2-(CHLOROMETHYL)-6-METHYLPYRIDINE
- Product Name
- 2-(CHLOROMETHYL)-6-METHYLPYRIDINE
- CAS No.
- 3099-29-4
- Chemical Name
- 2-(CHLOROMETHYL)-6-METHYLPYRIDINE
- Synonyms
- EOS-62430;2-Chloromethyl-6-methylpyridine;2-(Chloromethyl)-6-methylpyridin;Pyridine, 2-(chloromethyl)-6-methyl-;2-(chloromethyl)-6-methylpyridine(SALTDATA: HCl);2-(CHLOROMETHYL)-6-METHYLPYRIDINE ISO 9001:2015 REACH
- CBNumber
- CB0955607
- Molecular Formula
- C7H8ClN
- Formula Weight
- 141.6
- MOL File
- 3099-29-4.mol
2-(CHLOROMETHYL)-6-METHYLPYRIDINE Property
- Melting point:
- 159-161 °C
- Boiling point:
- 118-120 °C(Press: 65 Torr)
- Density
- 1.118±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 4.43±0.12(Predicted)
- Appearance
- Light brown to brown Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CBR01903
- Product name
- 2-(Chloromethyl)-6-methylpyridine
- Purity
- Aldrich<SUP>CPR</SUP>
- Packaging
- 1 g
- Price
- $179
- Updated
- 2025/07/31
- Product number
- C381723
- Product name
- 2-(Chloromethyl)-6-methylpyridine
- Packaging
- 1g
- Price
- $330
- Updated
- 2021/12/16
- Product number
- FC148709
- Product name
- 2-(Chloromethyl)-6-methylpyridine
- Packaging
- 250mg
- Price
- $367.5
- Updated
- 2021/12/16
- Product number
- FC148709
- Product name
- 2-(Chloromethyl)-6-methylpyridine
- Packaging
- 100mg
- Price
- $184
- Updated
- 2021/12/16
- Product number
- OR450025
- Product name
- 2-(Chloromethyl)-6-methylpyridine
- Packaging
- 1g
- Price
- $53
- Updated
- 2021/12/16
2-(CHLOROMETHYL)-6-METHYLPYRIDINE Chemical Properties,Usage,Production
Synthesis
1122-71-0
3099-29-4
Preparation of Example 10-1-1 2-chloromethyl-6-methylpyridine: (6-methylpyridin-2-yl)methanol (1.44 g, 11.7 mmol) was dissolved in dichloromethane (20 mL) and thionyl chloride (1.45 mL, 19.9 mmol) was added. The reaction mixture was stirred under reflux conditions for 40 min. Upon completion of the reaction, the reaction solution was cooled to room temperature and subsequently concentrated under reduced pressure. The concentrated residue was partitioned between sodium bicarbonate solution and ether. The organic layer was separated and concentrated under reduced pressure, and the resulting residue was purified by silica gel column chromatography (eluent: ethyl acetate) to afford the target product 2-chloromethyl-6-methylpyridine (1.42 g, 85.8% yield).1H-NMR (DMSO-d6) δ (ppm): 2.47 (3H, s), 4.72 (2H, s), 7.22 (1H, d, J = 7.6 Hz), 7.33 (1H, d, J = 7.6 Hz), 7.72 (1H, dd, J = 7.6, 7.6 Hz).
References
[1] Journal of the American Chemical Society, 2005, vol. 127, # 29, p. 10197 - 10204
[2] Patent: US2009/82403, 2009, A1. Location in patent: Page/Page column 64
[3] Patent: US2007/105904, 2007, A1. Location in patent: Page/Page column 61
[4] Chinese Chemical Letters, 2018, vol. 29, # 11, p. 1637 - 1640
[5] Chemistry Letters, 1998, # 9, p. 915 - 916
2-(CHLOROMETHYL)-6-METHYLPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(CHLOROMETHYL)-6-METHYLPYRIDINE manufacturers
- Product
- 2-(CHLOROMETHYL)-6-METHYLPYRIDINE 3099-29-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-10
- Product
- 2-(CHLOROMETHYL)-6-METHYLPYRIDINE 3099-29-4
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-08-30
- Product
- 2-(CHLOROMETHYL)-6-METHYLPYRIDINE 3099-29-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-09