N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE

Product Name: N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE
CAS No.: 68236-26-0
Chemical Name: N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE
Synonyms: N-(5-Bromothiophen-2-yl);2-AcetaMido-5-broMothiophene;N-(5-bromo-2-thienyl)Acetamide;Acetamide, N-(5-bromo-2-thienyl)-;N-(5-BroMothiophen-2-yl)acetaMide;N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE;N-(5-BROMO-THIOPHENE-2-YL)-ACETAMIDE
CBNumber: CB0840327
Molecular Formula: C6H6BrNOS
Formula Weight: 220.09
MOL File: 68236-26-0.mol

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N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE Property

Melting point:: 135-136 °C
Boiling point:: 357.0±27.0 °C(Predicted)
Density: 1.717±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 14.02±0.70(Predicted)
Appearance: Light yellow to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B993955
Product name: N-(5-Bromothiophen-2-yl)acetamide
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142241
Product name: N-(5-Bromothiophen-2-yl)acetamide
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142241
Product name: N-(5-Bromothiophen-2-yl)acetamide
Packaging: 100mg
Price: $113
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142241
Product name: N-(5-Bromothiophen-2-yl)acetamide
Packaging: 250mg
Price: $225
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0187688
Product name: N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE
Purity: 95.00%
Packaging: 5MG
Price: $503.26
Updated: 2021/12/16

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N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE Chemical Properties,Usage,Production

Synthesis

98453-21-5

68236-26-0

General procedure for the synthesis of 2-acetamido-5-bromothiophene from the compound (CAS: 98453-21-5): to a solution of ketoxime (0.01 mol) in tetrahydrofuran (THF, 10 mL) was added tripropylphosphinic anhydride (T3P, 15 mol%, 50% dissolved in ethyl acetate (EtOAc)), and the reaction mixture was heated under nitrogen protection at refluxed and stirred for 1-4 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the completion of the reaction, the solvent was evaporated under reduced pressure. The residue was diluted with distilled water (20 mL) and subsequently extracted with ethyl acetate (2 x 20 mL). The organic phases were combined and washed sequentially with saturated sodium bicarbonate (NaHCO3) solution (10 mL) and saturated sodium chloride (brine) solution. The organic phase was dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to afford the target product 2-acetamido-5-bromothiophene with high purity.

References

[1] Journal of Heterocyclic Chemistry, 1985, vol. 22, p. 301 - 304
[2] Tetrahedron Letters, 2011, vol. 52, # 10, p. 1074 - 1077
[3] Journal of Medicinal Chemistry, 2016, vol. 59, # 19, p. 8830 - 8847
[4] Synthesis, 2006, # 8, p. 1295 - 1300

N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE Suppliers

China 33 India 1 United Kingdom 2 United States 7 Global 43

Alchem Pharmtech,Inc.

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Fayeton Inc.

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View Lastest Price from N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE manufacturers

Career Henan Chemical Co

Product: N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE 68236-26-0
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2020-02-21

68236-26-0, N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDERelated Search:

Dibenzothiophene AKOS 93957 AKOS BBS-00000757 AKOS 92788 5-BROMO-2-(2-CHLORO-ACETYLAMINO)-4-PHENYL-THIOPHENE-3-CARBOXYLIC ACID ETHYL ESTER N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE BUTTPARK 85\16-21 AKOS BBS-00000761 AKOS 93827

N-(5-BROMO-THIOPHENE-2-YL)-ACETAMIDE

N-(2-BROMOTHIOPHEN-5-YL)-ACETAMIDE

2-AcetaMido-5-broMothiophene

N-(5-BroMothiophen-2-yl)acetaMide

N-(5-bromo-2-thienyl)Acetamide

N-(5-Bromothiophen-2-yl)

Acetamide, N-(5-bromo-2-thienyl)-

68236-26-0

C6H6BrNOS