4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER
- Product Name
- 4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER
- CAS No.
- 3095-48-5
- Chemical Name
- 4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER
- Synonyms
- Methyl 4-aMino-3,5-diMethylbenzoate;4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER;Benzoic acid, 4-aMino-3,5-diMethyl-, Methyl ester;4-amino-3,5-dimethyl-Benzoic acid methyl ester (7CI 8CI 9CI ACI);Benzoic acid, 4-amino-3,5-dimethyl-, methyl ester (7CI, 8CI, 9CI, ACI)
- CBNumber
- CB11010580
- Molecular Formula
- C10H13NO2
- Formula Weight
- 179.22
- MOL File
- 3095-48-5.mol
4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER Property
- Melting point:
- 106-107℃
- Boiling point:
- 331.3±37.0 °C(Predicted)
- Density
- 1.105±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 2.17±0.10(Predicted)
- Appearance
- Light yellow to brown Solid
Safety
- HS Code
- 2922498590
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M331630
- Product name
- Methyl4-Amino-3,5-dimethylbenzoate
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FA42885
- Product name
- 4-Amino-3,5-dimethyl-benzoic acid methyl ester
- Packaging
- 500mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- FA42885
- Product name
- 4-Amino-3,5-dimethyl-benzoic acid methyl ester
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 4758-1-10
- Product name
- Methyl 4-amino-3,5-dimethylbenzoate
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 119777
- Product name
- Methyl 4-amino-3,5-dimethylbenzoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $136
- Updated
- 2021/12/16
4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
3277-04-1
3095-48-5
Scheme 5, Step B. To a solution of methyl 3,5-dimethyl-4-nitrobenzoate (10.0 g, 0.0478 mol) in methanol (100 mL) at 0°C was sequentially added iron powder (15.7 g, 0.2869 mol) and 37% hydrochloric acid (1.72 g, 0.0478 mol). The reaction mixture was heated to 80 °C and kept for 16 hours. After completion of the reaction, the mixture was cooled to room temperature, filtered through a Celite TM bed and the filter cake was washed with methanol. The filtrate was concentrated to dryness to afford methyl 4-amino-3,5-dimethylbenzoate as an unpurified solid (7.8 g, 99% yield). Mass spectrum (m/z): 180.2 (M + 1).
References
[1] Patent: US6342610, 2002, B2. Location in patent: Page column 125
[2] Patent: WO2014/4230, 2014, A1. Location in patent: Sheet 18; 19
[3] Patent: WO2015/94912, 2015, A1. Location in patent: Page/Page column 10
[4] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 1, p. 105 - 109
4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER manufacturers
- Product
- 4-amino-3,5-dimethyl-benzoic acid methyl ester 3095-48-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-30
- Product
- 4-AMINO-3,5-DIMETHYL-BENZOIC ACID METHYL ESTER 3095-48-5
- Price
- US $9.80-8.00/KG
- Min. Order
- 1KG
- Purity
- 95%~99.99%
- Supply Ability
- 10 MT/ Month
- Release date
- 2020-10-28
- Product
- 4-amino-3,5-dimethyl-benzoic acid methyl ester 3095-48-5
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10