from dibenzylamine is reported.

Biochem/physiol Actions

N-Benzylhydroxylamine is a potential pharmacological agent in the prevention and progression of acrolein-induced damage to the retinal pigment epithelium.

Synthesis

3376-26-9

29601-98-7

The general procedure for the synthesis of N-benzylhydroxylamine hydrochloride from the compound (CAS:3376-26-9) was as follows: in a two-necked round-bottomed flask equipped with a stirrer, a mixture of dibenzylamine (1) (32.8 g, 0.17 mol), Na2WO4-2H2O (0.98 g, 3.33 mmol) and methanol (0.17 L) was cooled to -15 °C. A 30% aqueous solution of H2O2 (57 mL, 0.5 mol) was slowly added dropwise over about 1 h via a pressure equalizing dropping funnel. After the dropwise addition, the reaction mixture was stirred continuously at room temperature for 16 hours. Subsequently, the mixture was transferred to a 3 L beaker and crushed ice (1 kg) was added under vigorous stirring. The white precipitate formed was collected by filtration and washed several times with ice water (1 L) to completely remove the peroxide. The wet crude nitrone was dissolved in 20% aqueous HCl solution (0.33 L) and concentrated under reduced pressure at a water bath temperature of 70 °C. To remove trace water, the mixture was washed with toluene (3 x 33 mL) and subsequently concentrated under vacuum to dryness overnight. Finally, recrystallization was carried out using minimal amounts of hot methanol (30 mL) and ether (115 mL) to give a white crystalline pure product (19.3 g, 71% yield). The 1H and 13C NMR spectra of the product were in agreement with those reported in the literature; ESI-HRMS analysis resulted in a calculated value of 124.07 and a measured value of 124.0750 for C7H9NO(M + H)+.

References

[1] Synthetic Communications, 2005, vol. 35, # 18, p. 2445 - 2451
[2] Synthetic Communications, 2005, vol. 35, # 18, p. 2445 - 2451
[3] Journal of Organic Chemistry, 1983, vol. 48, # 9, p. 1444 - 1448
[4] Synthesis, 2009, # 18, p. 3174 - 3176
[5] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 17, p. 4969 - 4972

N-Benzylhydroxylamine hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N-Benzylhydroxylamine hydrochloride manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: N-Benzylhydroxylamine hydrochloride 29601-98-7
Price: US $49.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000 tons
Release date: 2025-09-05

Shaanxi Dideu New Materials Co. Ltd

Product: N-Benzylhydroxylamine hydrochloride 29601-98-7
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-02-20

Zhuozhou Wenxi import and Export Co., Ltd

Product: N-Benzylhydroxylamine hydrochloride 29601-98-7
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-26

29601-98-7, N-Benzylhydroxylamine hydrochlorideRelated Search:

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N-BENZYLHYDROXYLAMINE HYDROCHLORIDE

Benzenemethanamine, N-hydroxy-, hydrochloride

N-hydroxy-BenzeneMethanaMine hydrochloride

N-Benzylhydroxylamine hydrochloride 97%

BenzeneMethanaMine,N-hydroxy-, hydrochloride (1:1)

Benzyl(hydroxy)ammonium chloride

N-benzylhydroxylamine hydrochloride, N-benzyl-N-hydroxylamine hydrochloride, benzyl-hydroxylamine monohydrochloride, benzyl hydroxylamine hydrochloride, o-benzylhydroxyamine hydrochloride, O-benzylhydroxyamine HCl, N-hydroxy-1-phenylmethanamine hydrochloride

N-Benzylhydroxylamine hydrochloride≥ 98%(HPLC)

N-Benzylhydroxylamine Hydrochloride &gt

N-Benzylhydroxylammonium chloride

<i>N</i>-Benzylhydroxylamine hydrochloride

N-benzylhydroxylaminehydChemicalbookrochloride,N-benzyl-N-hydroxylaminehydrochloride,benzyl-hydroxylaminemonohydrochloride,benzylhydroxylaminehydrochloride,o-benzylhydroxyaminehydrochloride,O-benzylhydroxyamineHCl,N-hydroxy-1-phenylmethanaminehydrochloride

29601-98-7

C6H5CH2NHOHHCl

Hydroxylamines

Nitrogen Compounds

Organic Building Blocks

Building Blocks

Hydroxylamines

Nitrogen Compounds

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