1-(2-METHOXY-PHENYL)-ETHYLAMINE

Product Name: 1-(2-METHOXY-PHENYL)-ETHYLAMINE
CAS No.: 40023-74-3
Chemical Name: 1-(2-METHOXY-PHENYL)-ETHYLAMINE
Synonyms: AURORA KA-7736;ASINEX-REAG BAS 05269105;2-Methoxy-α-methylbenzylamine;1-(2-METHOXYPHENYL)ETHANAMINE;1-(2-METHOXY-PHENYL)-ETHYLAMINE;2-Methoxy-α-methylbenzenemethanamine;2-Methoxy-α-methylbenzenemethanamine;Benzenemethanamine, 2-methoxy-α-methyl-;Benzenemethanamine, 2-methoxy-a-methyl-;BenzeneMethanaMine, 2-Methoxy-.alpha.-Methyl-
CBNumber: CB1104943
Molecular Formula: C9H13NO
Formula Weight: 151.21
MOL File: Mol file

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1-(2-METHOXY-PHENYL)-ETHYLAMINE Property

Boiling point:: 244.1±23.0 °C(Predicted)
Density: 1.003±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 9.13±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: Xi
Risk Statements: 36
Safety Statements: 26
RIDADR: UN2735
HazardClass: IRRITANT
HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: M350150
Product name: 1-(2-Methoxyphenyl)ethylamine
Packaging: 500mg
Price: $175
Updated: 2021/12/16

Matrix Scientific

Product number: 018697
Product name: 1-(2-Methoxy-phenyl)-ethylamine
Packaging: 1g
Price: $299
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0032873
Product name: 1-(2-METHOXY-PHENYL)-ETHYLAMINE
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

Matrix Scientific

Product number: 018697
Product name: 1-(2-Methoxy-phenyl)-ethylamine
Packaging: 5g
Price: $885
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0032873
Product name: 1-(2-METHOXY-PHENYL)-ETHYLAMINE
Purity: 95.00%
Packaging: 2.5G
Price: $1227.82
Updated: 2021/12/16

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1-(2-METHOXY-PHENYL)-ETHYLAMINE Chemical Properties,Usage,Production

Synthesis

579-74-8

40023-74-3

GENERAL PROCEDURE: To a saturated NH4OAc ethanol solution (40 mL) was added activated zinc powder (5 eq.), 2'-methoxyacetophenone (1 eq.), NaBH3CN (3 eq.), and 30% aqueous ammonia solution (10 mL), in that order. The reaction mixture was stirred at 80 °C for 36 hours. After completion of the reaction, it was cooled to room temperature and concentrated under reduced pressure. The residue was dissolved with dichloromethane and adjusted to alkaline with 1 M NaOH aqueous solution (50 mL). The organic phase was separated and the aqueous phase was back-extracted with dichloromethane (2 x 25 mL). The organic phases were combined and acidified with HCl to pH 2.0. The organic layer was separated and the aqueous layer was extracted with dichloromethane (2 x 25 mL). After the aqueous layer was adjusted to pH 10.0 with NaOH, the organic layer was extracted with dichloromethane (3 × 25 mL). The organic layers were combined, dried with anhydrous Na2SO4 and the solvent was evaporated under reduced pressure to obtain the target product 1-(2-methoxyphenyl)ethylamine.

References

[1] Science, 2017, vol. 358, # 6361, p. 326 - 332
[2] Chemistry - A European Journal, 2014, vol. 20, # 1, p. 245 - 252
[3] Farmaco, 1991, vol. 46, # 7-8, p. 861 - 872
[4] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 13, p. 3592 - 3602
[5] Chirality, 2018, vol. 30, # 7, p. 900 - 906

1-(2-METHOXY-PHENYL)-ETHYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(2-METHOXY-PHENYL)-ETHYLAMINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 1-(2-METHOXY-PHENYL)-ETHYLAMINE 40023-74-3
Price: US $1.00-2.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100000KG
Release date: 2024-08-16

40023-74-3, 1-(2-METHOXY-PHENYL)-ETHYLAMINERelated Search:

AURORA KA-7736

ASINEX-REAG BAS 05269105

1-(2-METHOXYPHENYL)ETHANAMINE

1-(2-METHOXY-PHENYL)-ETHYLAMINE

2-Methoxy-α-methylbenzenemethanamine

2-Methoxy-α-methylbenzylamine

BenzeneMethanaMine, 2-Methoxy-.alpha.-Methyl-

Benzenemethanamine, 2-methoxy-a-methyl-

Benzenemethanamine, 2-methoxy-α-methyl-

2-Methoxy-α-methylbenzenemethanamine

40023-74-3