BUTTPARK 148\01-24

Product Name: BUTTPARK 148\01-24
CAS No.: 154532-34-0
Chemical Name: BUTTPARK 148\01-24
Synonyms: BUTTPARK 148\01-24;3-TERT-BUTYL-BENZONITRILE;3-(1,1-Dimethylethyl)benzonitrile;Benzonitrile, 3-(1,1-dimethylethyl)-
CBNumber: CB0674861
Molecular Formula: C11H13N
Formula Weight: 159.23
MOL File: 154532-34-0.mol

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BUTTPARK 148\01-24 Property

Boiling point:: 238℃
Density: 0.95
Flash point:: 98℃
storage temp.: Sealed in dry,Room Temperature
form: liquid
color: Clear

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B813988
Product name: 3-tert-Butyl-benzonitrile
Packaging: 100mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: 4837AD
Product name: 3-tert-Butylbenzonitrile
Packaging: 10g
Price: $178
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3737-1-31
Product name: 3-tert-Butylbenzonitrile
Packaging: 1g
Price: $210
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0377834
Product name: 3-TERT-BUTYLBENZONITRILE
Purity: 95.00%
Packaging: 5MG
Price: $503.83
Updated: 2021/12/16

Matrix Scientific

Product number: 084935
Product name: 3-tert-Butylbenzonitrile
Purity: 97%
Packaging: 1g
Price: $341
Updated: 2021/12/16

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BUTTPARK 148\01-24 Chemical Properties,Usage,Production

Synthesis

557-21-1

201851-06-1

154532-34-0

Zinc cyanide (1.57 g, 13.40 mmol) was added to a solution of 3-tert-butylphenyl trifluoromethanesulfonate (1.5 g, 6.70 mmol) in N,N-dimethylformamide (DMF, 10 mL). The reaction mixture was heated to 120 °C and the reaction was stirred at this temperature for 4 hours. Upon completion of the reaction, the mixture was cooled to room temperature, diluted with ether (2500 mL) and subsequently washed twice with 2N ammonium hydroxide solution (50 mL x 2). The organic phase was separated, washed with saturated sodium chloride solution (20 mL), dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography with the eluent being hexane solution of 5% ethyl acetate to give 3-tert-butylbenzonitrile in 75% yield.

References

[1] Patent: WO2009/42694, 2009, A1. Location in patent: Page/Page column 91
[2] Patent: WO2006/74940, 2006, A2. Location in patent: Page/Page column 30
[3] Patent: US2008/132477, 2008, A1. Location in patent: Page/Page column 50

BUTTPARK 148\01-24 Preparation Products And Raw materials

Raw materials

Preparation Products

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BUTTPARK 148\01-24 Suppliers

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View Lastest Price from BUTTPARK 148\01-24 manufacturers

Career Henan Chemical Co

Product: BUTTPARK 148\01-24 154532-34-0
Price: US $1.00/KG
Min. Order: 1g
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-09

154532-34-0, BUTTPARK 148\01-24Related Search:

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BUTTPARK 148\01-24

3-TERT-BUTYL-BENZONITRILE

3-(1,1-Dimethylethyl)benzonitrile

Benzonitrile, 3-(1,1-dimethylethyl)-

154532-34-0