AMINO-(3-NITRO-PHENYL)-ACETIC ACID
- Product Name
- AMINO-(3-NITRO-PHENYL)-ACETIC ACID
- CAS No.
- 30077-08-8
- Chemical Name
- AMINO-(3-NITRO-PHENYL)-ACETIC ACID
- Synonyms
- 3-Nitrophenylglycine;RS-3-Nitrophenylglycine;DL-m-Nitrophenylglycine;m-Nitro-DL-phenylglycine;2-Amino-2-(3-nitrophenyl);a-Amino-3-nitrobenzeneacetic acid;AMINO-(3-NITRO-PHENYL)-ACETIC ACID;Benzeneacetic acid, α-amino-3-nitro-;Benzeneacetic acid, a-amino-3-nitro-;2-Amino-2-(3-nitrophenyl)acetic acid
- CBNumber
- CB0757885
- Molecular Formula
- C8H8N2O4
- Formula Weight
- 196.16
- MOL File
- 30077-08-8.mol
AMINO-(3-NITRO-PHENYL)-ACETIC ACID Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CHM0028384
- Product name
- AMINO-(3-NITRO-PHENYL)-ACETIC ACID
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1030.84
- Updated
- 2021/12/16
- Product number
- SC-59441
- Product name
- Amino-(3-nitro-phenyl)-acetic acid
- Purity
- 95
- Packaging
- 5g
- Price
- $1833
- Updated
- 2021/12/16
- Product number
- SC-59441
- Product name
- Amino-(3-nitro-phenyl)-acetic acid
- Purity
- 95
- Packaging
- 10g
- Price
- $2383
- Updated
- 2021/12/16
- Product number
- SC-59441
- Product name
- Amino-(3-nitro-phenyl)-acetic acid
- Purity
- 95
- Packaging
- 25g
- Price
- $3117
- Updated
- 2021/12/16
- Product number
- CD21008901
- Product name
- 2-Amino-2-(3-nitrophenyl)aceticacid
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $99
- Updated
- 2021/12/16
AMINO-(3-NITRO-PHENYL)-ACETIC ACID Chemical Properties,Usage,Production
Synthesis
2835-06-5
30077-08-8
General procedure for the synthesis of 2-amino-2-(3-nitrophenyl)acetic acid from 2-amino-2-phenylacetic acid: 2-amino-2-phenylacetic acid (33 mmol, 5 g) was cooled to 0 °C and slowly added to a mixture of concentrated sulfuric acid (98% w/w, 5 mL) and fuming nitric acid (90% w/w, 5 mL). The reaction mixture was stirred at 0 °C for 1 h, followed by continued stirring at room temperature for 30 min. Upon completion of the reaction, hydrolysis was carried out with cold water (60 mL). The pH of the reaction solution was adjusted to neutral by dropwise addition of 10 M ammonia. The resulting mixture was stirred at 4 °C for 10 h. 2-Amino-2-(3-nitrophenyl)acetic acid was isolated by filtration. The product was washed with cold water to give a yellow powdery solid. Yield: 64%. 1H-NMR (DMSO, 200 MHz): δ= 8.27 (s, 1H, H-4), 8.10 (d, J = 8.1 Hz, 1H, H-6), 7.83 (d, J = 7.9 Hz, 1H, H-8), 7.64 (t, J = 7.9 Hz, 1H, H-7), 4.51 (s, 1H, H-2). Elemental analysis: calculated values for C8H8N2O4: C, 48.98; H, 4.11; N, 14.28. measured values: C, 48.92; H, 4.19; N, 14.31.
References
[1] Medicinal Chemistry Research, 2017, vol. 26, # 5, p. 975 - 986
[2] Chemische Berichte, 1885, vol. 18, p. 1181
AMINO-(3-NITRO-PHENYL)-ACETIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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