3,6-Dibromo-phenanthrenequinone
- Product Name
- 3,6-Dibromo-phenanthrenequinone
- CAS No.
- 53348-05-3
- Chemical Name
- 3,6-Dibromo-phenanthrenequinone
- Synonyms
- 3,6-Dibromophenanthrene-9,10-dione;3,6-DibroMo-phenanthrenequ;6-Dibromo-phenanthrenequinone;3,6-Dibromo-9,10-phenanthrenedione;3,6-Dibromo-9,1-phenanthrenequinone;9,10-Phenanthrenedione, 3,6-dibromo-;3,6-Dibromo-9,10-phenanthrenequinone;3,6-Dibromo-9,10-dihydrophenanthrene-9,10-dione;3,6-Dibromo-phenanthrenequinone ISO 9001：2015 REACH
- CBNumber
- CB11012645
- Molecular Formula
- C14H6Br2O2
- Formula Weight
- 366
- MOL File
- 53348-05-3.mol
3,6-Dibromo-phenanthrenequinone Property
- Melting point:
- 291 °C
- Boiling point:
- 501.0±43.0 °C(Predicted)
- Density
- 1.911
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- Light yellow to Brown
- InChI
- InChI=1S/C14H6Br2O2/c15-7-1-3-9-11(5-7)12-6-8(16)2-4-10(12)14(18)13(9)17/h1-6H
- InChIKey
- WPEJBJRFPBMVGJ-UHFFFAOYSA-N
- SMILES
- C1=C2C(C3=C(C(=O)C2=O)C=CC(Br)=C3)=CC(Br)=C1
Safety
- HS Code
- 2914.79.9000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- D4692
- Product name
- 3,6-Dibromophenanthrene-9,10-dione
- Packaging
- 1G
- Price
- $144
- Updated
- 2025/07/31
- Product number
- D427985
- Product name
- 3,6-Dibromophenanthrene-9,10-dione
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- D427985
- Product name
- 3,6-Dibromophenanthrene-9,10-dione
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- J90758
- Product name
- 3,6-Dibromo-phenanthrenequinone
- Packaging
- 1g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- J90758
- Product name
- 3,6-Dibromo-phenanthrenequinone
- Packaging
- 5g
- Price
- $45
- Updated
- 2021/12/16
3,6-Dibromo-phenanthrenequinone Chemical Properties,Usage,Production
Uses
3,6-Dibromo-phenanthrenequinone is an organic compound containing a phenanthrenequinone skeleton, and its molecule contains two bromine atoms. Due to the presence of bromine atoms, 3,6-dibromophenanthrenequinone has a higher electron density and better reactivity, making it have a high application value in organic synthesis. In addition, it is widely used in the preparation of organic electronic devices, solar cells, and optoelectronic materials.
Synthesis
84-11-7
53348-05-3
The general procedure for the synthesis of 3,6-dibromo-9,10-phenanthrenequinone from 9,10-phenanthrenequinone was as follows: 9,10-phenanthrenequinone (50 g), benzoyl peroxide (2.5 g), and nitrobenzene (250 mL) were added to a nitrogen-displaced reaction vessel and aerated with nitrogen. Subsequently, bromine (83 g) was added and the mixture was heated to reflux and stirred for 2 hours. Upon completion of the reaction, the mixture was allowed to cool to room temperature and ethanol (250 mL) was added to precipitate the product. The precipitated solid was collected by filtration, washed with ethanol and finally dried under vacuum to give 3,6-dibromo-9,10-phenanthrenequinone as a yellow solid in 70% yield.
References
[1] Journal of the American Chemical Society, 2004, vol. 126, # 19, p. 6035 - 6042
[2] Journal of Materials Chemistry, 2012, vol. 22, # 10, p. 4383 - 4390
[3] Patent: WO2005/123754, 2005, A2. Location in patent: Page/Page column 50-51; Sheet 28
[4] Chemistry - A European Journal, 2014, vol. 20, # 32, p. 10170 - 10178
[5] Journal of the American Chemical Society, 2014, vol. 136, # 1, p. 427 - 435
3,6-Dibromo-phenanthrenequinone Preparation Products And Raw materials
Raw materials
Preparation Products
3,6-Dibromo-phenanthrenequinone Suppliers
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View Lastest Price from 3,6-Dibromo-phenanthrenequinone manufacturers
- Product
- 3,6-Dibromo-phenanthrenequinone 53348-05-3
- Price
- US $25.00/ASSAYS
- Min. Order
- 100ASSAYS
- Purity
- 99.5%
- Supply Ability
- 100 mt
- Release date
- 2024-11-15
- Product
- 3,6-Dibromo-phenanthrenequinone 53348-05-3
- Price
- US $8.00/KG
- Min. Order
- 1KG
- Purity
- ＞98% HPLC
- Supply Ability
- 20 tons
- Release date
- 2020-02-17
- Product
- 3,6-Dibromo-phenanthrenequinone 53348-05-3
- Price
- US $6.60-0.00/g
- Min. Order
- 500g
- Purity
- 98%
- Supply Ability
- 500G ,1KG , 100KG
- Release date
- 2019-12-23