6-NITRO-5-METHYL (1H)INDAZOLE

Product Name: 6-NITRO-5-METHYL (1H)INDAZOLE
CAS No.: 72521-00-7
Chemical Name: 6-NITRO-5-METHYL (1H)INDAZOLE
Synonyms: 5-Methyl-6-nitroindazole;5-methyl-6-nitro-1H-indazole;6-NITRO-5-METHYL (1H)INDAZOLE;1H-Indazole, 5-methyl-6-nitro-
CBNumber: CB0789747
Molecular Formula: C8H7N3O2
Formula Weight: 177.16
MOL File: 72521-00-7.mol

More

Less

6-NITRO-5-METHYL (1H)INDAZOLE Property

Boiling point:: 379.7±22.0 °C(Predicted)
Density: 1.437
storage temp.: Sealed in dry,Room Temperature
pka: 11.30±0.40(Predicted)
Appearance: Light yellow to yellow Solid
InChI: InChI=1S/C8H7N3O2/c1-5-2-6-4-9-10-7(6)3-8(5)11(12)13/h2-4H,1H3,(H,9,10)
InChIKey: AZWAXIMNWVYSMP-UHFFFAOYSA-N
SMILES: N1C2=C(C=C(C)C([N+]([O-])=O)=C2)C=N1

More

Less

Safety

HS Code: 2933998090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: M339443
Product name: 5-Methyl-6-nitro-1H-indazole
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR948085
Product name: 5-Methyl-6-nitro-1H-indazole
Purity: 95%
Packaging: 1g
Price: $115
Updated: 2021/12/16

AK Scientific

Product number: Y9920
Product name: 5-Methyl-6-nitro-1H-indazole
Packaging: 10g
Price: $197
Updated: 2021/12/16

Apolloscientific

Product number: OR948085
Product name: 5-Methyl-6-nitro-1H-indazole
Purity: 95%
Packaging: 5g
Price: $240
Updated: 2021/12/16

Apolloscientific

Product number: OR948085
Product name: 5-Methyl-6-nitro-1H-indazole
Purity: 95%
Packaging: 10g
Price: $385
Updated: 2021/12/16

More

Less

6-NITRO-5-METHYL (1H)INDAZOLE Chemical Properties,Usage,Production

Synthesis

2124-47-2

72521-00-7

The general procedure for the synthesis of 5-methyl-6-nitroindazole from 2,4-dimethyl-5-nitroaniline is as follows: 1. 2,4-dimethyl-5-nitroaniline (1.662 g, 10.00 mmol) was dissolved in glacial acetic acid (100 ml) and the mixture was cooled to 0°C. 2. Sodium nitrite solution (1 equiv, 690 mg dissolved in 2 ml of water) was slowly added while keeping the reaction temperature below 25 °C. 3. Stirring of the reaction mixture was continued for 3 hours, followed by filtration. 4. The filtrate was allowed to stand at room temperature for 3 days and then concentrated under reduced pressure. 5. The concentrated residue was diluted with water and the resulting mixture was vigorously stirred. 6. The solid product was collected by filtration, washed thoroughly with cold water and dried. 7. 7. Finally, the product was purified by fast chromatography (dichloromethane/methanol with an eluent ratio of 99:1) to give 1.030 g (58.1% yield) of 5-methyl-6-nitro-1H-indazole in solid form.

References

[1] Bioorganic and Medicinal Chemistry, 2016, vol. 24, # 3, p. 403 - 427
[2] Patent: US2010/160373, 2010, A1. Location in patent: Page/Page column 28-29
[3] Patent: US2011/71143, 2011, A1. Location in patent: Page/Page column 37
[4] Journal of Medicinal Chemistry, 2015, vol. 58, # 21, p. 8413 - 8426
[5] Patent: WO2007/95124, 2007, A2. Location in patent: Page/Page column 89-90

6-NITRO-5-METHYL (1H)INDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

6-NITRO-5-METHYL (1H)INDAZOLE Suppliers

China 79 India 1 Switzerland 1 United States 6 Global 87

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Wuhan TCASChem Technology Co., Ltd.

Tel: 027-86697669 13986148687
Fax: 86-027-86697669
Email: sales@tcaschem.com
Country: China
ProdList: 3991
Advantage: 55

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

Shanghai Devinchem Ltd

Tel: 027-65318838 13646286950
Email: sales@devinchem.com
Country: China
ProdList: 2953
Advantage: 58

Shanghai ChriChem Co., Ltd.

Tel: 021-54880687
Fax: 021-54880687
Country: China
ProdList: 511
Advantage: 55

Taizhou Tongxin Bio-Tech Co., Ltd

Tel: 0523-86818997 18652728585
Email: sales@allyrise.com
Country: China
ProdList: 2966
Advantage: 60

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Hangzhou J&H Chemical Co., Ltd.

Tel: 0571-87396432
Fax: 0571-87396431
Email: sales@jhechem.com
Country: China
ProdList: 14912
Advantage: 59

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

More

Less

View Lastest Price from 6-NITRO-5-METHYL (1H)INDAZOLE manufacturers

Career Henan Chemical Co

Product: 6-NITRO-5-METHYL (1H)INDAZOLE 72521-00-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-11

72521-00-7, 6-NITRO-5-METHYL (1H)INDAZOLERelated Search:

1H-Indazole,6-chloro-4-iodo- 7-Methyl-6-nitro-1H-indazole 6-BROMO-1H-INDAZOLE-3-CARBALDEHYDE 6-(TRIFLUOROMETHYL)-4-BROMO INDAZOLE 6-BROMO-5-METHYL (1H)INDAZOLE 6-bromo-5-fluoro-1H-indazole 5-Iodo-1H-indazole 4-BROMO-6-CHLORO-1H-INDAZOLE 1H-Indazol-5-ol,6-broMo- 6-Nitroindazole 5-METHYL-1H-INDAZOLE 6-NITRO-5-METHYL (1H)INDAZOLE 3-IODO-5-METHYL-6-NITRO-1H-INDAZOLE 6-AMINO-5-METHYLINDOLE

6-NITRO-5-METHYL (1H)INDAZOLE

5-methyl-6-nitro-1H-indazole

5-Methyl-6-nitroindazole

1H-Indazole, 5-methyl-6-nitro-

72521-00-7